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21. 发明申请

US20130178586A1 HETEROPHASIC PROPYLENE COPOLYMER WITH EXCELLENT IMPACT/STIFFNESS BALANCE 有权
标题翻译：具有优异冲击/硬度平衡的异构丙烯共聚物
公开(公告)号：US20130178586A1
公开(公告)日：2013-07-11
申请号：US13813796
申请日：2011-08-01
申请人： Cornelia Kock , Petar Doshev , Elisabeth Potter , Guenter Gsellmann , Pauli Leskinen
发明人： Cornelia Kock , Petar Doshev , Elisabeth Potter , Guenter Gsellmann , Pauli Leskinen
IPC分类号： C08L23/14
CPC分类号： C08L23/14 , C08F210/06 , C08F297/086 , C08L23/12 , C08L23/16 , C08L2205/03 , C08L2205/035 , C08L2308/00 , C08L2314/02 , C08L2666/02 , C08F2/001 , C08F4/6492 , C08F4/6495 , C08F4/6465 , C08F210/16 , C08F2500/12 , C08F2500/17
摘要： Heterophasic propylene copolymer comprising a matrix (M) being a polypropylene, said polypropylene comprises at least three polypropylene fractions, the three polypropylene fractions differ from each other by the melt flow rate MFR2 (230° C.) and at least one of the three polypropylene fractions has a melt flow rate MFR2 (230° C.) in the range of 1.0 to 15.0 g/10 min, and an elastomeric propylene copolymer dispersed in said matrix, wherein the heterophasic propylene copolymer has a melt flow rate MFR2 (230° C.) of equal or more than 20.0 g/10 min, and the amorphous phase of the xylene cold soluble fraction of the heterophasic propylene copolymer has an intrinsic viscosity of equal or higher than 2.0 dl/g.
摘要翻译：包含基质（M）为聚丙烯的多相丙烯共聚物，所述聚丙烯包含至少三个聚丙烯部分，三个聚丙烯部分通过熔体流动速率MFR 2（230℃）彼此不同，并且三种聚丙烯中的至少一种熔体流动速率MFR2（230℃）在1.0至15.0g / 10min的范围内，和分散在所述基质中的弹性体丙烯共聚物，其中多相丙烯共聚物的熔体流动速率MFR 2（230℃ ）等于或大于20.0g / 10min，多相丙烯共聚物的二甲苯冷可溶部分的无定形相的特性粘度等于或高于2.0dl / g。

22. 发明申请

US20120015170A1 HIGH FLOW POLYPROPYLENE COMPOSITION 有权
标题翻译：高流动性聚丙烯组合物
公开(公告)号：US20120015170A1
公开(公告)日：2012-01-19
申请号：US13144522
申请日：2010-06-30
申请人： Petar Doshev , Pirjo Jaaskelainen , Saeid Kheirandish , Pauli Leskinen , Geir Kristian Johnsen , Hao Ding
发明人： Petar Doshev , Pirjo Jaaskelainen , Saeid Kheirandish , Pauli Leskinen , Geir Kristian Johnsen , Hao Ding
IPC分类号： C08L23/16 , C08L23/14 , B32B27/28 , C08L23/12
CPC分类号： C08L23/12 , C08K5/0083 , C08L23/14 , C08L23/142 , C08L2023/42 , C08L2666/06
摘要： The present invention relates to a high flow polypropylene composition comprising (A) a low molecular weight propylene homopolymer fraction and (B) a high molecular weight propylene copolymer fraction, having a comonomer content of not higher than 8 wt %, wherein the ratio between the MFR2 of fraction (A) and the MFR2 of fraction (B) is at least 3 and wherein the MFR2 of the entire composition is at least 5 g/10 min, the values of MFR2 being measured according to ISO 1133 (230° C., 2.16 kg load), and to processes for producing such compositions and to articles made there from.
摘要翻译：本发明涉及一种高流动聚丙烯组合物，其包含（A）低分子量丙烯均聚物部分和（B）共聚单体含量不高于8重量％的高分子量丙烯共聚物部分，其中，级分（A）的MFR 2和级分（B）的MFR 2为至少3，并且其中整个组合物的MFR 2为至少5g / 10min，MFR 2的值根据ISO 1133（230℃）测量，2.16kg负荷），以及用于生产这种组合物的方法和由其制成的制品。

