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21. 发明申请

US20100113706A1 Ethylene Polymers, Their Production And Use 有权
标题翻译：乙烯聚合物，其生产和使用
公开(公告)号：US20100113706A1
公开(公告)日：2010-05-06
申请号：US12266360
申请日：2008-11-06
申请人： Donna J. Crowther , Kuangyao Brian Peng
发明人： Donna J. Crowther , Kuangyao Brian Peng
IPC分类号： C08F4/16 , C08F110/02 , C08F4/44 , C08L23/06
CPC分类号： C08F210/16 , C08F2/00 , C08F210/14 , C08F2500/03 , C08F2500/17 , C08F2500/12 , C08F2500/18 , C08F2500/26
摘要： This invention relates to an ethylene polymer comprising ethylene and up to 5 mole % of at least one comonomer, wherein the ethylene polymer has an Mw, of 10,000 to 50,000, an Mw/Mn of between 1.5 to 4.5, a density of at least 0.925 g/cc, an unsaturation level of less than 1 per 1000 carbons, a melting point of at least 120° C., a Tc of greater than Z, where Z=0.501×(density in kg/m3)−367, and a Brookfield viscosity o at 140° C. of 100,000 mPas or more.
摘要翻译：本发明涉及包含乙烯和至多5摩尔％的至少一种共聚单体的乙烯聚合物，其中乙烯聚合物具有10,000至50,000的Mw，1.5至4.5的Mw / Mn，至少0.925的密度 g / cc，不小于1/1000个碳的不饱和度，熔点至少为120℃，Tc大于Z，其中Z = 0.501×（密度（kg / m3）-367），和布鲁克菲尔德粘度在140°C时为100,000 mPas以上。

22. 发明授权

US07541413B2 Olefin polymerization catalysts, their synthesis and use 有权
标题翻译：烯烃聚合催化剂，其合成和用途
公开(公告)号：US07541413B2
公开(公告)日：2009-06-02
申请号：US11866113
申请日：2007-10-02
申请人： Donna J. Crowther , Celestino M. Perez
发明人： Donna J. Crowther , Celestino M. Perez
IPC分类号： C08F4/02 , C08F4/80
CPC分类号： B01J31/1815 , B01J2231/12 , B01J2531/0238 , B01J2531/842 , C08F10/00 , C08F110/02 , C08F4/7042 , C08F2500/04
摘要： A catalyst system for the polymerization or copolymerization of α-olefins comprises a bis(imino)pyridyl complex of a transition metal on a support having an aluminum halide and/or an alkylaluminum halide chemically or physically bonded thereto.
摘要翻译：用于α-烯烃的聚合或共聚的催化剂体系包括在具有卤化铝和/或与其化学或物理结合的烷基铝卤化物的载体上的过渡金属的双（亚氨基）吡啶基复合物。

23. 发明授权

US06486278B1 Ethylene copolymerization process 失效
标题翻译：乙烯共聚方法
公开(公告)号：US06486278B1
公开(公告)日：2002-11-26
申请号：US09251819
申请日：1999-02-17
申请人： Rinaldo S. Schiffino , Donna J. Crowther
发明人： Rinaldo S. Schiffino , Donna J. Crowther
IPC分类号： C08F442
CPC分类号： C08F210/18 , C08F4/65908 , C08F4/65912 , Y10S526/943 , C08F2/06 , C08F4/65927 , C08F210/06 , C08F236/20 , C08F2500/25 , C08F2500/08 , C08F2500/04 , C08F2500/03
摘要： This invention is a solution process for the preparation of ethylene-&agr;-olefin-diolefin copolymers comprising contacting ethylene, one or more &agr;-olefin monomer, and one or more cyclic diene monomer, with a catalyst composition comprising a bridged, bis(cyclopentadienyl) zirconium compound having an unsubstituted cyclopentadienyl ligand, a multiply substituted cyclopentadienyl ligand, said ligands bridged by a covalent bridging group containing one or more Group 14 element, and two uninegative, activation reactive ligands and a catalyst activator compound. The invention process exhibits high catalyst activity, high comonomer incorporation and high diene monomer conversion rates and is particularly suitable for the preparation of elastomeric ethylene-propylene or ethylene-propylene-diene monomer elastomers.
摘要翻译：本发明是用于制备乙烯-α-烯烃 - 二烯烃共聚物的溶液方法，包括使乙烯，一种或多种α-烯烃单体和一种或多种环状二烯单体与催化剂组合物接触，所述催化剂组合物包含桥连的双（环戊二烯基）具有未取代的环戊二烯基配体的锆化合物，多取代的环戊二烯基配体，所述配体由含有一个或多个第14族元素的共价桥连基团桥连，以及两个非负号活化反应性配体和催化剂活化剂化合物。本发明方法表现出高催化剂活性，高共聚单体掺入和高二烯单体转化率，特别适用于制备弹性体乙烯 - 丙烯或乙烯 - 丙烯 - 二烯单体弹性体。

