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21. 发明授权

US5880070A Cross-linked succinimides from an acid derivative, a polyamine, and a polycarboxylic acid derivative 失效
标题翻译：来自酸衍生物，多胺和多元羧酸衍生物的交联琥珀酰亚胺
公开(公告)号：US5880070A
公开(公告)日：1999-03-09
申请号：US699745
申请日：1996-08-20
申请人： James J. Harrison , William R. Ruhe, Jr.
发明人： James J. Harrison , William R. Ruhe, Jr.
IPC分类号： C10L1/234 , C08F8/32 , C08F222/04 , C10L1/236 , C10L1/238 , C10L1/2383 , C10L1/30 , C10L10/00 , C10L10/08 , C10L10/18 , C10M133/56 , C10M149/06 , C10M159/12 , C10M161/00 , C10N30/04 , C10N40/25 , C10N70/00 , C10M145/00 , C10M149/00
CPC分类号： C10M161/00 , C08F8/32 , C10L1/2364 , C10L1/2366 , C10L1/238 , C10L1/2383 , C10L1/303 , C10L10/04 , C10L10/06 , C10M149/06 , C10M2205/00 , C10M2205/02 , C10M2207/123 , C10M2207/129 , C10M2207/22 , C10M2209/086 , C10M2215/04 , C10M2215/26 , C10M2215/28 , C10M2217/024 , C10M2217/046 , C10M2217/06 , C10N2240/10 , C10N2240/101 , C10N2240/104 , C10N2240/106
摘要： A polyalkylene succinimide composition prepared by reacting a mixture of an acid derivative, a polycarboxylic acid derivative; and a polyamine under reactive conditions. The acid derivative can be an alkenyl or alkylsuccinic acid derivative, a copolymer of a first unsaturated acidic reagent and a 1,1-disubstituted olefin, or mixtures of the alkenyl or alkylsuccinic acid derivative and the copolymer. The total reaction mixture contains from 4 to 40 wt. % of the polycarboxylic acid derivative, and contains from 0.1 to 1.5 equivalents of polyamine per equivalent of acidic groups of the acid derivative plus the acidic groups of the polycarboxylic acid derivative.
摘要翻译：一种聚亚烷基琥珀酰亚胺组合物，其通过酸衍生物，多元羧酸衍生物的混合物，和多胺在反应条件下。酸衍生物可以是烯基或烷基琥珀酸衍生物，第一不饱和酸性试剂和1,1-二取代烯烃的共聚物，或链烯基或烷基琥珀酸衍生物和共聚物的混合物。总反应混合物含有4-40wt。％的多元羧酸衍生物，并且每当量的酸衍生物的酸性基团与多元羧酸衍生物的酸性基团含有0.1至1.5当量的多胺。

22. 发明授权

US5792729A Dispersant terpolymers 失效
标题翻译：分散三元共聚物
公开(公告)号：US5792729A
公开(公告)日：1998-08-11
申请号：US699752
申请日：1996-08-20
申请人： James J. Harrison , William R. Ruhe, Jr.
发明人： James J. Harrison , William R. Ruhe, Jr.
IPC分类号： B01F17/52 , C08F8/32 , C08F8/42 , C08F8/46 , C08F210/10 , C08F210/14 , C08F222/06 , C08F255/00 , C08F255/08 , C08G73/10 , C10L1/14 , C10L1/22 , C10L10/08 , C10L10/18 , C10M149/10 , C10M149/12 , C10M149/14 , C08F267/04 , C10M155/04
CPC分类号： C08F210/14
摘要： A terpolymer having an average M.sub.n of from 600 to 100,000 is obtained by the terpolymerization of a 1-olefin having from 10 to 30 carbon atoms, maleic anhydride, and a 1,1 -disubstituted polyisobutylene having an average M.sub.n of from 500 to 5,000.
摘要翻译：平均Mn为600〜100,000的三元共聚物是通过具有10-30个碳原子的1-烯烃，马来酸酐和平均Mn为500-5,000的1,1-取代的聚异丁烯进行三聚反应得到的。

