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21. 发明授权

US06562478B1 Sealable multilayer film made of a grafted terpolymer 失效
标题翻译：由可接枝的三元共聚物制成的可密封多层膜
公开(公告)号：US06562478B1
公开(公告)日：2003-05-13
申请号：US09701941
申请日：2000-12-05
申请人： David Fischer , Bernd Lothar Marczinke , Werner Schöne , Franz Langhauser , Wolfgang Bidell , Roland Hingmann , Ulrich Moll , Meinolf Kersting , Günther Schweier , Peter John Vaughan Jones
发明人： David Fischer , Bernd Lothar Marczinke , Werner Schöne , Franz Langhauser , Wolfgang Bidell , Roland Hingmann , Ulrich Moll , Meinolf Kersting , Günther Schweier , Peter John Vaughan Jones
IPC分类号： B32B2732
CPC分类号： B32B27/08 , B29C47/0021 , B29C47/065 , B29C47/145 , B29C55/023 , B29K2995/0022 , B32B27/32 , B32B27/327 , B32B38/0008 , B32B2038/0028 , B32B2310/14 , B32B2553/00 , C08F210/06 , C08F210/16 , Y10T428/2495 , Y10T428/31913 , C08F210/08 , C08F2500/03 , C08F2500/20 , C08F210/14
摘要： A sealable coextruded film is made from at least one outer layer and from at least one base layer, where the outer layer is composed of a propylene terpolymer comprising from 80 to 99.5 mol % of structural units derived from propylene, from 0.2 to 15 mol % of structural units derived from ethene or from a C4-C6 1-olefin (I) and from 0.3 to 15 mol % of structural units derived from another C4-C12 1-olefin (II) different from the C4-C6 1-olefin (I), and where the propylene terpolymer has been prepared using metallocene catalysts.
摘要翻译：可密封的共挤出膜由至少一个外层和至少一个基层制成，其中外层由丙烯三元共聚物组成，丙烯三元共聚物包含80-99.5mol％的衍生自丙烯的结构单元，0.2-15mol％衍生自乙烯或来自C 4 -C 6 1-烯烃（I）的结构单元和0.3至15摩尔％的衍生自不同于C 4 -C 6 1-烯烃的另外的C 4 -C 12 1-烯烃（II）的结构单元（ I），并且其中使用茂金属催化剂制备丙烯三元共聚物。

22. 发明授权

US06521722B1 Gas-phase polymerization of C2-C8-alk-1-enes 失效
标题翻译： C2-C8-烷-1-烯的气相聚合
公开(公告)号：US06521722B1
公开(公告)日：2003-02-18
申请号：US09525063
申请日：2000-03-14
申请人： Wolfgang Bidell , Roland Hingmann , Franz Langhauser , Meinolf Kersting , Rainer Alexander Werner
发明人： Wolfgang Bidell , Roland Hingmann , Franz Langhauser , Meinolf Kersting , Rainer Alexander Werner
IPC分类号： C08F234
CPC分类号： C08F10/00 , C08F10/06 , C08F110/06 , C08F210/06 , Y10S526/901 , Y10S526/905 , C08F4/025 , C08F4/6465 , C08F2/34 , C08F4/6546 , C08F2500/12 , C08F2500/17 , C08F2500/24 , C08F210/16
摘要： In a process for the polymerization of C2-C8-alk-1-enes by means of a Ziegler-Natta catalyst system, in which polymerization is carried out from the gas phase in at least one reaction zone at from 40 to 120° C. and pressures of from 1 to 100 bar, the pressure and temperature in the reaction zone are set so that an operating point formed by these parameters in a pressure-temperature diagram is located at from 0.2 to 5.0 bar below the dew line of the respective reaction mixture above which condensation of the C2-C8-alk-1-enes occurs.
摘要翻译：在通过齐格勒 - 纳塔催化剂体系聚合C 2 -C 8 - 烷-1-烯的方法中，其中在至少一个反应区中的气相在40-120℃进行聚合。并且压力为1至100巴，反应区中的压力和温度被设定为使得在压力 - 温度图中由这些参数形成的操作点位于相应反应的露点以下0.2至5.0巴混合物，其中出现C2-C8-烷-1-烯的缩合。