24. 发明授权

US06300433B1 Olefin copolymerization process with bridged hafnocenes 有权
标题翻译：烯烃共聚方法与桥连氢键
公开(公告)号：US06300433B1
公开(公告)日：2001-10-09
申请号：US09422533
申请日：1999-10-21
申请人： George Rodriguez , Donna J. Crowther
发明人： George Rodriguez , Donna J. Crowther
IPC分类号： C08F452
CPC分类号： C08F10/00 , C07F17/00 , C08F4/65908 , C08F10/02 , C08F110/02 , C08F210/16 , C08F4/65927 , C08F210/14 , C08F2/06 , C08F2500/03 , C08F2500/04 , C08F2500/12 , C08F2500/08
摘要： The invention is directed to olefin polymerization processes using bridged hafnocene catalyst complexes that are surprisingly stable under high temperature olefin polymerization processes such that olefin copolymers can be prepared with high molecular weights and catalyst activities. More specifically, the invention is a polymerization process for ethylene copolymers having a melt index of about 0.850 to about 0.930 comprising contacting, under homogeneous polymerization conditions at a reaction temperature at or above 60° C. to 250° C., ethylene and one or more comonomers capable of insertion polymerization with a bridged hafnocene catalyst complex derived from A) a biscyclopentadienyl hafnium organometallic compound having i) at least one unsubstituted cyclopentadienyl ligand or aromatic fused-ring substituted cyclopentadienyl ligand, ii) one aromatic fused-ring substituted cyclopentadienyl ligand, iii) and a covalent bridge connecting the two cyclopentadienyl ligands, said bridge comprising a single carbon or silicon atom with two aryl groups, each substituted with a C1-C20 hydrocarbyl or hydrocarbylsilyl group at least one of which is a linear C3 or greater substitutent; and B) an activating cocatalyst.
摘要翻译：本发明涉及使用在高温烯烃聚合方法中出人意料地稳定的桥联茂茂催化剂络合物的烯烃聚合方法，使得可以以高分子量和催化剂活性制备烯烃共聚物。更具体地，本发明是一种熔体指数为约0.850至约0.930的乙烯共聚物的聚合方法，其包括在均相聚合条件下在等于或高于60℃至250℃的反应温度下接触乙烯和一种或能够与来自A）双环戊二烯基铪有机金属化合物的桥连的茂金属催化剂络合物进行插入聚合的更多共聚单体，其具有i）至少一个未取代的环戊二烯基配体或芳族稠环取代的环戊二烯基配体，ii）一个芳族稠环取代的环戊二烯基配体， iii）和连接两个环戊二烯基配体的共价桥，所述桥包含单个碳或硅原子与两个芳基，每个被C1-C20烃基或烃基甲硅烷基取代，其中至少一个是直链C3或更大的取代基; 和B）活化助催化剂。

