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21. 发明授权

US5162563A Process for preparing a diester of carboxylic acid 失效
标题翻译：制备羧酸酯的方法
公开(公告)号：US5162563A
公开(公告)日：1992-11-10
申请号：US599134
申请日：1990-10-17
申请人： Keigo Nishihira , Katsuhiko Mizutare , Shuji Tanaka
发明人： Keigo Nishihira , Katsuhiko Mizutare , Shuji Tanaka
IPC分类号： C07C68/00 , C07C69/96
CPC分类号： C07C68/00
摘要： A process for preparing a diester of carbonic acid which comprises bringing carbon monoxide into contact with an ester of nitrous acid in a vapor phase at a pressure greater than atmospheric pressure in the presence of a solid catalyst having (a) a platinum group metal or a compound thereof and (b) at least one metal compound of a metal selected from the group consisting of iron, copper, bismuth, cobalt, nickel and tin; carried on a carrier.

22. 发明授权

US06861563B2 Process for preparation of cyclododecanone 失效
标题翻译：环十二酮的制备方法
公开(公告)号：US06861563B2
公开(公告)日：2005-03-01
申请号：US10486735
申请日：2002-08-09
申请人： Ryoji Sugise , Shuji Tanaka , Takashi Doi , Masayuki Nishio , Sadao Niida , Tsunao Matsuura
发明人： Ryoji Sugise , Shuji Tanaka , Takashi Doi , Masayuki Nishio , Sadao Niida , Tsunao Matsuura
IPC分类号： C07C45/58 , C07C45/67
CPC分类号： C07C45/58 , C07C49/413
摘要： In the process for producing a cyclododecanone by isomerizing an epoxycyclododecane-containing starting material in the presence of an isomerization reaction catalyst containing lithium bromide and/or lithium iodide, in order to perform the reaction with high efficiency (high reaction rate) and high selectivity and stably produce a high-purity cyclododecanone in industry while maintaining a high-level reaction rate, the epoxycyclododecane-containing starting material is produced by contacting an epoxycyclododecadiene with hydrogen in the presence of a hydrogen-reduction catalyst and has a content of the hydroxyl group-containing cyclododecane compounds contained in the epoxycyclododecane-containing starting material controlled to 5 mol % or less.
摘要翻译：在通过在含有溴化锂和/或碘化锂的异构化反应催化剂的存在下异构化含环氧环十二烷的原料来制备环十二酮的方法中，为了以高效率（高反应速率）和高选择性进行反应，以及在保持高反应速率的同时稳定地生产高纯度环十二烷酮，含环氧环十二烷的原料是通过在氢还原催化剂存在下使环氧环十二烷与氢接触而制得的，含有环氧十二烷的原料中含有的环十二烷化合物控制在5摩尔％以下。

23. 发明授权

US06472498B2 Diaryl carbonate product and production of polycarbonate 有权
标题翻译：碳酸二芳酯产品和聚碳酸酯的生产
公开(公告)号：US06472498B2
公开(公告)日：2002-10-29
申请号：US09923466
申请日：2001-08-06
申请人： Ryoji Sugise , Shuji Tanaka , Kohichi Kashiwagi , Takashi Doi , Hirofumi Ii , Masayuki Nishio , Shinichi Yoshida , Yutaka Asada , Kazuo Miyamoto
发明人： Ryoji Sugise , Shuji Tanaka , Kohichi Kashiwagi , Takashi Doi , Hirofumi Ii , Masayuki Nishio , Shinichi Yoshida , Yutaka Asada , Kazuo Miyamoto
IPC分类号： C08G6400
CPC分类号： C07C68/08 , C07C69/96 , C08G64/307
摘要： A composition consisting essentially of a diaryl carbonate and contains a furan ring-containing compound in an amount of not more than 1 ppm is favorably employable for producing less colored polycarbonate.
摘要翻译：基本上由碳酸二芳酯组成并且含有不超过1ppm的含呋喃环的化合物的组合物有利地用于制备较少着色的聚碳酸酯。

