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21. 发明授权

US07754840B2 Bimodal high density polyethlyene 有权
标题翻译：双峰高密度聚乙烯
公开(公告)号：US07754840B2
公开(公告)日：2010-07-13
申请号：US10635864
申请日：2003-08-06
申请人： Donald R. Loveday , David H. McConville , John F. Szul , Kersten Anne Erickson , Simon Mawson , Tae Hoon Kwack , Frederick J. Karol , David James Schreck
发明人： Donald R. Loveday , David H. McConville , John F. Szul , Kersten Anne Erickson , Simon Mawson , Tae Hoon Kwack , Frederick J. Karol , David James Schreck
IPC分类号： C08F110/02 , B29C73/00 , F16L55/16 , F16L11/00
CPC分类号： C08F10/02 , C08F4/659 , C08F4/65912 , C08F4/65916 , C08F4/6592 , C08F10/00 , C08F210/16 , C08F2420/04 , C08L23/0815 , C08L23/16 , C08L2205/02 , C08L2314/06 , Y10S526/943 , C08F2/00 , C08F4/025 , C08L2666/04 , C08F210/14 , C08F2500/12 , C08F2500/04 , C08F2500/02 , C08F2500/01 , C08F2500/26 , C08F2500/05 , C08F4/64148 , C08F4/65904 , C08F4/64158 , C08F4/64144 , C08F4/64151
摘要： The present invention is directed to a bimodal polyethylene comprising ethylene derived units and units derived from at least one of a C4 to C12 olefin; wherein the polyethylene has a density of from 0.940 to 0.970 g/cm3; an I21/I2 of 80 or more; a residual Group 4 metal content of 2.0 ppm or less: a Mw/Mn of from 20 to 60; and wherein the polyethylene comprises a high molecular weight component and a low molecular weight component, the high molecular weight component present from 40 to 60 weight percent based on the total polyethylene, and wherein the bimodal polyethylene has a weight avenge molecular weight Mw of 180,000 a.m.u. or more.
摘要翻译：本发明涉及包含乙烯衍生单元和衍生自C 4 -C 12烯烃中的至少一种的单元的双峰聚乙烯; 其中聚乙烯的密度为0.940-0.970g / cm3; 80以上的I21 / I2 残留的4族金属含量为2.0ppm以下：Mw / Mn为20〜60; 并且其中所述聚乙烯包含高分子量组分和低分子量组分，所述高分子量组分占总聚乙烯的40至60重量％，并且其中所述双峰聚乙烯具有18,000重量分子量的分子量Mw。或者更多。

22. 发明授权

US07223825B2 Single catalyst low, medium and high density polyethylenes 有权
公开(公告)号：US07223825B2
公开(公告)日：2007-05-29
申请号：US11438624
申请日：2006-05-22
申请人： Rainer Kolb , John F. Szul
发明人： Rainer Kolb , John F. Szul
IPC分类号： C08F4/64 , C08F10/02
CPC分类号： C08F10/00 , C08F4/65912 , C08F4/65916 , C08F4/65925 , C08F210/16 , Y10S526/901 , Y10S526/905 , C08F2/34 , C08F210/14 , C08F2500/12 , C08F2500/24
摘要： A method of polymerizing olefins comprising combining in one embodiment ethylene and optionally one or more α-olefins with a catalyst composition in a continuous polymerization reactor at a pressure of less than 10,000 kPa; wherein the catalyst composition comprises a hafnocene; and isolating a polyethylene having a density in the range of from 0.930 to 0.975 g/cm3. Also provided is a method of transitioning a continuous polymerization reactor from production of a low density polyethylene to a medium or high density polyethylene. Also provided is a medium to high density polyethylene suitable for injection or rotomolding applications. Also provided is a single catalyst composition suitable for such needs.