25. 发明授权

US06291609B1 High temperature olefin polymerization process 有权
标题翻译：高温烯烃聚合工艺
公开(公告)号：US06291609B1
公开(公告)日：2001-09-18
申请号：US09261637
申请日：1999-03-03
申请人： Donna J. Crowther , Bernard J. Folie , John F. Walzer, Jr. , Rinaldo S. Schiffino
发明人： Donna J. Crowther , Bernard J. Folie , John F. Walzer, Jr. , Rinaldo S. Schiffino
IPC分类号： C08F442
CPC分类号： C08F10/00 , C08F4/65908 , C08F4/65912 , C08F4/65927 , C08F210/06 , C08F210/16 , C08F210/18 , C08L23/142 , C08L23/16 , C08L2205/025 , C08L2308/00 , C08L2312/00 , C08L2314/06 , Y10S526/916 , Y10S526/943 , C08F2/06 , C08F4/6592 , C08F2/001 , C08L2666/04 , C08F2500/17 , C08F2500/03 , C08F2500/08 , C08F2500/15 , C08F2500/21 , C08F2500/04 , C08F2500/20 , C08F210/14 , C08F2500/12 , C08F2500/25 , C08F236/20
摘要： The invention is directed to olefin polymerization processes using bridged hafnocene catalyst complexes comprising highly substituted noncoordinating anions that are surprisingly stable under high temperature olefin polymerization processes such that olefin copolymers having significant amount of incorporated comonomer can be prepared with high molecular weights. More specifically, the invention is a polymerization process for ethylene copolymers having a melt index of about 0.87 to about 0.930 comprising contacting, under homogeneous polymerization conditions at a reaction temperature at or above 140° C. to 225° C., ethylene and one or more comonomers capable of insertion polymerization with a bridged hafnocene catalyst complex derived from A) a biscyclopentadienyl hafnium organometallic compound having i) at least one unsubstituted cyclopentadienyl ligand or aromatic fused-ring substituted cyclopentadienyl ligand, ii) one aromatic fused-ring substituted cyclopentadienyl ligand, iii) and a covalent bridge connecting the two cyclopentadienyl ligands, said bridge comprising a single carbon or silicon atom; and B) an activating cocatalyst, precursor ionic compound comprising a halogenated tetraaryl-substituted Group 13 anion wherein each aryl substituent contains at least two cyclic aromatic rings.
摘要翻译：本发明涉及使用包含高度取代的非配位阴离子的桥联茂金属催化剂络合物的烯烃聚合方法，其在高温烯烃聚合方法中令人惊奇地稳定，使得可以以高分子量制备具有显着量的掺入共聚单体的烯烃共聚物。更具体地，本发明是一种熔体指数为约0.87至约0.930的乙烯共聚物的聚合方法，其包括在均相聚合条件下在140℃至225℃或更高的温度下接触乙烯和一种或能够与来自A）双环戊二烯基铪有机金属化合物的桥连的茂金属催化剂络合物进行插入聚合的更多共聚单体，其具有i）至少一个未取代的环戊二烯基配体或芳族稠环取代的环戊二烯基配体，ii）一个芳族稠环取代的环戊二烯基配体， iii）和连接两个环戊二烯基配体的共价桥，所述桥包含单个碳或硅原子; 和B）活化助催化剂，包含卤化四芳基取代的第13族阴离子的前体离子化合物，其中每个芳基取代基含有至少两个环状芳环。

26. 发明授权

US09663727B2 Functionalized polymers containing polyamine succinimide for antifouling in hydrocarbon refining processes 有权
公开(公告)号：US09663727B2
公开(公告)日：2017-05-30
申请号：US14870839
申请日：2015-09-30
申请人： Man Kit Ng , Mohsen S Yeganeh , Timothy Andrew Barckholtz , Glen Barry Brons , Hong Cheng , Geoffrey Marshall Keiser , Donna J. Crowther , Patrick Brant , David T. Ferrughelli , Clarence Chase , Emmanuel Ulysse , Edward Andrew Lemon
发明人： Man Kit Ng , Mohsen S Yeganeh , Timothy Andrew Barckholtz , Glen Barry Brons , Hong Cheng , Geoffrey Marshall Keiser , Donna J. Crowther , Patrick Brant , David T. Ferrughelli , Clarence Chase , Emmanuel Ulysse , Edward Andrew Lemon
IPC分类号： C08F8/32 , C10G33/04 , C10G75/04 , C10L1/236 , C10L1/2383 , C10L10/04 , C07D207/408 , C08F8/46 , C08F10/00 , C08F290/04
CPC分类号： C10G33/04 , C07D207/408 , C08F8/32 , C10G75/04 , C10L1/2364 , C10L1/2383 , C10L10/04
摘要： A multipurpose chemical additives (MPC) is disclosed to mitigate fouling in hydrocarbon refinery processes, such as in a heat exchanger. A method for reducing fouling of a hydrocarbon is also disclosed that includes (i) providing a crude hydrocarbon for a refining process; and (ii) adding an additive to the crude hydrocarbon.