23. 发明授权

US5753597A Polymeric dispersants 失效
标题翻译：聚合分散剂
公开(公告)号：US5753597A
公开(公告)日：1998-05-19
申请号：US699749
申请日：1996-08-20
申请人： James J. Harrison , William R. Ruhe, Jr.
发明人： James J. Harrison , William R. Ruhe, Jr.
IPC分类号： C08L23/00 , C08F8/32 , C08L35/00 , C08L79/02 , C10L1/22 , C10L1/236 , C10L1/238 , C10L1/2383 , C10L1/30 , C10L10/00 , C10M149/06 , C10M161/00 , C10M149/12 , C10M149/14 , C10M159/12 , C08J3/24
CPC分类号： C10L1/2364 , C08F8/32 , C10L1/221 , C10L1/2366 , C10L1/2368 , C10L1/238 , C10L1/2383 , C10L1/303 , C10L10/04 , C10M149/06 , C10M161/00 , C10M2215/04 , C10M2215/26 , C10M2215/28 , C10M2217/024 , C10M2217/028 , C10M2217/046 , C10M2217/06 , C10M2227/061 , C10N2240/08 , C10N2240/10 , C10N2240/101 , C10N2240/102 , C10N2240/103 , C10N2240/104 , C10N2240/106 , C10N2270/02
摘要： A polysuccinimide composition is prepared by reacting a mixture of a copolymer of a first unsaturated acidic reagent and a 1,1-disubstituted olefin; a copolymer of a second unsaturated acidic reagent and a 1-olefin, and a polyamine under reactive conditions; then treating the reaction product with either a cyclic carbonate or a linear mono- or polycarbonate or boron compound under reactive conditions. The two unsaturated acidic reagents can be the same or different. The mixture contains from 0.1 to 1.5 equivalents of polyamine per equivalent of acidic groups of the first and second copolymers.
摘要翻译：通过使第一不饱和酸性试剂和1,1-二取代烯烃的共聚物的混合物反应制备聚琥珀酰亚胺组合物; 第二不饱和酸性试剂和1-烯烃的共聚物和多胺在反应条件下; 然后在反应条件下用环状碳酸酯或直链单 - 或聚碳酸酯或硼化合物处理反应产物。两种不饱和酸性试剂可以相同或不同。该混合物每当量的第一和第二共聚物的酸性基团含有0.1至1.5当量的多胺。

24. 发明授权

US5716912A Polyalkylene succinimides and post-treated derivatives thereof 失效
公开(公告)号：US5716912A
公开(公告)日：1998-02-10
申请号：US631648
申请日：1996-04-09
申请人： James J. Harrison , William R. Ruhe, Jr.
发明人： James J. Harrison , William R. Ruhe, Jr.
IPC分类号： C08F8/00 , C08F8/32 , C10L1/14 , C10L1/16 , C10L1/18 , C10L1/22 , C10L1/234 , C10L1/236 , C10L1/238 , C10L1/24 , C10L1/26 , C10L1/30 , C10L10/00 , C10M133/56 , C10M149/06 , C10M159/12 , C10M161/00 , C10M149/10
CPC分类号： C10M159/12 , C08F8/00 , C08F8/14 , C08F8/32 , C08F8/48 , C10L1/143 , C10L1/221 , C10L1/234 , C10L1/236 , C10L1/2364 , C10L1/2366 , C10L1/2368 , C10L1/238 , C10L1/303 , C10L10/04 , C10L10/08 , C10M133/56 , C10M149/06 , C10M161/00 , C08F2800/20 , C08F2810/50 , C10L1/1608 , C10L1/1616 , C10L1/1824 , C10L1/2383 , C10L1/2493 , C10L1/2691 , C10M2207/142 , C10M2207/32 , C10M2215/04 , C10M2215/26 , C10M2215/28 , C10M2217/024 , C10M2217/046 , C10M2217/06 , C10M2227/00 , C10M2227/06 , C10M2227/061 , C10M2227/062 , C10M2227/063 , C10M2227/065 , C10M2227/066 , C10N2240/10 , C10N2240/101 , C10N2240/104 , C10N2240/106 , C10N2270/02
摘要： A succinimide composition is prepared by reacting a mixture of an alkenyl or alkylsuccinic acid derivative, an unsaturated acidic reagent copolymer, and a polyamine under reactive conditions; then treating the reaction product with either a cyclic carbonate or a linear mono- or polycarbonate or boron compound under reactive conditions. The alkenyl or alkyl substituent of the alkenyl or alkylsuccinic acid derivative has a Mn of from 1800 to 3000. The unsaturated acidic reagent copolymer has a Mn of from 2000 to 4800, and is a copolymer of an unsaturated acidic reagent and an olefin having an average of from 14 to 30 carbon atoms. The polyamine has at least three nitrogen atoms and 4 to 20 carbon atoms. The mixture contains from 1.5 to 10 equivalents of the alkenyl or alkylsuccinic acid derivative per equivalent of unsaturated acidic reagent copolymer and from 0.4 to 1.0 moles of polyamine per equivalent of alkenyl or alkylsuccinic acid derivative plus unsaturated acidic reagent copolymer.