23. 发明申请

US20110174415A1 METHOD TO PRODUCE VERY STIFF POLYPROPYLENE 失效
标题翻译：生产非常柔软的聚丙烯的方法
公开(公告)号：US20110174415A1
公开(公告)日：2011-07-21
申请号：US12998263
申请日：2009-10-06
申请人： Pauli Leskinen , Michiel Bergstra
发明人： Pauli Leskinen , Michiel Bergstra
IPC分类号： F16L9/00 , C08F110/06 , C08F10/06 , C08F2/01
CPC分类号： C08F110/06 , C08F10/06 , C08F210/06 , C08F2400/02 , C08F2/001 , C08F2/38 , C08F210/16 , C08F2500/04 , C08F2500/11 , C08F2500/12
摘要： The present invention relates to a process for the preparation of a propylene homo- or copolymer, comprising the following steps: (i) feeding propylene and hydrogen, and optionally one or more comonomers, to a reactor R1, wherein the hydrogen is fed to the reactor R1 in a periodically varying amount, (ii) preparing a first fraction of the propylene homo- or copolymer in the reactor R1 in the presence of a catalyst, (iii) transferring the first fraction to a reactor R2, and (iv) preparing a second fraction of the propylene homo- or copolymer in the reactor R2, wherein the melt flow rate MFR (2.16 kg, 230° C.) of the propylene homo- or copolymer is higher than the melt flow rate MFR (2.16 kg, 230° C.) of the first fraction.
摘要翻译：本发明涉及一种制备丙烯均聚物或共聚物的方法，包括以下步骤：（i）将丙烯和氢气以及任选的一种或多种共聚单体进料到反应器R1中，其中将氢气供给到反应器R1以周期性变化的量，（ii）在催化剂存在下，在反应器R1中制备丙烯均聚物或共聚物的第一部分，（iii）将第一部分转移到反应器R2，和（iv）制备丙烯均聚物或共聚物在反应器R2中的第二部分，其中丙烯均聚物或共聚物的熔体流动速率MFR（2.16kg，230℃）高于熔体流动速率MFR（2.16kg，230 ℃）。

24. 发明授权

US06872682B1 α-olefin polymerization catalyst system and its use for the polymerization of α-olefins 失效
标题翻译： α-烯烃聚合催化剂体系及其在α-烯烃聚合中的应用
公开(公告)号：US06872682B1
公开(公告)日：2005-03-29
申请号：US09890357
申请日：2000-02-11
申请人： Kauno Alastalo , Pauli Leskinen
发明人： Kauno Alastalo , Pauli Leskinen
IPC分类号： C08F4/655 , C08F4/44 , C08F4/657 , C08F10/00 , B01J31/00 , B01J37/00 , C08F4/02 , C08F4/60
CPC分类号： C08F10/00 , C08F2/44 , C08F4/6492 , C08F4/6491
摘要： A catalyst system for the polymerization of α-olefins prepared by a process which includes catalyst activation whereby a solid transitional metal compound is contacted with an organoaluminum compound and catalyst prepolymerization whereby a premonomer is prepolymerized in the presence of the activated catalyst. High activity, low fines polymerization can be achieved if in the first step of catalyst activation a first reaction mixture is prepared by contacting the solid transitional metal compound with a first organoaluminum compound in the presence of an oil and in the second step, the first reaction mixture is contacted with a second organoaluminum compound to give a second reaction mixture, the second organoaluminum compound being the same as or different from the first organoaluminum compound.
摘要翻译：用于通过包括催化剂活化的方法制备的α-烯烃聚合的催化剂体系，其中固体过渡金属化合物与有机铝化合物接触，催化剂预聚合，由此在活化催化剂存在下将预聚单体预聚合。如果在催化剂活化的第一步骤中，通过在油的存在下使固体过渡金属化合物与第一有机铝化合物接触来制备第一反应混合物，并且在第二步骤中，第一反应混合物与第二有机铝化合物接触，得到第二反应混合物，第二有机铝化合物与第一有机铝化合物相同或不同。