27. 发明授权

US09502705B2 Microporous film, methods for making such film, and use for such film as battery separator film 有权
标题翻译：微孔膜，制造这种膜的方法，以及用于这种膜的电池隔膜
公开(公告)号：US09502705B2
公开(公告)日：2016-11-22
申请号：US13996028
申请日：2011-12-20
申请人： Patrick Brant , Takeshi Ishihara , Satoshi Miyaoka , Donna J. Crowther , Koichi Kono
发明人： Patrick Brant , Takeshi Ishihara , Satoshi Miyaoka , Donna J. Crowther , Koichi Kono
IPC分类号： H01M2/16 , C08J5/18 , B29C55/00 , B32B27/06 , B32B27/32 , B29K23/00 , B29K105/04
CPC分类号： H01M2/16 , B29C55/005 , B29K2023/10 , B29K2105/041 , B32B27/06 , B32B27/32 , B32B2307/5825 , B32B2307/724 , B32B2457/10 , C08J5/18 , C08J2323/10 , H01M2/1653
摘要： A microporous membrane includes a low melting polypropylene, the low melting polypropylene being a polypropylene homopolymer or copolymer having an MFR≧2.0×102, a Tm of 85.0° C. to 130.0° C., and a Te-Tm≦10° C.
摘要翻译：微孔膜包括低熔点聚丙烯，低熔点聚丙烯是MFR≥2.0×102，Tm为85.0℃〜130.0℃，Te-Tm≤10℃的聚丙烯均聚物或共聚物。

28. 发明授权

US09289728B2 Microporous membranes, methods for making such membranes, and the use of such membranes as battery separator film 有权
标题翻译：微孔膜，制造这种膜的方法以及使用这种膜作为电池隔膜
公开(公告)号：US09289728B2
公开(公告)日：2016-03-22
申请号：US13260643
申请日：2010-03-05
申请人： Takeshi Ishihara , Satoshi Miyaoka , Koichi Kono , Donna J. Crowther , Patrick Brant
发明人： Takeshi Ishihara , Satoshi Miyaoka , Koichi Kono , Donna J. Crowther , Patrick Brant
IPC分类号： H01M2/16 , B29C47/00 , H01M10/02 , H01M10/26 , H01M4/64 , B01D71/26 , B01D71/76 , B32B27/32 , H01M2/14
CPC分类号： B01D71/26 , B01D71/76 , B29C47/00 , B32B27/32 , H01M2/14 , H01M2/16 , H01M2/164 , H01M2/1653
摘要： The invention relates to microporous membranes comprising polymer and having well-balanced permeability, shutdown temperature, and pin puncture strength. The invention also relates to methods for making such membranes, and the use of such membranes as battery separator film in, e.g., lithium ion secondary batteries. The membrane has a shutdown temperature
摘要翻译：本发明涉及包含聚合物并具有良好平衡渗透性，关闭温度和针穿刺强度的微孔膜。本发明还涉及制造这种膜的方法，以及在例如锂离子二次电池中使用这种膜作为电池隔膜。膜的关闭温度<130.5°C