24. 发明授权

US06191302B1 Process for producing alkyl nitrite 有权
标题翻译：亚硝酸烷基酯的制备方法
公开(公告)号：US06191302B1
公开(公告)日：2001-02-20
申请号：US09176372
申请日：1998-10-21
申请人： Keigo Nishihira , Shuji Tanaka , Shinichi Yoshida
发明人： Keigo Nishihira , Shuji Tanaka , Shinichi Yoshida
IPC分类号： C07C20302
CPC分类号： C07C201/04 , C07C203/00
摘要： An alkyl nitrite can be produced on an industrial scale with a high efficiency and with a low yield of by-products by the process wherein nitrogen oxide-containing feed gas is brought into an alkyl alcohol liquid in a distillation column reactor while circulating a liquid fraction, produced in the reactor and containing the alkyl alcohol, through a circulation path including a lower section of the reactor and a cooler to remove the reaction heat vigorously generated in the reactor, and while controlling the weight ratio of the circulating liquid fraction to the total alkyl alcohol fed into the reactor to 50:1 to 200:1, the molar ratio of the total alkyl alcohol fed to the reactor and contained in the circulating liquid fraction to nitrogen oxide in the feed gas to 20:1 to 150:1, and the content of the alkyl alcohol in the liquid fraction to 15 to 60% by weight; and the resultant gas fraction containing the target alkyl nitrite is collected from the reactor.
摘要翻译：亚硝酸烷基酯可以在工业规模上以高效率和低产率的副产物生产，其中将含氮氧化物的进料气体在蒸馏塔反应器中进入烷基醇液体，同时使液体馏分在反应器中生产并含有烷基醇，通过包括反应器的下部的循环路径和冷却器，以除去在反应器中剧烈产生的反应热，同时控制循环液体馏分与总的重量比将进料到反应器中的烷基醇的摩尔比为50:1至200:1，进料到反应器中并且包含在循环液体馏分中的总烷基醇与进料气体中的氮氧化物的摩尔比为20:1-150:1，并且液体馏分中的烷基醇的含量为15〜60重量％从反应器收集含有目标亚硝酸烷基酯的所得气体馏分。

25. 发明授权

US5705677A Diphenyl oxalate-phenol adduct, process for producing the adduct and method of producing diphenyl oxalate from the adduct 失效
标题翻译：草酸二苯酚 - 苯酚加合物，加合物的制备方法和从加合物生产草酸二苯酯的方法
公开(公告)号：US5705677A
公开(公告)日：1998-01-06
申请号：US757070
申请日：1996-11-26
申请人： Keigo Nishihira , Shuji Tanaka , Yuki Nishida , Hirofumi Ii , Satoru Fujitsu
发明人： Keigo Nishihira , Shuji Tanaka , Yuki Nishida , Hirofumi Ii , Satoru Fujitsu
IPC分类号： C07C69/017 , C07C69/36
CPC分类号： C07C69/017 , C07C69/36
摘要： A novel crystalline adduct of diphenyl oxalate and phenol in a molar ratio of 1:2 and having a high purity is produced by melting a mixture containing diphenyl oxalate and phenol at a temperature of 100.degree. C. or more; cooling the melt to a temperature of less than 100.degree. C. to allow a resultant adduct of diphenyl oxalate and phenol in a molar ratio of 1:2 to crystallize and deposit from the melt; and collecting the crystalline adduct. Diphenyl oxalate with a high purity is produced by melting the crystalline adduct to dissociate it into diphenyl oxalate and phenol, and evaporating away the dissociated phenol from the melt to collect the dissociated diphenyl oxalate.
摘要翻译：通过在100℃或更高的温度下熔化含有草酸二苯酯和苯酚的混合物，产生摩尔比为1:2且具有高纯度的草酸二苯酯和苯酚的新型结晶加合物; 将熔体冷却至低于100℃的温度，使所得到的草酸二苯酯和苯酚的摩尔比为1:2的加合物从熔体中结晶和沉积; 并收集结晶加合物。通过熔化结晶加合物将其分解成草酸二苯酯和苯酚，并将离解的苯酚从熔体中蒸发掉以收集离解的草酸二苯酯，从而产生高纯度的二苯基草酸盐。

