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21. 发明授权

US4319025A Anthraquinone-azomethine compounds, processes for their preparation and processes for dyeing synthetic fibre materials and for pigmenting organic macromolecular substances 失效
标题翻译：蒽醌 - 偶氮甲碱化合物，其制备方法和合成纤维材料染色工艺和有机高分子物质着色
公开(公告)号：US4319025A
公开(公告)日：1982-03-09
申请号：US170449
申请日：1980-07-21
申请人： Rutger Neeff , Meinhard Rolf , Walter Muller
发明人： Rutger Neeff , Meinhard Rolf , Walter Muller
IPC分类号： C09B56/00 , C09B1/20 , C09B55/00 , C07D213/68
CPC分类号： C09B1/205 , C09B55/00 , Y10S8/922 , Y10S8/924 , Y10S8/927
摘要： Anthraquinone-azomethine compounds of the formula ##STR1## or of the tautomeric formula ##STR2## or of the tautomeric formula ##STR3## in which A denotes an anthraquinone radical which is free from sulphonic acid groups and optionally further substituted and which preferably consists of at most 5 fused rings,R.sub.1 denotes hydrogen, C.sub.1 -C.sub.4 -alkyl, hydroxy-C.sub.1 -C.sub.4 -alkyl, optionally substituted phenyl, carboxyl, carboxylic acid, C.sub.1 -C.sub.4 -alkyl ester or hydroxyl,R.sub.2 denotes hydrogen, halogen, nitro, cyano, optionally substituted carbamoyl or optionally substituted sulphamoyl, sulphonic acid C.sub.1 -C.sub.4 -alkyl ester, sulphonic acid aryl ester, C.sub.1 -C.sub.4 - alkylcarbonyl, C.sub.1 -C.sub.4 -alkoxycarbonyl, optionally substituted benzoyl, alkyl or optionally substituted phenyl sulphone, or a hetero-aromatic radical, for example a radical of the formula ##STR4## or of the formula ##STR5## or of the formula ##STR6## R.sub.3 denotes optionally substituted aryl or hetero-aryl, cycloalkyl or C.sub.1 -C.sub.12 -alkyl, it being possible for the alkyl chain to be interrupted by oxygen or sulphur and /or substituted by hydroxyl, N(R.sub.5).sub.2 -- or --N(R.sub.5).sub.3.sup..sym. X.sup..crclbar. groups,R.sub.4 denotes a substituent,R.sub.5 denotes hydrogen, C.sub.1 -C.sub.4 -alkyl, cycloalkyl or optionally substituted aryl,X denotes an anion,m denotes 1, 2, 3 or 4 andn denotes 0, 1, 2, 3 or 4,processes for their preparation and processes for dyeing synthetic fibre materials and for pigmenting organic macromolecular substances using the new anthraquinone-azomethine compounds.
摘要翻译：式（I）的蒽醌 - 偶氮甲碱化合物或互变异构体式（Ia）或互变异构式（IMA）（Ib）的蒽醌 - 偶氮甲碱化合物，其中A表示不含磺酸基团的蒽醌基团，任选进一步取代并且优选由至多5个稠环组成，R 1表示氢，C 1 -C 4 - 烷基，羟基-C 1 -C 4 - 烷基，任选取代的苯基，羧基，羧酸，C 1 -C 4 - 烷基酯或羟基， R 2表示氢，卤素，硝基，氰基，任选取代的氨基甲酰基或任选取代的氨磺酰基，磺酸C 1 -C 4 - 烷基酯，磺酸芳基酯，C 1 -C 4烷基羰基，C 1 -C 4烷氧基羰基，任选取代的苯甲酰基，烷基或任选取代的苯基砜或杂芳族基团，例如式（II）或式（IMAGE）（III）或式（IV）的基团R 3表示任选取代的芳基或杂芳基，环烷基或C 1 -C 12 - 烷基可能的烷基链被氧或硫中断，和/或由羟基，N（R 5）2或-N（R 5）3（+）X（ - ）基团取代，R 4表示取代基，R 5表示氢，C 1 -C 4 - 烷基，环烷基或任选取代的芳基，X表示阴离子，m表示1,2,3或4，n表示0,1,2,3或4，其制备方法和合成纤维染色方法材料和使用新的蒽醌 - 偶氮甲碱化合物着色有机高分子物质。

22. 发明授权

US4260540A Azo dye pigments containing 4-quinazolinone moieties 失效
标题翻译：含有4-喹唑啉酮部分的偶氮染料颜料
公开(公告)号：US4260540A
公开(公告)日：1981-04-07
申请号：US022295
申请日：1979-03-20
申请人： Meinhard Rolf , Rutger Neeff , Walter Muller
发明人： Meinhard Rolf , Rutger Neeff , Walter Muller
IPC分类号： C07D239/88 , C07D487/14 , C09B29/01 , C09B29/32 , C09B31/10 , C09B35/035 , C09K17/00 , C09B29/22 , C09B29/36 , C09B62/08
CPC分类号： C09B35/035 , C07D239/88 , C09B29/0022 , C09B29/32 , C09B31/10
摘要： Heterocyclic compounds of the formula ##STR1## wherein R.sub.1 denotes hydrogen or C.sub.1 -C.sub.4 -alkyl or the two R.sub.1 s together denote CO,R.sub.2 denotes a substituent andn denotes 0, 1, 2, 3 or 4,processes for their preparation, azo pigments prepared therefrom by a coupling reaction with a diazo component of an aromatic or hetero-aromatic amine free from sulphonic acid groups, and the use of these azo pigments for pigmenting organic macromolecular materials and especially in the spin dyeing of polyacrylonitrile.
摘要翻译：式IMA的杂环化合物，其中R 1表示氢或C 1 -C 4烷基或两个R 1一起表示CO，R 2表示取代基，n表示0,1,2,3或4，其制备方法，偶氮颜料通过与不含磺酸基团的芳族或杂芳族胺的重氮组分的偶联反应制备，以及这些偶氮颜料用于着色有机高分子材料，特别是在聚丙烯腈的纺丝染色中的用途。

23. 发明授权

US4246401A Axomethine pigments 失效
标题翻译：阿魏酸颜料
公开(公告)号：US4246401A
公开(公告)日：1981-01-20
申请号：US21676
申请日：1979-03-19
申请人： Rutger Neeff , Meinhard Rolf , Walter Muller
发明人： Rutger Neeff , Meinhard Rolf , Walter Muller
IPC分类号： C09B55/00 , C09B23/16 , C07D403/02
CPC分类号： C09B23/164
摘要： Azomethine pigments of the formula ##STR1## or of the tautomeric formula ##STR2## in which D denotes the radical of an aromatic or heteroaromatic amine which is free from sulphonic acid groups,R.sub.1 denotes hydrogen or C.sub.1 -C.sub.4 -alkyl, in particular methyl, or both the R.sub.1, at the same time, denote CO,R.sub.2 denotes a substituent,m denotes an integer, preferably 1 or 2, andn denotes 0, 1, 2, 3 or 4,a processes for their preparation.
摘要翻译：其中D表示不含磺酸基团的芳族或杂芳族胺基团，R1表示氢或C1-C4-烷基，特别是甲基，环烷基，或两者同时表示CO，R 2表示取代基，m表示整数，优选1或2，n表示0,1,2,3或4表示其制备方法。

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