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21. 发明申请

US20090220684A1 PROCESS OF APPLYING A COATING SYSTEM 有权
标题翻译：涂布系统的应用过程
公开(公告)号：US20090220684A1
公开(公告)日：2009-09-03
申请号：US12465884
申请日：2009-05-14
申请人： Mark Daniel Gorman , Brian Thomas Hazel , Brett Allen Rohrer Boutwell , Ramgopal Darolia
发明人： Mark Daniel Gorman , Brian Thomas Hazel , Brett Allen Rohrer Boutwell , Ramgopal Darolia
IPC分类号： B05D5/12
CPC分类号： C23C10/02 , C23C10/48 , C23C10/50 , Y10T428/12458 , Y10T428/12736 , Y10T428/1275 , Y10T428/12861 , Y10T428/12875 , Y10T428/12944 , Y10T428/26 , Y10T428/265
摘要： A coating process for an article having a substrate formed of a metal alloy that is prone to the formation of a secondary reaction zone (SRZ). The coating process forms a coating system that includes an aluminum-containing overlay coating and a stabilizing layer between the overlay coating and the substrate. The overlay coating contains aluminum in an amount greater by atomic percent than the metal alloy of the substrate, such that there is a tendency for aluminum to diffuse from the overlay coating into the substrate. The stabilizing layer is predominantly or entirely formed of at least one platinum group metal (PGM), namely, platinum, rhodium, iridium, and/or palladium. The stabilizing layer is sufficient to inhibit diffusion of aluminum from the overlay coating into the substrate so that the substrate remains essentially free of an SRZ that would be deleterious to the mechanical properties of the alloy.
摘要翻译：一种具有由容易形成二次反应区（SRZ）的金属合金形成的基材的制品的涂布方法。涂覆工艺形成涂层系统，其包括含铝覆盖涂层和覆盖涂层与基底之间的稳定层。覆盖涂层含有比基底的金属合金更大原子百分数的铝，使得铝从覆盖涂层扩散到基底中的倾向。稳定层主要或完全由至少一种铂族金属（PGM），即铂，铑，铱和/或钯形成。稳定层足以抑制铝从覆盖涂层扩散到衬底中，使得衬底基本上不含对合金的机械性能有害的SRZ。

22. 发明申请

US20080160201A1 Thermal barrier coating/environmental barrier coating system for a ceramic-matrix composite (CMC) article to improve high temperature capability 有权
标题翻译：陶瓷基复合材料（CMC）制品的隔热涂层/环境屏障涂层系统，以提高高温能力
公开(公告)号：US20080160201A1
公开(公告)日：2008-07-03
申请号：US11899336
申请日：2007-09-05
申请人： Brett Allen Rohrer Boutwell , Irene Spitsberg , Christine Govern , Bangalore A. Nagaraj , Brian Thomas Hazel , Ramgopal Darolia , Curtis Alan Johnson , Yan Gao , Mark Daniel Gorman
发明人： Brett Allen Rohrer Boutwell , Irene Spitsberg , Christine Govern , Bangalore A. Nagaraj , Brian Thomas Hazel , Ramgopal Darolia , Curtis Alan Johnson , Yan Gao , Mark Daniel Gorman
IPC分类号： B05D1/38
CPC分类号： C04B41/009 , C04B41/52 , C04B41/89 , C04B2111/0025 , C23C28/042 , C23C28/322 , C23C28/345 , C23C28/3455 , F01D5/288 , F05D2230/90 , F05D2300/2118 , F05D2300/50211 , F05D2300/611 , C04B41/4527 , C04B41/5096 , C04B41/5035 , C04B41/522 , C04B41/5024 , C04B41/5037 , C04B41/5031 , C04B41/5042 , C04B41/5044 , C04B41/4529 , C04B35/565 , C04B35/584 , C04B35/806
摘要： In accordance with an embodiment of the invention, an article is provided. The article comprises a substrate comprised of silicon containing material, an environmental barrier coating (EBC) overlying the substrate and a thermal barrier coating (TBC) on the environmental barrier coating. The thermal barrier coating comprising a compound having a rhombohedral phase.
摘要翻译：根据本发明的实施例，提供了一种制品。该制品包括由含硅材料构成的衬底，覆盖衬底的环境阻挡涂层（EBC）和环境屏障涂层上的热障涂层（TBC）。该热障涂层包含具有菱面体相的化合物。