23. 发明授权

US06204315B1 Non-flammable, thermoplastic molded materials based on polyphenylene ethers 失效
标题翻译：基于聚苯醚的不可燃，热塑性成型材料
公开(公告)号：US06204315B1
公开(公告)日：2001-03-20
申请号：US09194614
申请日：1998-11-30
申请人： Martin Weber , Robert Weiss , Walter Heckmann , Roland Hingmann , Hans-Joachim Hähnle
发明人： Martin Weber , Robert Weiss , Walter Heckmann , Roland Hingmann , Hans-Joachim Hähnle
IPC分类号： C08K542
CPC分类号： C08L51/04 , C08K5/49 , C08L25/06 , C08L33/26 , C08L53/00 , C08L71/12 , C08L2666/02 , C08L2666/04
摘要： Flame-retardant thermoplastic molding materials containing A) at least one polyphenylene ether, B) at least one vinylaromatic polymer, and C) at least one flameproofing agent furthermore comprise D) as an antidrip agent, a high molecular weight polymer based on acrylamide having a viscosity of more than about 1.5 mpas, measured in 0.1% strength aqueous solution at 25° C., and are used for the production of fibers, films and moldings.
摘要翻译：含有A）至少一种聚苯醚的阻燃热塑性成型材料，B）至少一种乙烯基芳族聚合物，和C）至少一种防火剂，还包含D）作为抗吸附剂，基于丙烯酰胺的高分子量聚合物，其粘度更高大约1.5mpas，在0.1％强度的水溶液中在25℃下测量，并且用于生产纤维，膜和模制品。

24. 发明授权

US09145674B2 Vacuum insulation panels comprising nanoporous polymer particles 有权
标题翻译：包含纳米孔聚合物颗粒的真空绝热板
公开(公告)号：US09145674B2
公开(公告)日：2015-09-29
申请号：US13594249
申请日：2012-08-24
申请人： Klaus Hahn , Elena Khazova , Jan Kurt Walter Sandler , Marc Fricke , Maria-Kristin Sommer , Roland Hingmann
发明人： Klaus Hahn , Elena Khazova , Jan Kurt Walter Sandler , Marc Fricke , Maria-Kristin Sommer , Roland Hingmann
IPC分类号： E04B1/80
CPC分类号： E04B1/803 , Y02A30/242 , Y02B80/12 , Y10T428/231
摘要： The invention relates to a vacuum insulation panel comprising a barrier film and a core material having a density in the range from 50 to 350 kg/m3, wherein the core material comprises a mixture of A) from 30 to 100 percent by weight of nanoporous polymer particles which have a cell count in the range from 1000 to 100 000 cells/mm, where at least 60 percent by weight of the nanoporous polymer particles have a particle size of less than 100 μm in the sieve analysis in accordance with DIN 66165, and B) from 0 to 70 percent by weight of pyrogenic or precipitated silica, and also a process for the production thereof.
摘要翻译：本发明涉及一种真空绝热板，其包括阻挡膜和密度在50至350kg / m 3范围内的芯材料，其中芯材料包括A）30至100重量％的纳米多孔聚合物细胞数在1000至100000个细胞/ mm范围内的颗粒，其中至少60重量％的纳米多孔聚合物颗粒在根据DIN 66165的筛分分析中具有小于100μm的粒度，以及 B）0至70重量％的热解或沉淀二氧化硅，以及其制备方法。

