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21. 发明授权

US4814511A Working up cyclohexyl hydroperoxide containing reaction mixtures 失效
标题翻译：加工含环己基氢过氧化物的反应混合物
公开(公告)号：US4814511A
公开(公告)日：1989-03-21
申请号：US111605
申请日：1987-10-23
申请人： Gerald Neubauer , Rolf Schnabel , Juergen Hartig , Josef Ritz
发明人： Gerald Neubauer , Rolf Schnabel , Juergen Hartig , Josef Ritz
IPC分类号： C07C27/00 , B01J21/06 , B01J23/16 , B01J23/44 , C07B61/00 , C07C29/132 , C07C29/88 , C07C35/08 , C07C45/00 , C07C45/33 , C07C45/53 , C07C49/403 , C07C67/00
CPC分类号： C07C45/33 , C07C29/132 , C07C29/88 , C07C45/53 , C07C2101/14
摘要： Cyclohexyl hydroperoxide containing reaction mixtures obtained by oxidation of cyclohexane with molecular oxygen or molecular oxygen containing gases in the liquid phase at from 130.degree. to 200.degree. C. and under from 5 to 125 bar are worked up by reaction with cycloolefins at elevated temperature in the presence of catalysts to react cyclohexyl hydroperoxide with cyclohexene at elevated temperatures in the presence of cyclohexene-soluble compounds of transition metals of groups 4 or 5 or 6 of the periodic table or of one or more cyclohexane-insoluble compounds of a transition metal of group 4 or 5 or 6, or in the presence of selenium, tellurium or a boride, and the resulting cyclohexene oxide at elevated temperatures to cyclohexanol in the presence of hydrogenation catalysts.
摘要翻译：通过在130〜200℃，5〜125巴下的液相中用分子氧或分子氧气体氧化环己烷得到的含环己基氢过氧化物的反应混合物通过与环烯烃在高温下存在催化剂以使环己基氢过氧化物与环己烯在升高的温度下在周期表第4或5或6族的过渡金属的环己烯可溶性化合物的存在下或一种或多种环己烷不溶性的第4族过渡金属的化合物或5或6，或在硒，碲或硼化物的存在下，将得到的环己烯氧化物在升高的温度下在氢化催化剂存在下进行。

22. 发明授权

US5496941A Process for continuous purification of crude caprolactam prepared from 6-aminocapronitrile 失效
标题翻译：从6-氨基己腈制备的己内酰胺的连续纯化方法
公开(公告)号：US5496941A
公开(公告)日：1996-03-05
申请号：US375410
申请日：1995-01-18
申请人： Josef Ritz , Rolf Fischer , Werner Schnurr , Gu/ nther Achhammer , Hermann Luyken , Eberhard Fuchs
发明人： Josef Ritz , Rolf Fischer , Werner Schnurr , Gu/ nther Achhammer , Hermann Luyken , Eberhard Fuchs
IPC分类号： C07D201/08 , C07D201/16
CPC分类号： C07D201/16 , Y02P20/52
摘要： Crude capronitrile is purified by hydrogenation, subsequent treatment in an acidic medium and subsequent distillation in an alkaline medium, by a process in which(a) 6-aminocapronitrile is converted into crude caprolactam by reaction with water,(b) high boilers and low boilers are separated off from the crude caprolactam from step (a),(c) the crude caprolactam from step (b) is treated with hydrogen at from 50.degree. to 150.degree. C. and from 1.5 to 250 bar in the presence of a hydrogenation catalyst and, if desired, of a solvent to give a mixture A,(d1) mixture A in a solvent is passed, at from 30.degree. to 80.degree. C. and from 1 to 5 bar, over an ion exchanger containing terminal acid groups to give a mixture B1, or(d2) mixture A is distilled in the presence of sulfuric acid, any solvent present being removed before the addition of the sulfuric acid, to give a mixture B2, and(e) mixture B1 or mixture B2 is distilled in the presence of a base to give pure caprolactam.
摘要翻译：通过氢化纯化粗碳腈，随后在酸性介质中处理，随后在碱性介质中进行蒸馏，其中（a）通过与水反应将（a）6-氨基己腈转化为粗己内酰胺，（b）高锅炉和低锅炉与步骤（a）中的粗己内酰胺分离，（c）步骤（b）中的粗己内酰胺在氢化催化剂存在下在50-150℃和1.5-250巴下用氢处理并且如果需要，得到溶剂以得到混合物A，（d1）溶剂中的混合物A在30℃至80℃和1至5巴条件下通过含有末端酸基团的离子交换剂得到混合物B1，或（d2）在硫酸存在下蒸馏混合物A，在加入硫酸之前，除去存在的任何溶剂，得到混合物B2，并且（e）蒸馏出混合物B1或混合物B2 在碱的存在下得到纯己内酰胺。

23. 发明授权

US4634584A Stabilized solutions of hydroxylamine or its salts in water or alcohols, and their preparation 失效
标题翻译：羟胺或其盐在水或醇中的稳定溶液及其制备
公开(公告)号：US4634584A
公开(公告)日：1987-01-06
申请号：US682068
申请日：1984-12-17
申请人： Otto-Alfred Grosskinsky , Elmar Frommer , Josef Ritz , Erwin Thomas , Franz-Josef Weiss
发明人： Otto-Alfred Grosskinsky , Elmar Frommer , Josef Ritz , Erwin Thomas , Franz-Josef Weiss
IPC分类号： C07D307/62 , C01B21/14 , C07C53/10 , C07C53/122
CPC分类号： C07C53/10 , C01B21/149 , C07C53/122
摘要： Stabilized solutions of hydroxylamine or its salts in water or alcohols, containing the lactone of the formula ##STR1## and their preparation.
摘要翻译：稳定的羟胺或其盐在水或醇中的溶液，其含有式（I）的内酯及其制备。