25. 发明授权

US06576710B1 Multi-stage process for the preparation of &agr;-olefin polymers having controlled stereoregularity and products prepared thereof 失效
标题翻译：用于制备具有受控的立构规整性的α-烯烃聚合物的多阶段方法及其制备的产物
公开(公告)号：US06576710B1
公开(公告)日：2003-06-10
申请号：US09890796
申请日：2001-09-26
申请人： Päivi Huovinen , Pauli Leskinen , Thomas Garoff
发明人： Päivi Huovinen , Pauli Leskinen , Thomas Garoff
IPC分类号： C08L2300
CPC分类号： C08F10/06 , C08F10/00 , C08F110/06 , C08F4/642 , C08F4/6465 , C08F4/6492 , C08F2/001 , C08F2500/12
摘要： The invention relates to the preparation of an &agr;-olefin polymer product having controlled stereoregularity, comprising the successive step of: (i) producing a first polymerization product by contacting under polymerization conditions an &agr;-olefin monomer with a polymerization catalyst system comprising a transition metal compound, a first organometal compound and a stereoregulating external electron donor to give a first polymerization reaction mixture; (ii) producing a second polymerization product by contacting additional &agr;-olefin monomer with the first polymerization reaction mixture. The controlled stereoregularity is achieved in such a way that in step (ii) the second polymerization product is produced in the presence of a stereoregularity controlling agent. The stereoregularity controlling agent e.g. a second organometal compound which contains, on an atom basis, more halogen per metal than the first organometal compound, or 0.01-1.2 % of an olefin which is not said &agr;-olefin monomer, calculated on the total molar amount of olefin and &agr;-olefin monomer.
摘要翻译：本发明涉及具有受控立构规整性的α-烯烃聚合物产物的制备，其包括以下连续步骤：（i）通过在聚合条件下使α-烯烃单体与包含过渡金属的聚合催化剂体系接触来制备第一聚合产物化合物，第一有机金属化合物和立体调节外电子给体，得到第一聚合反应混合物; （ii）通过使附加的α-烯烃单体与第一聚合反应混合物接触而产生第二聚合产物。控制的立构规整性以这样的方式实现：在步骤（ii）中，第二聚合产物是在立体规则性控制剂的存在下制备的。立构规整性控制剂例如第二有机金属化合物，其以原子计含有比第一有机金属化合物更多的卤素/金属，或0.01-1.2％的不是所述α-烯烃单体的烯烃，以烯烃和α-烯烃的总摩尔量计算，烯烃单体。

26. 发明授权

US6040260A Process for the preparation of repolymerized catalyst composition and a process for polymerizing .alpha.-olefins 失效
标题翻译：制备再聚合催化剂组合物的方法和聚合α-烯烃的方法
公开(公告)号：US6040260A
公开(公告)日：2000-03-21
申请号：US876442
申请日：1997-06-16
申请人： Ismo Pentti , Pauli Leskinen
发明人： Ismo Pentti , Pauli Leskinen
IPC分类号： C08F4/609 , C08F4/64 , C08F4/654 , C08F10/00 , C08F110/06
CPC分类号： C08F10/00 , C08F110/06 , Y10S526/903 , Y10S526/904
摘要： The present invention concerns prepolymerized catalyst composition for polymerization of .beta.-olefins, a process for the preparation thereof and a process for polymerization of .beta.-olefins. According to the polymerization process a procatalyst composition containing a transition metal is prepolymerized with a monomer in order to produce a prepolymerized Ziegler-Natta type catalyst composition and said catalyst composition is contacted with an alpha-olefin monomer, in particular with ethylene or propylene, for preparing a polymer. According to the invention the procatalyst composition is preferably prepolymerized in a medium which is inert to the catalyst components, the viscosity of the medium being so high that the catalyst does not substantially settle in this medium. Because the catalyst composition according to the invention does not have to be dried before being fed into the medium, its activity is high before and during polymerization.
摘要翻译：本发明涉及用于聚合β-烯烃的预聚合催化剂组合物，其制备方法和β-烯烃聚合方法。根据聚合方法，将含有过渡金属的原料催化剂组合物与单体预聚合以制备预聚合的齐格勒 - 纳塔型催化剂组合物，并将所述催化剂组合物与α-烯烃单体，特别是与乙烯或丙烯接触，用于制备聚合物。根据本发明，原催化剂组合物优选在对催化剂组分是惰性的介质中预聚合，介质的粘度如此之高，使得催化剂基本上不会沉淀在该介质中。因为根据本发明的催化剂组合物在进料到介质中之前不必被干燥，因此在聚合之前和聚合过程中其活性很高。