23. 发明授权

US06897273B2 Catalyst composition, method of polymerization and polymer therefrom 失效
标题翻译：催化剂组合物，聚合方法和聚合物
公开(公告)号：US06897273B2
公开(公告)日：2005-05-24
申请号：US09729557
申请日：2000-12-04
申请人： John F. Szul , Tae Hoon Kwalk , David James Schreck , Simon Mawson , Matthew G. McKee , Kersten Anne Terry , Mark G. Goode , Gregory T. Whiteker , Eric A. Lucas
发明人： John F. Szul , Tae Hoon Kwalk , David James Schreck , Simon Mawson , Matthew G. McKee , Kersten Anne Terry , Mark G. Goode , Gregory T. Whiteker , Eric A. Lucas
IPC分类号： C08J5/18 , C08F4/642 , C08F4/646 , C08F4/659 , C08F4/6592 , C08F10/00 , C08F10/02 , C08F210/16 , C08L23/08 , C08F4/44 , B01J31/38
CPC分类号： C08F10/02 , C08F4/659 , C08F4/65912 , C08F4/65925 , C08F210/16 , C08L23/0815 , C08L2314/06 , Y10S526/943 , C08F2/34 , C08F4/65916 , C08F4/65904 , C08L2666/04 , C08F210/14 , C08F2500/12 , C08F2500/26
摘要： This invention relates to a process to polymerize olefin(s) comprising combining a solution, slurry or solid comprising one or more bulky ligand metallocene catalyst compounds, an optional support, and or one or more activator(s) with a solution comprising one or more phenoxide catalyst compounds, and thereafter, introducing one or more olefin(s) and the combination into a polymerization reactor. This invention also relates to a polymer of ethylene wherein the polymer has a density of 0.910 to 0.930 g/cc, a melt index of 0.3 to 2.0 dg/min, and a 15 to 35 μm thick film of the polymer has a 45° gloss of 60 or more, a haze of 7% or less, and a dart impact of 600 g or more.
摘要翻译：本发明涉及聚合烯烃的方法，包括将包含一种或多种庞大配体茂金属催化剂化合物，任选的载体和/或一种或多种活化剂的溶液，浆料或固体与包含一种或多种酚氧化物催化剂化合物，然后将一种或多种烯烃和组合引入聚合反应器中。本发明还涉及一种乙烯聚合物，其中聚合物的密度为0.910至0.930g / cc，熔体指数为0.3至2.0dg / min，而15至35μm厚的聚合物膜具有45°的光泽度为60以上，雾度为7％以下，落镖冲击为600g以上。

24. 发明授权

US06586544B2 Solution feed of multiple catalysts 有权
公开(公告)号：US06586544B2
公开(公告)日：2003-07-01
申请号：US10122778
申请日：2002-04-15
申请人： John F. Szul , Kersten Anne Erickson , Simon Mawson , David James Schreck , Mark G. Goode , Paul T. Daniell , Matthew G. McKee , Clark C. Williams
发明人： John F. Szul , Kersten Anne Erickson , Simon Mawson , David James Schreck , Mark G. Goode , Paul T. Daniell , Matthew G. McKee , Clark C. Williams
IPC分类号： C08F442
CPC分类号： C08F210/16 , C08F4/65912 , C08F4/65916 , C08F4/6592 , C08F10/00 , C08F10/02 , C08L23/0815 , C08L2205/02 , C08L2314/06 , Y10S526/943 , C08F4/025 , C08F4/65904 , C08F4/659 , C08L2666/04 , C08F210/14 , C08F2500/12 , C08F2500/04 , C08F2500/02 , C08F2500/01 , C08F2500/26 , C08F4/64044
摘要： This invention relates to methods to introduce multiple catalysts, activators or catalyst systems into a gas phase reactor.

25. 发明授权

US06399722B1 Solution feed of multiple catalysts 有权
标题翻译：多种催化剂的溶液进料
公开(公告)号：US06399722B1
公开(公告)日：2002-06-04
申请号：US09451792
申请日：1999-12-01
申请人： John F. Szul , Kersten Anne Erickson , Simon Mawson , David James Schreck , Mark G. Goode , Paul T. Daniell , Matthew G. McKee , Clark C. Williams
发明人： John F. Szul , Kersten Anne Erickson , Simon Mawson , David James Schreck , Mark G. Goode , Paul T. Daniell , Matthew G. McKee , Clark C. Williams
IPC分类号： C08F442
CPC分类号： C08F210/16 , C08F4/65912 , C08F4/65916 , C08F4/6592 , C08F10/00 , C08F10/02 , C08L23/0815 , C08L2205/02 , C08L2314/06 , Y10S526/943 , C08F4/025 , C08F4/65904 , C08F4/659 , C08L2666/04 , C08F210/14 , C08F2500/12 , C08F2500/04 , C08F2500/02 , C08F2500/01 , C08F2500/26 , C08F4/64044
摘要： This invention relates to methods to introduce multiple catalysts, activators or catalyst systems into a gas phase reactor.
摘要翻译：本发明涉及将多种催化剂，活化剂或催化剂体系引入气相反应器的方法。