25. 发明申请

US20130052393A1 VACUUM INSULATION PANELS COMPRISING NANOPOROUS POLYMER PARTICLES 有权
标题翻译：包含纳米聚合物颗粒的真空绝缘板
公开(公告)号：US20130052393A1
公开(公告)日：2013-02-28
申请号：US13594249
申请日：2012-08-24
申请人： Klaus Hahn , Elena Khazova , Jan Kurt Walter Sandler , Marc Fricke , Maria-Kristin Sommer , Roland Hingmann
发明人： Klaus Hahn , Elena Khazova , Jan Kurt Walter Sandler , Marc Fricke , Maria-Kristin Sommer , Roland Hingmann
IPC分类号： B32B1/06 , B05D5/00
CPC分类号： E04B1/803 , Y02A30/242 , Y02B80/12 , Y10T428/231
摘要： The invention relates to a vacuum insulation panel comprising a barrier film and a core material having a density in the range from 50 to 350 kg/m3, wherein the core material comprises a mixture of A) from 30 to 100 percent by weight of nanoporous polymer particles which have a cell count in the range from 1000 to 100 000 cells/mm, where at least 60 percent by weight of the nanoporous polymer particles have a particle size of less than 100 μm in the sieve analysis in accordance with DIN 66165, and B) from 0 to 70 percent by weight of pyrogenic or precipitated silica, and also a process for the production thereof.
摘要翻译：本发明涉及一种真空绝热板，其包括阻挡膜和密度在50至350kg / m 3范围内的芯材料，其中芯材料包括A）30至100重量％的纳米多孔聚合物细胞数在1000至100000个细胞/ mm范围内的颗粒，其中至少60重量％的纳米多孔聚合物颗粒在根据DIN 66165的筛分分析中具有小于100μm的粒度，以及 B）0至70重量％的热解或沉淀二氧化硅，以及其制备方法。

26. 发明授权

US07196140B2 Highly flowable propylene block copolymers 有权
标题翻译：高流动性丙烯嵌段共聚物
公开(公告)号：US07196140B2
公开(公告)日：2007-03-27
申请号：US10296256
申请日：2001-05-23
申请人： Ulrich Dahn , Wolfgang Bidell , Hans-Jürgen Zimmermann , Roland Hingmann , Joachim Rösch , Günther Schweier , Jürgen Oelze
发明人： Ulrich Dahn , Wolfgang Bidell , Hans-Jürgen Zimmermann , Roland Hingmann , Joachim Rösch , Günther Schweier , Jürgen Oelze
IPC分类号： C08F297/08 , C08F297/00 , C08F4/64 , C08F4/642
CPC分类号： C08F297/08 , C08F10/06 , C08F110/06 , C08F210/06 , C08L53/00 , C08F2/001 , C08F2/34 , C08L2666/02 , C08F2500/12 , C08F2500/17 , C08F210/16
摘要： The invention relates to highly flowable propylene block copolymers that comprise 50 to 80 wt.-% of a propylene homopolymer and 10 to 70 wt.-% of a propylene copolymer having 5 to 50 wt.-% of a C2–C8 alk-1-ene polymerized into it that is different from propylene, and that are obtainable from the gaseous phase by a two-step polymerization by means of a Ziegler-Natta catalyst system. In a first polymerization step, the propylene is polymerized at a pressure of 10 to 50 bar, a temperature of 50 to 100° C. and an average dwelling time of the reaction mixture of 0.3 to 5 hours in the presence of at least 2.0% by volume, based on the total volume, of hydrogen. The propylene homopolymer obtained in said first polymerization step is transferred together with the Ziegler-Natta catalyst system into an intermediate container, expanded for 0.01 to 5 minutes to less than 5 bar and maintained at a temperature of 10 to 80° C. The pressure in the intermediate container is then increased by 5 to 60 bar by introducing under pressure a gaseous mixture, and the propylene homopolymer is then transferred to a second polymerization step together with the Ziegler-Natta catalyst system. In said second polymerization step, a mixture from propylene and a C2–C8 alk-1-ene is polymerized into the propylene homopolymer at a pressure of 10 to 50 bar, a temperature of 50 to 100° C. and an average dwelling time of 0.5 to 5 hours. The weight ratio between the monomers reacted in the first and those reacted in the second polymerization step are adjusted to be in the range of from 4:1 to 1:1.
摘要翻译：本发明涉及高流动性丙烯嵌段共聚物，其包含50至80重量％的丙烯均聚物和10至70重量％的丙烯共聚物，其具有5至50重量％的C 2 其中聚合成与丙烯不同的烷基-1-烯，并且可以通过采用齐格勒 - 纳塔催化剂体系的两步聚合由气相获得。在第一聚合步骤中，丙烯在10至50巴的压力，50至100℃的温度和在至少2.0％的存在下反应混合物的平均停留时间为0.3至5小时的聚合反应，，基于总体积的氢气。将所述第一聚合步骤中获得的丙烯均聚物与齐格勒 - 纳塔催化剂体系一起转移到中间容器中，膨胀0.01至5分钟至小于5巴，并保持在10至80℃的温度。然后通过在压力下引入气体混合物将中间容器增加5至60巴，然后将丙烯均聚物与齐格勒 - 纳塔催化剂体系一起转移到第二聚合步骤。在所述第二聚合步骤中，将丙烯和C 12 -C 13烷-1-烯的混合物在10至50巴的压力下聚合成丙烯均聚物，温度为50〜100℃，平均停留时间为0.5〜5小时。在第一聚合步骤中反应的单体和在第二聚合步骤中反应的单体之间的重量比被调节至4:1至1:1的范围内。