27. 发明授权

US5385992A Method for the dosage of a fluidized polymerization catalyst into a polymerization reactor 失效
标题翻译：流化聚合催化剂进入聚合反应器的方法
公开(公告)号：US5385992A
公开(公告)日：1995-01-31
申请号：US119150
申请日：1993-10-26
申请人： Jukka Koskinen , Klaus Nyfors , Pauli Leskinen
发明人： Jukka Koskinen , Klaus Nyfors , Pauli Leskinen
IPC分类号： B01J8/24 , B01J8/00 , C08F2/00 , C08F2/14 , F04B7/06
CPC分类号： B01J8/003 , B01J8/002 , B01J8/0035 , F04B7/06
摘要： A method is provided for controlling the dosage of a fluidized polymerizing catalyst into a polymerization reactor. The method comprises mixing a solid polymerization catalyst with wax and feeding the flowing catalyst-wax mixture through a pipe to the dosage pump. The inlet opening of the cylinder of the dosage pump is opened to draw catalyst-wax mixture through the inlet opening by means of the back motion of the piston. The inlet opening is then closed and the outlet opening is opened. Flowing catalyst-wax mixture is then pressed from the cylinder through the outlet opening by means of the back motion of the piston. The outlet opening is then closed. Opening and closing of the inlet and outlet openings is carried out by rotating an intermediate pipe arranged between the cylinder and piston so that a transmission opening in the intermediate pipe moves upon either the inlet or outlet opening. The intermediate pipe surface always covers at least one of the inlet or outlet openings.
摘要翻译： PCT No.PCT / FI92 / 00080 Sec。 371日期：1993年10月26日 102（e）日期1993年10月26日PCT 1991年3月20日PCT公布。第WO92 / 16747号公报日期为1992年10月1日。提供了一种控制流化聚合催化剂进入聚合反应器的剂量的方法。该方法包括将固体聚合催化剂与蜡混合，并将流动的催化剂 - 蜡混合物通过管道送入剂量泵。剂量泵的气缸的入口打开，通过活塞的反向运动通过进口开启催化剂 - 蜡混合物。然后关闭入口，并打开出口。然后通过活塞的反向运动，将流动的催化剂 - 蜡混合物从汽缸压出出口。然后关闭出口。通过旋转布置在气缸和活塞之间的中间管来进行入口和出口的打开和关闭，使得中间管中的传动开口在入口或出口开口上移动。中间管表面总是覆盖入口或出口中的至少一个。