24. 发明授权

US4601800A Preparation of aqueous solutions of hydroxylammonium carbonate 失效
标题翻译：羟基碳酸铵水溶液的制备
公开(公告)号：US4601800A
公开(公告)日：1986-07-22
申请号：US685255
申请日：1984-12-24
申请人： Franz-Josef Weiss , Wolfgang Habermann , Peter Hammes , Josef Ritz , Erwin Thomas , Peter Thoma
发明人： Franz-Josef Weiss , Wolfgang Habermann , Peter Hammes , Josef Ritz , Erwin Thomas , Peter Thoma
IPC分类号： C25B1/00 , B01D57/02 , B01D61/44 , B01D61/50 , B01D61/54 , C01B21/14 , C01C1/26 , C25C7/00
CPC分类号： C01B21/1454 , B01D61/44
摘要： Aqueous solutions of hydroxylammonium carbonate are prepared from aqueous hydroxylammonium salt solutions by electrodialysis by a method in which the aqueous hydroxylammonium salt solution is fed into the middle zone of an electrolysis cell, which is divided into a cathode zone, an anode zone and a middle zone by means of semipermeable membranes, and is electrolyzed, and the catholyte used is an aqueous solution of an ammonium carbonate or an alkali metal carbonate or of one of the corresponding bicarbonates.
摘要翻译：羟基碳酸铵水溶液是通过电渗析由羟基铵盐水溶液制备的，其方法是将羟基铵盐水溶液进料到电解池的中间区域，该电解槽分为阴极区域，阳极区域和中间区域通过半透膜进行电解，所使用的阴极电解液是碳酸铵或碱金属碳酸盐或相应的碳酸氢盐之一的水溶液。

25. 发明授权

US4576804A Stabilized solutions of hydroxylamine or its salts 失效
标题翻译：稳定的羟胺或其盐的溶液
公开(公告)号：US4576804A
公开(公告)日：1986-03-18
申请号：US677306
申请日：1984-12-03
申请人： Otto-Alfred Grosskinsky , Elmar Frommer , Josef Ritz , Erwin Thomas , Franz-Josef Weiss
发明人： Otto-Alfred Grosskinsky , Elmar Frommer , Josef Ritz , Erwin Thomas , Franz-Josef Weiss
IPC分类号： C01B21/14 , C07C53/10 , C07C53/122
CPC分类号： C07C53/122 , C01B21/149 , C07C53/10
摘要： Stabilized solutions of hydroxylamine or its salts in water or alcohols, containing hydroxyanthraquinones, and their preparation.
摘要翻译：羟胺或其盐在含有羟基蒽醌的水或醇中的稳定溶液及其制备。

26. 发明授权

US4629613A Stabilized solutions of hydroxylamine or its salts in water or alcohols, and their preparation 失效
标题翻译：羟胺或其盐在水或醇中的稳定溶液及其制备
公开(公告)号：US4629613A
公开(公告)日：1986-12-16
申请号：US682071
申请日：1984-12-17
申请人： Otto-Alfred Grosskinsky , Elmar Frommer , Josef Ritz , Erwin Thomas , Franz-Josef Weiss
发明人： Otto-Alfred Grosskinsky , Elmar Frommer , Josef Ritz , Erwin Thomas , Franz-Josef Weiss
IPC分类号： C07D215/26 , C01B21/14 , C07C53/10 , C07C53/122 , C01B21/20
CPC分类号： C01B21/149 , C07C53/10 , C07C53/122
摘要： Stabilized solutions of hydroxylamine or its salts in water or alcohols, containing 8-hydroxyquinaldines, and their preparation.
摘要翻译：羟胺或其盐在含有8-羟基喹啉的水或醇中的稳定溶液及其制备。

27. 发明授权

US4551318A Stabilized solutions of hydroxylamine or its salts in water or alcohols, and their preparation 失效
标题翻译：羟胺或其盐在水或醇中的稳定溶液及其制备
公开(公告)号：US4551318A
公开(公告)日：1985-11-05
申请号：US685257
申请日：1984-12-24
申请人： Otto-Alfred Grosskinsky , Elmar Frommer , Josef Ritz , Erwin Thomas , Franz-Josef Weiss
发明人： Otto-Alfred Grosskinsky , Elmar Frommer , Josef Ritz , Erwin Thomas , Franz-Josef Weiss
IPC分类号： C07D311/60 , C01B21/14 , C07C53/10 , C07C53/122 , C01B21/20
CPC分类号： C01B21/149 , C07C53/10 , C07C53/122
摘要： Stabilized solutions of hydroxylamine or its salts, containing anthocyans of the formula ##STR1## where R.sup.1, R.sup.2, R.sup.3 and R.sup.4 are each hydrogen, hydroxyl or C.sub.1 -C.sub.4 -alkoxy and X is an anion of a strong mineral acid, and their preparation.
摘要翻译：羟胺或其盐的稳定化溶液，其含有式“IMAGE”的花青素，其中R1，R2，R3和R4各自为氢，羟基或C1-C4-烷氧基，X为强无机酸的阴离子及其制备。

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