27. 发明申请

US20050038208A1 Highly flowable propylene block copolymers 有权
标题翻译：高流动性丙烯嵌段共聚物
公开(公告)号：US20050038208A1
公开(公告)日：2005-02-17
申请号：US10296256
申请日：2001-05-23
申请人： Ulrich Dahn , Wolfgang Bidell , Hans-Jurgen Zimmermann , Roland Hingmann , Joachim Rosch , Gunther Schweier , Jurgen Oelze
发明人： Ulrich Dahn , Wolfgang Bidell , Hans-Jurgen Zimmermann , Roland Hingmann , Joachim Rosch , Gunther Schweier , Jurgen Oelze
IPC分类号： C08J5/00 , C08F2/00 , C08F4/642 , C08F10/06 , C08F110/06 , C08F210/06 , C08F297/08 , C08L53/00 , D01F6/30
CPC分类号： C08F297/08 , C08F10/06 , C08F110/06 , C08F210/06 , C08L53/00 , C08F2/001 , C08F2/34 , C08L2666/02 , C08F2500/12 , C08F2500/17 , C08F210/16
摘要： The invention relates to highly flowable propylene block copolymers that comprise 50 to 80 wt.-% of a propylene homopolymer and 10 to 70 wt.-% of a propylene copolymer having 5 to 50 wt.-% of a C2-C8 alk-1-ene polymerized into it that is different from propylene, and that are obtainable from the gaseous phase by a two-step polymerization by means of a Ziegler-Natta catalyst system. In a first polymerization step, the propylene is polymerized at a pressure of 10 to 50 bar, a temperature of 50 to 100° C. and an average dwelling time of the reaction mixture of 0.3 to 5 hours in the presence of at least 2.0% by volume, based on the total volume, of hydrogen. The propylene homopolymer obtained in said first polymerization step is transferred together with the Ziegler-Natta catalyst system into an intermediate container, expanded for 0.01 to 5 minutes to less than 5 bar and maintained at a temperature of 10 to 80° C. The pressure in the intermediate container is then increased by 5 to 60 bar by introducing under pressure a gaseous mixture, and the propylene homopolymer is then transferred to a second polymerization step together with the Ziegler-Natta catalyst system. In said second polymerization step, a mixture from propylene and a C2-C8 alkylene is polymerized into the propylene homopolymer at a pressure of 10 to 50 bar, a temperature of 50 to 100° C. and an average dwelling time of 0.5 to 5 hours. The weight ratio between the monomers reacted in the first and those reacted in the second polymerization step are adjusted to be in the range of from 4:1 to 1:1.
摘要翻译：本发明涉及高流动性丙烯嵌段共聚物，其包含50至80重量％的丙烯均聚物和10至70重量％的丙烯共聚物，其具有5至50重量％的C 2 -C 8烷基-1 其与丙烯不同，并且可通过采用齐格勒 - 纳塔催化剂体系的两步聚合由气相获得。在第一聚合步骤中，丙烯在10至50巴的压力，50至100℃的温度和在至少2.0％的存在下反应混合物的平均停留时间为0.3至5小时的聚合反应，，基于总体积的氢气。将所述第一聚合步骤中获得的丙烯均聚物与齐格勒 - 纳塔催化剂体系一起转移到中间容器中，膨胀0.01至5分钟至小于5巴，并保持在10至80℃的温度。然后通过在压力下引入气体混合物将中间容器增加5至60巴，然后将丙烯均聚物与齐格勒 - 纳塔催化剂体系一起转移到第二聚合步骤。在所述第二聚合步骤中，将丙烯和C 2 -C 8亚烷基的混合物在10至50巴的压力，50至100℃的温度和0.5至5小时的平均停留时间内聚合成丙烯均聚物。在第一聚合步骤中反应的单体和在第二聚合步骤中反应的单体之间的重量比被调节至4:1至1:1的范围内。