28. 发明申请

US20120190784A1 HETEROPHASIC POLYPROPYLENE COPOLYMER COMPOSITION 有权
标题翻译：异构聚丙烯共聚物组合物
公开(公告)号：US20120190784A1
公开(公告)日：2012-07-26
申请号：US13261048
申请日：2010-06-15
申请人： Werner Posch , Michael Tranninger , Pauli Leskinen , Bo Malm , Sybille Simon , Norbert Reichelt
发明人： Werner Posch , Michael Tranninger , Pauli Leskinen , Bo Malm , Sybille Simon , Norbert Reichelt
IPC分类号： C08L23/10 , C08K7/06 , C08K7/14 , C08K3/34 , C08K3/26
CPC分类号： C08L23/10 , B29C45/0001 , C08F110/06 , C08F210/06 , C08F297/08 , C08L23/0815 , C08L23/16 , C08L2205/02 , C08L2207/02 , C08L2314/02 , C08F2/001 , C08L2666/06 , C08F210/16 , C08F2500/12 , C08F2500/17 , C08F2500/11
摘要： Heterophasic polypropylene composition comprising (A) 45 to 70 wt % of a propylene homo- or copolymer matrix with an MFR2 in accordance with ISO 1133 (230° C., 2.16 kg load) of ≧80 g/10 min and (B) 25 to 40 wt % of an elastomeric propylene-ethylene copolymer, having an intrinsic viscosity IV (ISO 1628, with decalin as solvent) of ≧ 3.3 dl/g and an ethylene content of 20 to 50 wt %, (C) 0-15 wt % of an elastomeric ethylene/alpha-olefin random copolymer (D) 3-25 parts per weight of inorganic filler, the heterophasic polypropylene compositions having a total MFR2 (230° C./2.16 kg) in accordance with ISO 1133 of ≧5 g/10 min, a Charpy notched impact strength according to ISO 179/1eA at +23° C. of ≧15.0 kJ/m2, preferably ≧25.0 kJ/m2, a minimum value for the Charpy notched impact strength according to ISO 179/1eA at −200 C of ≧7.0 kJ/m2, preferably ≧10.0 kJ/m2 and a tensile modulus according to ISO 527-3 of ≧1200 MPa; their preparation and use for producing injection moulded articles being free of flow marks.
摘要翻译：多相聚丙烯组合物，其包含（A）45至70重量％的丙烯均聚物或共聚物基体，其具有根据ISO 1133（230℃，2.16kg负荷）≥80g/ 10min的MFR 2和（B）25 至40重量％的丙烯 - 乙烯共聚物，其特性粘度IV（ISO 1628，作为溶剂的十氢化萘）为≥3.3dl/ g，乙烯含量为20〜50重量％，（C）为0〜15重量％％的弹性体乙烯/α-烯烃无规共聚物（D）3-25重量份的无机填料，根据ISO 1133的总共MFR 2（230℃/ 2.16kg）的多相聚丙烯组合物为≥5g / 10分钟，根据ISO 179 / 1eA在+ 23℃下的夏比缺口冲击强度为≥15.0kJ/ m 2，优选≥25.0kJ/ m 2，根据ISO 179 / 1eA的夏比缺口冲击强度的最小值在-200℃，≥7.0kJ/ m 2，优选≥10.0kJ/ m 2，并且根据ISO 527-3的≧1200MPa的拉伸模量; 它们的制备和用于生产没有流痕的注塑制品。