23. 发明授权

US07326441B2 Coating systems containing beta phase and gamma-prime phase nickel aluminide 有权
标题翻译：包含β相和γ相的镍化合物的涂层体系
公开(公告)号：US07326441B2
公开(公告)日：2008-02-05
申请号：US10904844
申请日：2004-12-01
申请人： Ramgopal Darolia , Joseph David Rigney , Gillion Herman Marijnissen , Eric Richard Irma Carolus Vergeldt , Annejan Bernard Kloosterman
发明人： Ramgopal Darolia , Joseph David Rigney , Gillion Herman Marijnissen , Eric Richard Irma Carolus Vergeldt , Annejan Bernard Kloosterman
IPC分类号： B05D3/02
CPC分类号： F01D5/288 , C23C4/18 , C23C10/02 , C23C10/48 , C23C10/50 , C23C10/52 , C23C28/021 , C23C28/321 , C23C28/3455 , C23C30/00 , F05D2230/90 , F05D2300/611 , Y10T428/12611 , Y10T428/12618 , Y10T428/12736 , Y10T428/12937 , Y10T428/12944 , Y10T428/12951 , Y10T428/24967 , Y10T428/264 , Y10T428/265 , Y10T428/31678
摘要： A coating and process for depositing the coating on a substrate. The coating is a nickel aluminide overlay coating of predominantly the beta (NiAl) and gamma-prime (Ni3Al) intermetallic phases, and is suitable for use as an environmental coating and as a bond coat for a thermal barrier coating (TBC). The coating can be formed by depositing nickel and aluminum in appropriate amounts to yield the desired beta+gamma prime phase content. Alternatively, nickel and aluminum can be deposited so that the aluminum content of the coating exceeds the appropriate amount to yield the desired beta+gamma prime phase content, after which the coating is heat treated to diffuse the excess aluminum from the coating into the substrate to yield the desired beta+gamma prime phase content.
摘要翻译：用于将涂层沉积在基材上的涂层和方法。涂层是主要是β（NiAl）和γ-prime（Ni 3 Al 3 Al）金属间相的镍铝化物覆盖涂层，并且适合用作环境涂层和作为粘合涂层隔热涂层（TBC）。可以通过以适当的量沉积镍和铝来形成所述涂层，以产生所需的β+γ初相相含量。或者，可以沉积镍和铝，使得涂层的铝含量超过适当的量以产生所需的β+γ初相相含量，之后热处理涂层以将过量的铝从涂层扩散到基底中产生期望的β+γ'相相含量。

24. 发明授权

US07244467B2 Process for a beta-phase nickel aluminide overlay coating 有权
标题翻译：一种β相镍铝覆盖涂层的工艺
公开(公告)号：US07244467B2
公开(公告)日：2007-07-17
申请号：US10604368
申请日：2003-07-15
申请人： Theodore Robert Grossman , Ramgopal Darolia , Joseph David Rigney
发明人： Theodore Robert Grossman , Ramgopal Darolia , Joseph David Rigney
IPC分类号： C23C16/00
CPC分类号： C23C14/5886 , C23C4/18 , C23C14/16 , C23C26/00 , C23C28/3215 , C23C28/345 , C23C28/3455
摘要： A process for forming a beta-phase nickel aluminide (NiAl) overlay coating that is suitable for use as a bond coat for a thermal barrier coating (TBC). The overlay coating is deposited by a method that produces a generally columnar grain structure in which grains extend through the coating such that at least some grain boundaries are open at the coating surface. The coating is then peened with a particulate media, followed by heating the overlay coating to a temperature sufficient to cause the overlay coating to recrystallize and form new grain boundaries that are not open to the outer surface of the coating and significantly less susceptible to accelerated oxidation than the original grain boundaries. The particulate media is formed of a composition containing nickel and aluminum, such that an oxide scale that forms on the surface of the coating after the peening operation is substantially free of deleterious oxide compounds, notably iron-containing spinels.
摘要翻译：用于形成适合用作热障涂层（TBC）的粘合涂层的β-相镍铝化物（NiAl）覆盖涂层的方法。覆盖涂层通过产生大致柱状晶粒结构的方法沉积，其中晶粒延伸穿过涂层，使得至少一些晶界在涂层表面开口。然后用颗粒介质对涂层进行喷丸处理，然后将覆盖涂层加热至足以使覆盖涂层再结晶并形成不对涂层外表面开放的新晶粒边界，并显着降低易受加速氧化影响的温度比原来的晶界。颗粒介质由包含镍和铝的组合物形成，使得在喷丸操作之后在涂层表面上形成的氧化皮基本上不含有害氧化物化合物，特别是含铁尖晶石。