28. 发明授权

US06245944B1 Process for producing substituted indanones 失效
标题翻译：制备取代茚满酮的方法
公开(公告)号：US06245944B1
公开(公告)日：2001-06-12
申请号：US09202091
申请日：1998-12-09
申请人： Carsten Süling , Heike Gregorius , Walter Dobler , Roland Hingmann , Bernhard Rieger , Ulf Dietrich , Jürgen Matthäus Wagner , Hans-Joachim Müller
发明人： Carsten Süling , Heike Gregorius , Walter Dobler , Roland Hingmann , Bernhard Rieger , Ulf Dietrich , Jürgen Matthäus Wagner , Hans-Joachim Müller
IPC分类号： C07C4546
CPC分类号： C07C49/675
摘要： A process for preparing a compound of the formula I where R1 and R2 are hydrogen or C1-C4-alkyl and R3 is C1-C10-alkyl, phenyl or C1-C4-alkyl-substituted phenyl, comprises reacting a compound II with a compound of the formula III where X is chlorine, bromine or iodine, in the presence of a Friedel-Crafts catalyst in one step to give a compound I.
摘要翻译：制备式I化合物的方法，其中R 1和R 2是氢或C 1 -C 4烷基，R 3是C 1 -C 10 - 烷基，苯基或C 1 -C 4烷基取代的苯基，包括使化合物II与式III其中X是氯，溴或碘，在Friedel-Crafts催化剂存在下，一步得到化合物I.

29. 发明授权

US06200922B1 Catalyst systems of the Ziegler-Natta type 失效
标题翻译：齐格勒 - 纳塔型催化剂系统
公开(公告)号：US06200922B1
公开(公告)日：2001-03-13
申请号：US08869761
申请日：1997-06-05
申请人： Stephan Hüffer , Wolfgang Bidell , Patrik Müller , Ulrich Moll , Roland Hingmann , Günther Schweier
发明人： Stephan Hüffer , Wolfgang Bidell , Patrik Müller , Ulrich Moll , Roland Hingmann , Günther Schweier
IPC分类号： B01J2106
CPC分类号： C08F10/00 , C08F110/06 , C08F4/6465 , C08F4/025 , C08F4/6546 , C08F2500/12 , C08F2500/24
摘要： The catalyst systems comprise as active constituents a) a titanium-containing solid component comprising a compound of titanium, a compound of magnesium, a halogen, an inorganic oxide as support and a carboxylic ester as electron donor compound, and also, as cocatalyst, b) an aluminum compound and c) optionally a further electron donor compound, wherein the inorganic oxide used has a pH of from 1 to 6, an average particle diameter of from 5 to 200 &mgr;m, an average primary particle diameter of from 1 to 20 &mgr;M and voids or channels having an average diameter of from 0.1 to 20 &mgr;m and a macroscopic share of the volume of the overall particle within the range from 5 to 30%.
摘要翻译：催化剂体系包括作为活性成分的含钛固体组分，其包含钛化合物，镁化合物，卤素，作为载体的无机氧化物和作为电子给体化合物的羧酸酯的化合物，以及作为助催化剂的b）铝化合物和任选的另外的电子给体化合物，其中使用的无机氧化物的pH为1至6，平均粒径为5至200μm，平均一次粒径为1至20μm，空隙或平均直径为0.1-20μm的通道，并且整个颗粒的体积的宏观份额在5至30％的范围内。