26. 发明授权

US5631396A Process for continuously producing dimethyl carbonate 失效
标题翻译：连续生产碳酸二甲酯的方法
公开(公告)号：US5631396A
公开(公告)日：1997-05-20
申请号：US647164
申请日：1996-05-09
申请人： Keigo Nishihira , Shinichi Yoshida , Shuji Tanaka , Yutaka Asada
发明人： Keigo Nishihira , Shinichi Yoshida , Shuji Tanaka , Yutaka Asada
IPC分类号： B01J27/13 , C07B61/00 , C07C68/00 , C07C68/08 , C07C69/96
CPC分类号： C07C68/00
摘要： Dimethyl carbonate ((CH.sub.3 O).sub.2 CO) is continuously produced by a catalytic reaction (first step) of CO with CH.sub.3 NO.sub.2, with a significantly reduced loss of CH.sub.3 ONO by the process including a second step wherein (CH.sub.3 O).sub.2 CO in a reaction product gas of the first step is absorbed by dimethyl oxalate while contacting the resultant liquid fraction with CO to recover CH.sub.3 ONO, a third step wherein CH.sub.3 ONO is regenerated from NO in the condensed gas fraction produced in the second step and molecular oxygen and CH.sub.3 OH introduced into the third step, the resultant regenerated gas fraction being recycled and reused as a feed gas for the first step, and a fourth step wherein (CH.sub.3 O).sub.2 CO contained in the liquid fraction of the second step is collected.
摘要翻译：通过CO与CH3NO2的催化反应（第一步）连续制备碳酸二甲酯（（CH 3 O）2 CO），通过包括第二步骤的CH 3 NOO的显着降低的损失，其中（CH 3 O）2 CO在反应产物气体中的第一步被草酸二甲酯吸收，同时使所得液体馏分与CO接触以回收CH 3 NOO，第三步是在第二步产生的冷凝气体馏分中从NO再生CH3ONO，并将第三步中引入分子氧和CH3OH，所产生的再生气体馏分被再循环并重新用作第一步骤的进料气体;以及第四步骤，其中收集第二步骤的液体馏分中所含的（CH 3 O）2 CO。

27. 发明授权

US5315032A Method of producing an N-hydroxycarbamate compound 失效
标题翻译： N-羟基氨基甲酸酯化合物的制造方法
公开(公告)号：US5315032A
公开(公告)日：1994-05-24
申请号：US67551
申请日：1993-05-26
申请人： Keigo Nishihira , Shuji Tanaka , Katsuhiko Mizutare , Masahiro Kondo
发明人： Keigo Nishihira , Shuji Tanaka , Katsuhiko Mizutare , Masahiro Kondo
IPC分类号： C07C269/00 , C07C269/04 , C07C271/00 , C07C271/16 , C07C261/00
CPC分类号： C07C269/04
摘要： An N-hydroxycarbamate compound of the formula ROCONHOH in which R is C.sub.1-8 alkyl, C.sub.3-12 cycloalkyl, aryl or aralkyl group, is produced by reacting a carbonic acid diester of the formula ROCOOR in which R is as defined above, with hydroxylamine in the presence of a basic substance, for example, an alkali metal hydroxide or alkoxide.
摘要翻译：其中R是C 1-8烷基，C 3-12环烷基，芳基或芳烷基的式ROCONHOH的N-羟基氨基甲酸酯化合物是通过使式ROCOOR的碳酸二酯（其中R如上定义）与羟胺在碱性物质的存在下，例如碱金属氢氧化物或醇盐。