25. 发明申请

US20070160859A1 Layered thermal barrier coatings containing lanthanide series oxides for improved resistance to CMAS degradation 审中-公开
标题翻译：包含镧系元素氧化物的分层热障涂层，以改善对CMAS降解的抵抗力
公开(公告)号：US20070160859A1
公开(公告)日：2007-07-12
申请号：US11327091
申请日：2006-01-06
申请人： Ramgopal Darolia , Bangalore A. Nagaraj , Douglas G. Konitzer , Mark D. Gorman , Ming Fu
发明人： Ramgopal Darolia , Bangalore A. Nagaraj , Douglas G. Konitzer , Mark D. Gorman , Ming Fu
IPC分类号： B32B15/04
CPC分类号： C23C28/042 , C23C28/048 , C23C28/321 , C23C28/3215 , C23C28/325 , C23C28/345 , C23C28/3455 , C23C28/36 , F01D5/288 , F05D2300/2118 , Y02T50/67 , Y02T50/671 , Y02T50/6765
摘要： A coating applied as a two layer system. The outer layer is an oxide of a group IV metal selected from the group consisting of zirconium oxide, hafnium oxide and combinations thereof, which are doped with an effective amount of a lanthanum series oxide. These metal oxides doped with a lanthanum series addition comprises a high weight percentage of the outer coating. As used herein, lanthanum series means an element selected from the group consisting of lanthanum (La), cerium (Ce), praseodymium (Pr), neodymium (Nd), promethium (Pm), samarium (Sm), europium (Eu), gadolinium (Gd), terbium (Tb), dysprosium (Dy), holmium (Ho), erbium (Er), thulium (Tm), ytterbium (Yb), lutetium (Lu) and combinations thereof, and lanthanum series oxides are oxides of these elements. When the zirconium oxide is doped with an effective amount of a lanthanum series oxide, a dense reaction layer is formed at the interface of the outer layer of TBC and the CMAS. This dense reaction layer prevents CMAS infiltration below it. The second layer, or inner layer underlying the outer layer, comprises a layer of partially stabilized zirconium oxide.
摘要翻译：涂层作为两层体系。外层是掺杂有有效量的镧系氧化物的选自氧化锆，氧化铪及其组合的IV族金属的氧化物。掺杂有镧系列添加剂的这些金属氧化物包括外涂层的高重量百分比。如本文所用，镧系指选自镧（La），铈（Ce），镨（Pr），钕（Nd），ium（Pm），钐（Sm），铕（Eu），钆（Gd），铽（Tb），镝（Dy），钬（Ho），铒（Er），ium（Tm），镱（Yb），镥（Lu）及其组合，以及镧系氧化物是这些元素。当氧化锆掺杂有效量的镧系氧化物时，在TBC的外层和CMAS的界面处形成致密的反应层。这种致密的反应层可防止CMAS渗透在其下方。外层的第二层或内层包含部分稳定的氧化锆层。