30. 发明授权

US6156691A Ziegler-Natta catalyst systems modified during their preparation 失效
标题翻译：齐格勒 - 纳塔催化剂体系在制备过程中改进
公开(公告)号：US6156691A
公开(公告)日：2000-12-05
申请号：US928394
申请日：1997-09-12
申请人： Stephan Huffer , Ulrich Moll , Ian David McKenzie , Franz Langhauser , Peter Kolle , Roland Hingmann , Gunther Schweier , Rainer Hemmerich , Jurgen Kerth
发明人： Stephan Huffer , Ulrich Moll , Ian David McKenzie , Franz Langhauser , Peter Kolle , Roland Hingmann , Gunther Schweier , Rainer Hemmerich , Jurgen Kerth
IPC分类号： C08F4/02 , C08F4/642 , C08F4/646 , C08F4/654 , C08F4/658 , C08F10/00 , B01J31/00
CPC分类号： C08F10/00
摘要： In catalyst systems of the Ziegler-Natta type modified during their preparation and comprising as active constituentsa) a titanium-containing solid component which is obtained by reacting a compound of titanium with a compound of magnesium, a halogen, an inorganic oxide as support, a C.sub.1 -C.sub.8 -alkanol and a carboxylic ester as electron donor compound,and also as cocatalystb) an aluminum compound andc) if desired, a further electron donor compound,the titanium-containing solid component a) is prepared by first, in a first stage, admixing an inorganic oxide as support with a solution of a chlorine-free compound of magnesium in an inert solvent, stirring this mixture for from 0.5 to 5 hours at from 10 to 120.degree. C. and subsequently reacting it while stirring continually in an inert solvent with a C.sub.1 -C.sub.8 -alkanol in an at least 1.3-fold excess, based on the compound of magnesium, to give a chlorine-free intermediate, then, without purification or extraction of the intermediate, adding a compound of trivalent or tetravalent titanium and a carboxylic ester as electron donor compound to this intermediate, stirring the resulting mixture for at least 30 minutes at from 20 to 130.degree. C., subsequently filtering off and washing the solid thus obtained and subsequently, in a second stage, extracting the solid obtained from the first stage in an inert solvent comprising at least 5% by weight of titanium tetrachloride and washing it with a liquid alkane.
摘要翻译：在其制备过程中改性的齐格勒 - 纳塔型催化剂体系中，包含作为活性成分的含钛固体成分a）通过使钛化合物与镁，卤素，无机氧化物作为载体反应而得到的含钛固体成分，作为电子给体化合物的C1-C8-链烷醇和羧酸酯，以及作为助催化剂的b）铝化合物，和c）如果需要，另外的电子给体化合物，含钛固体组分a）首先在第一阶段，将无机氧化物作为载体与无氯化合物的镁在惰性溶剂中的溶液混合，在10至120℃下搅拌该混合物0.5至5小时，随后在持续搅拌下反应在基于镁化合物的至少1.3倍过量的C 1 -C 8烷醇的惰性溶剂中，得到无氯中间体，然后不经纯化或萃取中间体，加入一种磅三价或四价钛和羧酸酯作为电子给体化合物，在20至130℃下搅拌所得混合物至少30分钟，随后过滤并洗涤由此获得的固体，随后在第二阶段，在包含至少5重量％的四氯化钛的惰性溶剂中萃取从第一阶段获得的固体，并用液体烷烃洗涤。

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