28. 发明授权

US4492792A Process for preparing 4-amino-5-dialkoxy-methylpyrimidine derivatives 失效
标题翻译： 4-氨基-5-二烷氧基 - 甲基嘧啶衍生物的制备方法
公开(公告)号：US4492792A
公开(公告)日：1985-01-08
申请号：US461191
申请日：1983-01-26
申请人： Kozo Fujii , Keigo Nishihira , Hiroyuki Sawada , Shuji Tanaka , Mamoru Nakai , Hiroshi Yoshida , Teruhiko Inoue
发明人： Kozo Fujii , Keigo Nishihira , Hiroyuki Sawada , Shuji Tanaka , Mamoru Nakai , Hiroshi Yoshida , Teruhiko Inoue
IPC分类号： C07D239/42 , C07D317/32 , C07D239/02
CPC分类号： C07D239/42 , C07C255/00
摘要： A process for preparing a 4-amino-5-dialkoxymethylpyrimidine derivative of the formula: ##STR1## which comprises reacting a propanenitrile derivative represented by the formula (I) or the novel compound represented by formula (II): ##STR2## with an amidine of the formula: ##STR3## wherein R.sup.1 to R.sup.6 are as defined in the specification. Also disclosed is a process for making the novel compounds of formula (II).
摘要翻译：制备下式的4-氨基-5-二烷氧基甲基嘧啶衍生物的方法：包括使由式（I）表示的丙腈衍生物或由式（II）表示的新化合物：（I）（II），其具有下式的脒：其中R 1至R 6如说明书中所定义。还公开了制备式（II）的新型化合物的方法。

29. 发明授权

US07714160B2 Process for producing alkyl nitrite 有权
标题翻译：亚硝酸烷基酯的制备方法
公开(公告)号：US07714160B2
公开(公告)日：2010-05-11
申请号：US10946475
申请日：2004-09-21
申请人： Ryoji Sugise , Shuji Tanaka , Hirofumi Ii , Kazuaki Mii
发明人： Ryoji Sugise , Shuji Tanaka , Hirofumi Ii , Kazuaki Mii
IPC分类号： C07C203/04
CPC分类号： C07C201/04 , C07C203/00
摘要： An alkyl nitrite is produced with high efficiency by bringing a nitrogen monoxide gas into contact with an aqueous solution of an alkyl alcohol and nitric acid in a reactor 2, which aqueous solution may be a liquid fraction generated in an alkyl nitrite-production process in which an alkyl alcohol is reacted with nitrogen monoxide and oxygen in a reaction column 1.
摘要翻译：通过在反应器2中使一氧化氮气体与烷基醇和硝酸的水溶液接触，可以高效率地生产亚硝酸烷基酯，该水溶液可以是在亚硝酸烷基酯制备方法中产生的液体馏分，其中在反应塔1中使烷基醇与一氧化氮和氧气反应。

30. 发明授权

US06844464B2 Process for producing alkyl nitrite 有权
公开(公告)号：US06844464B2
公开(公告)日：2005-01-18
申请号：US10388302
申请日：2003-03-13
申请人： Ryoji Sugise , Shuji Tanaka , Hirofumi Ii , Kazuaki Mii
发明人： Ryoji Sugise , Shuji Tanaka , Hirofumi Ii , Kazuaki Mii
IPC分类号： C07C201/04 , C07C203/00 , C07C203/02
CPC分类号： C07C201/04 , C07C203/00
摘要： An alkyl nitrite is produced with high efficiency by bringing a nitrogen monoxide gas into contact with an aqueous solution of an alkyl alcohol and nitric acid in a reactor 2, which aqueous solution may be a liquid fraction generated in an alkyl nitrite-production process in which an alkyl alcohol is reacted with nitrogen monoxide and oxygen in a reaction column 1.

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