26. 发明申请

US20070020399A1 Diffusion barrier and protective coating for turbine engine component and method for forming 审中-公开
标题翻译：用于涡轮发动机部件的扩散阻挡层和保护涂层以及成型方法
公开(公告)号：US20070020399A1
公开(公告)日：2007-01-25
申请号：US11168660
申请日：2005-06-28
申请人： Mark Gorman , Bangalore Nagaraj , Ramgopal Darolia
发明人： Mark Gorman , Bangalore Nagaraj , Ramgopal Darolia
IPC分类号： B05D3/00 , B05D3/04 , B05D1/36 , H05H1/24 , B05D1/08 , B05D3/02
CPC分类号： C25D5/48 , C23C4/02 , C23C4/18 , C23C28/322 , C23C28/345 , C23C28/3455 , C23C28/36 , C25D5/34 , F01D5/288 , F05D2230/90 , F05D2300/143 , F05D2300/21 , F05D2300/2112 , F05D2300/2118 , F05D2300/22 , F05D2300/228 , F05D2300/2281 , F05D2300/611 , Y02T50/67 , Y02T50/6765
摘要： A turbine engine component comprising a substrate made of a nickel-base or cobalt-base superalloy, a non-metallic oxide or nitride diffusion barrier layer overlying the substrate, and a protective coating overlying the barrier layer, the protective coating comprising at least one platinum group metal selected from the group consisting of platinum, palladium, rhodium, ruthenium and iridium. The diffusion barrier layer may be a deposited or thermally grown oxide material, especially aluminum oxide. The protective coating may be heat treated to increase homogeneity of the coating and adherence with the substrate. The component typically further comprises a ceramic thermal barrier coating overlying the protective coating. Also disclosed are methods for forming a protective coating system on the turbine engine component by forming the non-metallic oxide or nitride diffusion barrier layer on the substrate and then depositing the platinum group metal on top of the barrier layer.
摘要翻译：一种涡轮发动机部件，包括由镍基或钴基超合金制成的基板，覆盖在基板上的非金属氧化物或氮化物扩散阻挡层以及覆盖在阻挡层上的保护涂层，所述保护涂层包含至少一种铂选自铂，钯，铑，钌和铱的组金属。扩散阻挡层可以是沉积的或热生长的氧化物材料，特别是氧化铝。可以对保护涂层进行热处理以增加涂层的均匀性和与基材的粘合性。该组件通常还包括覆盖保护涂层的陶瓷热障涂层。还公开了通过在衬底上形成非金属氧化物或氮化物扩散阻挡层然后将铂族金属沉积在阻挡层的顶部上来在涡轮发动机部件上形成保护涂层系统的方法。

27. 发明申请

US20060121294A1 Low thermal conductivity thermal barrier coating system and method therefor 失效
标题翻译：低热导率热障涂层系统及其方法
公开(公告)号：US20060121294A1
公开(公告)日：2006-06-08
申请号：US11006367
申请日：2004-12-06
申请人： Brett Allen Boutwell , Ramgopal Darolia , Curtis Johnson , Irene Spitsberg , Mark Gorman , Yan Gao
发明人： Brett Allen Boutwell , Ramgopal Darolia , Curtis Johnson , Irene Spitsberg , Mark Gorman , Yan Gao
IPC分类号： B32B15/04 , B32B9/00
CPC分类号： C04B41/009 , C04B35/486 , C04B41/5042 , C04B41/87 , C04B2111/0025 , C04B2235/3224 , C04B2235/3225 , C04B2235/3227 , C04B2235/3229 , C04B2235/76 , C04B2235/767 , C23C4/11 , C23C28/321 , C23C28/3215 , C23C28/325 , C23C28/345 , C23C28/3455 , C23C30/00 , F01D5/288 , F05D2230/90 , F05D2300/611 , C04B41/4527 , C04B35/565 , C04B35/806
摘要： In accordance with an embodiment of the invention, a thermal barrier coating for inclusion in a thermal barrier coating system is provided. The thermal barrier coating comprises a compound having a rhombohedral phase. In accordance with another embodiment of the invention, a thermal barrier coating is provided that comprises a compound having the formula of: A4B3O12, wherein A is at least one rare earth element; and B is selected from the group consisting of Zr, Hf and mixtures thereof.
摘要翻译：根据本发明的实施例，提供了用于包含在热障涂层系统中的热障涂层。热障涂层包括具有菱面体相的化合物。根据本发明的另一个实施方案，提供了一种热障涂层，其包含具有下列结构式的化合物：A 4 S 3 N 12 O / >其中A是至少一种稀土元素; B选自Zr，Hf及其混合物。