26. 发明授权

US08754177B2 Polymerization process 有权
标题翻译：聚合过程
公开(公告)号：US08754177B2
公开(公告)日：2014-06-17
申请号：US12637349
申请日：2009-12-14
申请人： Donna J. Crowther , John F. Szul
发明人： Donna J. Crowther , John F. Szul
IPC分类号： C08F4/653 , C08F4/642 , C08F4/6592 , C08F210/02
CPC分类号： C08F10/00 , C08F4/65912 , C08F4/65927 , C08F210/16 , Y10S526/943 , C08F4/65904 , C08F210/08 , C08F2500/12
摘要： The invention relates to a polymerization process, the polymerization process includes contacting a cyclic bridged metallocene catalyst represented by the following formula: LA(A)LBMQn wherein A is a divalent group bound to each of LA and LB; each of LA and LB are bound to M, and each Q is bound to M; LA and LB are independently selected from the group consisting of cyclopentadienyl ligands and substituted cyclopentadienyl ligands; A is a divalent bridging group comprising a heterocyclic ring comprising from 3 to 6 carbon atoms and one silyl, thus forming a 4 to 7 member divalent ring; M is a Group 4, 5, or 6 transition metal; Q is independently a halogen, a hydride, or a hydrocarbyl radical having from 1 to 20 carbon atoms; wherein n is 1 or 2; with an activator, and optionally a support, to form an activated catalyst and, subsequently, contacting the activated catalyst with ethylene and optionally, at least one C3-C8 alpha olefin comonomer.
摘要翻译：本发明涉及聚合方法，聚合方法包括使由下式表示的环状桥连金属茂催化剂：LA（A）LBMQn，其中A是与LA和LB各自结合的二价基团; LA和LB各自与M结合，每个Q与M相连; LA和LB独立地选自环戊二烯基配体和取代的环戊二烯基配体; A是包含含有3至6个碳原子的杂环和1个甲硅烷基的二价桥连基，从而形成4至7元的二价环; M是第4,5或6族过渡金属; Q独立地为卤素，氢化物或具有1至20个碳原子的烃基; 其中n为1或2; 与活化剂和任选的载体形成活化的催化剂，随后使活化的催化剂与乙烯和任选的至少一种C 3 -C 8α-烯烃共聚单体接触。

27. 发明授权

US08497329B2 Methods of controlling polymer properties 有权
标题翻译：控制聚合物性能的方法
公开(公告)号：US08497329B2
公开(公告)日：2013-07-30
申请号：US12523400
申请日：2008-01-18
申请人： Rainer Kolb , James M. Farley , John F. Szul , Mark P. Ossowski
发明人： Rainer Kolb , James M. Farley , John F. Szul , Mark P. Ossowski
IPC分类号： C08F4/6592 , C08F210/02
CPC分类号： C08F10/02 , C08F210/16 , C08F2400/02 , Y10S526/943 , C08F2/001 , C08F2/00 , C08F210/14 , C08F2500/12 , C08F2500/05 , C08F2500/24
摘要： The invention generally provides for methods for controlling polymer properties. In particular, invention provides for methods for controlling the comonomer composition distribution of polyolefins such as ethylene alpha-olefin copolymers by altering at least one or more of the following parameters: the molar ratio of hydrogen to ethylene, the molar ratio of comonomer to ethylene, the partial pressure of ethylene, and the reactor temperature without substantially changing the density and/or the melt index of the copolymer.
摘要翻译：本发明通常提供了控制聚合物性质的方法。特别地，本发明提供了通过改变至少一个或多个以下参数来控制聚烯烃如乙烯α-烯烃共聚物的共聚单体组成分布的方法：氢与乙烯的摩尔比，共聚单体与乙烯的摩尔比，乙烯的分压和反应器温度，而基本上不改变共聚物的密度和/或熔体指数。