29. 发明授权

US08951409B2 Polyalkylene epoxy polyamine additives for fouling mitigation in hydrocarbon refining processes 有权
标题翻译：聚烯烃环氧多胺添加剂，用于在碳氢化合物精炼过程中减轻污染
公开(公告)号：US08951409B2
公开(公告)日：2015-02-10
申请号：US12642606
申请日：2009-12-18
申请人： Man Kit Ng , Glen B. Brons , Steven W. Levine , Kevin Mallory , Hong Cheng , Patrick Brant , Donna J. Crowther
发明人： Man Kit Ng , Glen B. Brons , Steven W. Levine , Kevin Mallory , Hong Cheng , Patrick Brant , Donna J. Crowther
IPC分类号： C10G9/16 , C10G75/04 , C10G7/10 , C10G29/20 , C10G21/20
CPC分类号： C10G75/04 , C10G2300/4075 , C10G2300/80
摘要： The present invention provides a method for reducing fouling, including particulate-induced fouling, in a hydrocarbon refining process including the steps of providing a crude hydrocarbon for a refining process and adding an antifouling agent containing a polymer base unit and a polyamine group to the crude hydrocarbon. The antifouling agent can be obtained by reacting an epoxidation reagent with a vinyl-terminated polymer, such as polypropylene or poly(ethylene-co-propylene), to form a terminal epoxy group, followed by reacting a polyamine with the epoxy group.
摘要翻译：本发明提供了一种在烃精炼方法中减少包括颗粒引起的结垢的污垢的方法，包括以下步骤：提供用于精制方法的粗烃，并将含有聚合物基单元和多胺基团的防污剂加入到粗品烃。防污剂可以通过使环氧化试剂与聚乙烯基封端的聚合物如聚（乙烯 - 共 - 丙烯）反应形成末端环氧基，然后使多胺与环氧基反应而获得。

30. 发明授权

US08372930B2 High vinyl terminated propylene based oligomers 有权
标题翻译：高乙烯基封端的丙烯基低聚物
公开(公告)号：US08372930B2
公开(公告)日：2013-02-12
申请号：US12143663
申请日：2008-06-20
申请人： Patrick Brant , Donna J. Crowther , Andrew G. Narvaez, Jr.
发明人： Patrick Brant , Donna J. Crowther , Andrew G. Narvaez, Jr.
IPC分类号： C08F110/06 , C08F210/06 , C08F210/16 , C08F210/18
CPC分类号： C08F210/06 , C08F210/16 , C08F2500/20 , C08F2500/02
摘要： This invention relates to a co-oligomer having an Mn of 300 to 30,000 g/mol comprising 10 to 90 mol % propylene and 10 to 90 mol % of ethylene, wherein the oligomer has at least X % allyl chain ends, where: 1) X=(−0.94 (mole % ethylene incorporated)+100), when 10 to 60 mole % ethylene is present in the co-oligomer, and 2) X=45, when greater than 60 and less than 70 mole % ethylene is present in the co-oligomer, and 3) X=(1.83*(mole % ethylene incorporated)−83), when 70 to 90 mole % ethylene is present in the co-oligomer. This invention also relates to a homo-oligomer, comprising propylene, wherein the oligomer has: at least 93% allyl chain ends, an Mn of about 500 to about 20,000 g/mol, an isobutyl chain end to allylic vinyl group ratio of 0.8:1 to 1.2:1.0, and less than 100 ppm aluminum. This invention also relates to a process of making homo-oligomer, comprising propylene, wherein the productivity is greater than 4500 g/mmol Hf (or Zr)/hour.
摘要翻译：本发明涉及Mn为300〜30,000g / mol，包含10-90mol％丙烯和10-90mol％乙烯的共低聚物，其中低聚物具有至少X％的烯丙基链末端，其中：1）当共聚低聚物中存在10至60摩尔％的乙烯时，X =（ - 0.94（摩尔％乙烯掺入）+100），和2）X = 45，当大于60且小于70摩尔％时存在乙烯在共低聚物中，3）X =（1.83 *（摩尔％乙烯掺入）-83），当共聚低聚物中存在70至90摩尔％的乙烯时。本发明还涉及包含丙烯的均聚物，其中低聚物具有：至少93％的烯丙基链端，约500至约20,000g / mol的Mn，异丁基链端至烯丙基乙烯基的比例为0.8： 1至1.2：1.0和小于100ppm的铝。本发明还涉及制备包含丙烯的均聚物的方法，其中生产率大于4500g / mmol Hf（或Zr）/小时。

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