28. 发明申请

US20060035102A1 Strengthened bond coats for thermal barrier coatings 失效
标题翻译：加强热障涂层的粘合层
公开(公告)号：US20060035102A1
公开(公告)日：2006-02-16
申请号：US11248249
申请日：2005-10-13
申请人： Ramgopal Darolia , Joseph Rigney , Gillion Marijnissen , Eric Richard Vergeldt , Annejan Kloosterman
发明人： Ramgopal Darolia , Joseph Rigney , Gillion Marijnissen , Eric Richard Vergeldt , Annejan Kloosterman
IPC分类号： B32B15/00 , B32B15/04
CPC分类号： C23C28/3215 , C23C28/34 , C23C28/341 , C23C28/345 , C23C28/3455 , C23C28/36 , Y10T428/12493 , Y10T428/12535 , Y10T428/12576 , Y10T428/12611 , Y10T428/12618 , Y10T428/12736 , Y10T428/12806 , Y10T428/12875 , Y10T428/12931 , Y10T428/12937 , Y10T428/12944 , Y10T428/25 , Y10T428/252 , Y10T428/256 , Y10T428/265
摘要： A strengthened bond coat for improving the adherence of a thermal barrier coating to an underlying metal substrate to resist spallation without degrading oxidation resistance of the bond coat. The bond coat comprises a bond coating material selected from the group consisting of overlay alloy coating materials, aluminide diffusion coating materials and combinations thereof. Particles comprising a substantially insoluble bond coat strengthening compound and having a relatively fine particle size of about 2 microns or less are dispersed within at least the upper portion of the bond coat in an amount sufficient to impart strengthening to the bond coat, and thus limit ratcheting or rumpling thereof.
摘要翻译：一种增强的粘合涂层，用于改善热障涂层对底层金属基材的粘附性，以抵抗剥离而不降低粘结涂层的抗氧化性。粘合涂层包括选自覆盖合金涂层材料，铝化物扩散涂层材料及其组合的粘合涂层材料。包含基本上不溶性的粘合涂层强化化合物并且具有约2微米或更小的相对较细的粒度的颗粒以足以赋予粘结涂层强化的量分散在粘合涂层的至少上部内部，从而限制棘轮或其皱纹。