28. 发明授权

US08476464B2 Alkylene oxide purification systems 有权
标题翻译：环氧烷净化系统
公开(公告)号：US08476464B2
公开(公告)日：2013-07-02
申请号：US13567135
申请日：2012-08-06
申请人： John F. Szul , James H. McCain , Floyd L. Pfeffer , Harvey E. Andresen , Phillip R. Fairchild , Kent E. Newman
发明人： John F. Szul , James H. McCain , Floyd L. Pfeffer , Harvey E. Andresen , Phillip R. Fairchild , Kent E. Newman
IPC分类号： C07D301/32
CPC分类号： C07D301/32
摘要： Embodiments of the present disclosure provide processes, columns, and systems for removing acetaldehyde from alkylene oxide in a feed stream and for providing an alkylene oxide-water stream that can be directly transferred to a glycol reaction process. The alkylene oxide purification column includes a first section to convert a feed stream into a gas phase portion and a liquid phase portion and a second section located in the column above the first section to separate alkylene oxide from the acetaldehyde, water, and other impurities that enter the second section from the first section.
摘要翻译：本公开的实施方案提供了用于从进料流中的环氧烷除去乙醛并提供可直接转移到二醇反应过程的环氧烷 - 水流的方法，塔和系统。环氧烷纯化塔包括将进料流转化为气相部分和液相部分的第一部分和位于第一部分上方的塔中的第二部分，以将烯化氧与乙醛，水和其它杂质分离，从第一部分输入第二部分。

29. 发明申请

US20120302776A1 ALKYLENE OXIDE PURIFICATION SYSTEMS 有权
标题翻译：亚烷基氧化物净化系统
公开(公告)号：US20120302776A1
公开(公告)日：2012-11-29
申请号：US13567135
申请日：2012-08-06
申请人： John F. Szul , James H. McCain , Floyd L. Pfeffer , Harvey E. Andresen , Phillip R. Fairchild , Kent E. Newman
发明人： John F. Szul , James H. McCain , Floyd L. Pfeffer , Harvey E. Andresen , Phillip R. Fairchild , Kent E. Newman
IPC分类号： C07D301/32 , B01D3/00
CPC分类号： C07D301/32
摘要： Embodiments of the present disclosure provide processes, columns, and systems for removing acetaldehyde from alkylene oxide in a feed stream and for providing an alkylene oxide-water stream that can be directly transferred to a glycol reaction process. The alkylene oxide purification column includes a first section to convert a feed stream into a gas phase portion and a liquid phase portion and a second section located in the column above the first section to separate alkylene oxide from the acetaldehyde, water, and other impurities that enter the second section from the first section.
摘要翻译：本公开的实施方案提供了用于从进料流中的环氧烷除去乙醛并提供可直接转移到二醇反应过程的环氧烷 - 水流的方法，塔和系统。环氧烷纯化塔包括将进料流转化为气相部分和液相部分的第一部分和位于第一部分上方的塔中的第二部分，以将烯化氧与乙醛，水和其它杂质分离，从第一部分输入第二部分。

30. 发明授权

US08183400B2 Alkylene oxide recovery systems 有权
标题翻译：环氧树脂回收系统
公开(公告)号：US08183400B2
公开(公告)日：2012-05-22
申请号：US12460755
申请日：2009-07-24
申请人： John F. Szul , James H. Mccain , Floyd L. Pfeffer , Harvey E. Andresen , Phillip R. Fairchild , Kent E. Newman
发明人： John F. Szul , James H. Mccain , Floyd L. Pfeffer , Harvey E. Andresen , Phillip R. Fairchild , Kent E. Newman
IPC分类号： C07D301/32 , B01D3/26 , B01D3/38
CPC分类号： C07D301/32
摘要： Embodiments of the present disclosure include processes and systems for recovering alkylene oxide. System embodiments include a stripping section located in an alkylene oxide recovery column to convert a feed stream comprising to a first gas phase portion comprising alkylene oxide, a condensing zone comprising at least a first condenser and a second condenser configured in series, and a reabsorption region located in the alkylene oxide recovery column above the last of the at least two condensers.
摘要翻译：本公开的实施方案包括用于回收烯化氧的方法和系统。系统实施方案包括位于烯化氧回收塔中的汽提段，以将包含至少包含环氧烷的第一气相部分的进料流，包含至少第一冷凝器和串联配置的第二冷凝器的冷凝区域和再吸收区域位于氧化烯回收塔中，位于至少两个冷凝器的最后一个上方。

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