29. 发明申请

US20110294940A1 METHOD FOR IMPROVING FLOWABILITY OF HETEROPHASIC POLYPROPYLENE POWDER 有权
标题翻译：改善异丙基聚丙烯粉末流动性的方法
公开(公告)号：US20110294940A1
公开(公告)日：2011-12-01
申请号：US12998704
申请日：2009-11-18
申请人： Pauli Leskinen , Olli Tuominen , Veli-Matti Keinänen
发明人： Pauli Leskinen , Olli Tuominen , Veli-Matti Keinänen
IPC分类号： C08L23/12 , C08K3/34 , C08F2/01 , C08L23/16
CPC分类号： C08F255/02 , B01J8/24 , B01J19/2435 , B01J2219/0004 , C08F110/06 , C08F210/06 , C08F297/083 , C08K3/34 , C08L23/12 , C08L23/16 , C08L51/06 , C08L2207/02 , C08L2308/00 , C08L2314/02 , C08F2/001 , C08L2666/06 , C08L2666/02 , C08F210/16 , C08F2500/17 , C08F2500/18 , C08F2500/24
摘要： Method for the preparation of a sticky high impact heterophasic polypropylene (HECO) in a reactor facility comprising in series (i) a first reaction system, (ii) a first conveying line connecting the first reactor system with a second reactor system comprising an outlet, (iii) a second conveying line connecting the outlet with a purge bin comprising a feeder, and (iv) a conveying system being connected with the feeder, and the preparation of said heterophasic polypropylene (HECO) comprises the steps in the order of (a) producing in said first reactor system the polypropylene matrix (M), (b) transferring at least a part of said polypropylene to said second reactor system via the first conveying line, (c) producing in said second reactor system the elastomeric copolymer obtaining the heterophasic polypropylene (HECO), (d) discharging said heterophasic polypropylene (HECO) from said second reactor system via the outlet, (e) transferring said discharged heterophasic polypropylene (HECO) via the second conveying line to said purge bin comprising said feeder, and (f) transferring further said discharged heterophasic polypropylene (HECO) from said purge bin via said feeder to said conveying system, the produced heterophasic polypropylene (HECO) is provided with an additive, said additive is fed to the produced heterophasic polypropylene (α) at the outlet of the second reactor system, or (β) at the feeder (F) of the purge bin (PB).
摘要翻译：在反应器设备中制备粘性高冲击多相聚丙烯（HECO）的方法，其包括串联（i）第一反应体系，（ii）将第一反应器系统与包含出口的第二反应器系统连接的第一输送管线，（iii）将出口连接到包括进料器的净化箱的第二输送管线，以及（iv）与进料器连接的输送系统，并且所述多相聚丙烯（HECO）的制备包括以下步骤：（a ）在所述第一反应器系统中生产所述聚丙烯基质（M），（b）经由所述第一输送管线将至少一部分所述聚丙烯转移到所述第二反应器系统，（c）在所述第二反应器系统中产生所述弹性共聚物，多相聚丙烯（HECO），（d）通过出口从所述第二反应器系统排出所述多相聚丙烯（HECO），（e）将所述排出的异相聚丙烯（HECO）vi 第二输送管线到包括所述进料器的清洗箱，和（f）将所述排出的多相聚丙烯（HECO）从所述进料槽经由所述进料器进一步传送到所述输送系统，所生产的异相聚丙烯（HECO）具有添加剂，所述添加剂在第二反应器系统的出口处供给到生产的异相聚丙烯（α），或者在清洗箱（PB）的进料器（F）处进料。

30. 发明申请

US20110224387A1 PREPARATION OF PROPYLENE COPOLYMER WITH DYNAMICALLY OPERATED REACTOR 有权
标题翻译：具有动态反应器的丙烯共聚物的制备
公开(公告)号：US20110224387A1
公开(公告)日：2011-09-15
申请号：US12998307
申请日：2009-10-06
申请人： Michiel Bergstra , John Severn , Torvald Vestberg , Pauli Leskinen , Bo Malm , Olli Tuominen , Pirjo Jääskeläinen
发明人： Michiel Bergstra , John Severn , Torvald Vestberg , Pauli Leskinen , Bo Malm , Olli Tuominen , Pirjo Jääskeläinen
IPC分类号： C08F210/06 , C08F2/01 , C08F4/64
CPC分类号： C08F210/06 , C08F210/16 , C08F2400/02 , C08F2/00 , C08F2/38 , C08F2/001 , C08F2500/12 , C08F2500/17 , C08F2500/19 , C08F2500/04
摘要： The present invention relates to a process for the preparation of a propylene copolymer P1 having ethylene-derived comonomer units, which comprises the following steps: (i) introducing propylene, ethylene, and hydrogen into a polymerisation reactor R1, wherein the ethylene is fed to the polymerisation reactor R1 in a periodically varying amount, (ii) preparing the propylene copolymer in the polymerisation reactor R1 in the presence of a catalyst.
摘要翻译：本发明涉及一种制备具有乙烯衍生的共聚单体单元的丙烯共聚物P1的方法，其包括以下步骤：（i）将丙烯，乙烯和氢气引入聚合反应器R1中，其中将乙烯进料至聚合反应器R1以周期性变化的量，（ii）在催化剂存在下在聚合反应器R1中制备丙烯共聚物。

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