29. 发明申请

US20060029723A1 METHOD FOR REPAIRING COATED COMPONENTS USING NIAL BOND COATS 有权
标题翻译：使用NIAL BOND COATS修复涂层组件的方法
公开(公告)号：US20060029723A1
公开(公告)日：2006-02-09
申请号：US10714430
申请日：2003-11-13
申请人： Joseph Rigney , Ching-Pang Lee , Ramgopal Darolia
发明人： Joseph Rigney , Ching-Pang Lee , Ramgopal Darolia
IPC分类号： C23C16/52 , B05D3/00
CPC分类号： B23P6/002 , C23C10/02 , C23C10/60 , C23C28/321 , C23C28/3215 , C23C28/345 , C23C28/3455 , C23C28/36 , C25D3/50 , C25D7/00 , C25D7/008 , F05B2230/31 , F05B2230/90 , F05C2253/12
摘要： According to an embodiment of the invention, a method for repairing a coated high pressure turbine blade, which has been exposed to engine operation, to restore coated airfoil contour dimensions of the blade, and improve upon the prior bond coat is disclosed. The method comprises providing an engine run high pressure turbine blade including a base metal substrate made of a nickel-based alloy and having thereon a thermal barrier coating system. The thermal barrier coating system comprises a diffusion bond coat on the base metal substrate and a top ceramic thermal barrier coating comprising a yttria stabilized zirconia material. The top ceramic thermal barrier coating has a nominal thickness t. The method further comprises removing the thermal barrier coating system, wherein a portion of the base metal substrate also is removed, and determining the thickness of the base metal substrate removed. The portion of the base metal substrate removed has a thickness, Δt. The method also comprises applying a β phase NiAl overlay coating to the substrate, and determining the difference in thickness, Δx, between the β phase NiAl overlay coating and the previously removed bond coat. The method further comprises reapplying the top ceramic thermal barrier coating to a nominal thickness of t+Δt-Δx, wherein Δt compensates for the portion of removed base metal substrate. Advantageously, the coated airfoil contour dimensions of the high pressure turbine blade are restored to about the coated dimensions preceding the engine run.
摘要翻译：根据本发明的实施例，公开了一种已经暴露于发动机操作的用于修复涂覆的高压涡轮机叶片以恢复叶片的被覆翼型轮廓尺寸并改进先前的粘结涂层的方法。该方法包括提供一种发动机运行的高压涡轮叶片，其包括由镍基合金制成的基底金属基底并且具有热障涂层系统。热障涂层系统包括在基底金属基底上的扩散粘合涂层和包含氧化钇稳定的氧化锆材料的顶部陶瓷热障涂层。顶部陶瓷热障涂层具有标称厚度t。该方法还包括去除热障涂层系统，其中基底金属衬底的一部分也被去除，并且确定移除的母体金属衬底的厚度。去除的贱金属基材的部分厚度为Deltat。该方法还包括将β相NiAl覆盖涂层施加到基底上，并确定β相NiAl覆盖涂层与先前去除的粘结涂层之间的厚度差异Deltax。该方法还包括将顶部陶瓷热障涂层重新施加到t + Deltat-Deltax的标称厚度，其中Deltat补偿去除的基底金属基底的部分。有利地，高压涡轮机叶片的被覆翼型轮廓尺寸恢复到发动机运行之前的涂层尺寸。

30. 发明申请

US20050271514A1 COATING AND COATING PROCESS INCORPORATING RAISED SURFACE FEATURES FOR AN AIR-COOLED SURFACE 有权
标题翻译：包含空气冷却表面的提高表面特性的涂层和涂层工艺
公开(公告)号：US20050271514A1
公开(公告)日：2005-12-08
申请号：US10906903
申请日：2005-03-11
申请人： Ching-Pang Lee , Robert Schafrik , Ramgopal Darolia , Joseph Rigney
发明人： Ching-Pang Lee , Robert Schafrik , Ramgopal Darolia , Joseph Rigney
IPC分类号： B32B15/16 , C08F2/48 , C23C4/02 , C23C4/08 , C23C14/02 , C23C14/04 , C23C14/16 , C23C16/06 , C23C28/00 , F23M5/00 , F23R3/00 , F28F13/18
CPC分类号： C23C4/02 , C23C4/073 , C23C4/08 , C23C14/025 , C23C14/044 , C23C14/16 , C23C28/021 , C23C28/022 , F05B2240/11 , F05B2250/60 , F05B2260/224 , F05C2253/12 , F23M5/00 , F23M2900/05004 , F23R3/002 , F28F13/18 , F28F13/185 , Y10T428/12063 , Y10T428/12493 , Y10T428/12639 , Y10T428/12646 , Y10T428/12931 , Y10T428/12944 , Y10T428/12993
摘要： A coating and coating process for incorporating surface features on an air-cooled substrate surface of a component for the purpose of promoting heat transfer from the component. The coating process generally comprises depositing a first metallic coating material on the surface of the component using a first set of coating conditions to form a first environmental coating layer, and then depositing a second metallic coating material using a second set of coating conditions that differ from the first set, such that an outer environmental coating layer is formed having raised surface features that cause the surface of the outer environmental coating layer to be rougher than the surface of the first environmental coating layer.
摘要翻译：用于将部件的空气冷却基板表面上的表面特征引入到涂层和涂覆方法中，以促进从部件的热传递。涂覆方法通常包括使用第一组涂覆条件在组件的表面上沉积第一金属涂层材料以形成第一环境涂层，然后使用第二组涂覆条件沉积第二金属涂层材料第一组，使得外部环境涂层形成具有使外部环境涂层的表面比第一环境涂层的表面更粗糙的凸起表面特征。

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