25. 发明授权

US5625004A Two-step thermal process for the preparation of alkenyl succinic anhydride 失效
标题翻译：用于制备烯基琥珀酸酐的两步热处理
公开(公告)号：US5625004A
公开(公告)日：1997-04-29
申请号：US918990
申请日：1992-07-23
申请人： James J. Harrison , William R. Ruhe, Jr.
发明人： James J. Harrison , William R. Ruhe, Jr.
IPC分类号： C07D307/60 , B01F17/00 , C08F8/46 , C08F255/08 , C10L1/198 , C10M129/93 , C10M133/52 , C10N20/04 , C10N30/04 , C10N70/00 , C10M145/02 , C08F255/02 , C08F255/10
CPC分类号： C10M133/52 , B01F17/0028 , C08F255/08 , C08F255/10 , C08F8/46 , C10L1/198 , C10M129/93 , C10M2207/123 , C10M2207/129 , C10M2207/22 , C10M2215/086 , C10M2215/28
摘要： A process for the preparation of an alkenyl-substituted succinic anhydride wherein the alkenyl substituent has a number average molecular weight of from about 500 to 5000 and the average number of succinic groups per alkenyl group is greater than 1.2 which comprises:(a) reacting a polyolefin having an alkylvinylidene isomer content of less than about 10 percent and a number average molecular weight of about 500 to 5000 with maleic anhydride at a temperature in the range of about 200.degree. C. to 250.degree. C. to provide a mixture of alkenyl succinic anhydride having an average of about 1.0 succinic group per alkenyl group and unreacted polyolefin, and(b) reacting the mixture of alkenyl succinic anhydride and unreacted polyolefin from step (a) with maleic anhydride in the presence of a free radical initiator at a temperature in the range of about 100.degree. C. to 220.degree. C. to thereby provide an alkenyl succinic anhydride having an average of greater than 1.2 succinic groups per alkenyl group.
摘要翻译：一种制备链烯基取代的琥珀酸酐的方法，其中烯基取代基的数均分子量为约500至5000，并且每个烯基的琥珀酸基团的平均数大于1.2，其包括：（a）使具有小于约10％的烷基亚乙烯基异构体含量和约500至5000的数均分子量的聚烯烃与马来酸酐在约200℃至250℃的温度范围内提供烯基琥珀酸酯的混合物平均每个烯基具有约1.0个琥珀酸基团和未反应的聚烯烃的酸酐，和（b）使烯基琥珀酸酐和来自步骤（a）的未反应的聚烯烃的混合物与马来酸酐在游离基引发剂的存在下，在约100℃至220℃的范围内，从而提供每个烯基平均具有大于1.2个琥珀酸基的链烯基琥珀酸酐。

26. 发明授权

US5112507A Polymeric dispersants having alternating polyalkylene and succinic groups 失效
标题翻译：聚合分散剂具有交替的聚亚烷基和琥珀酸基团
公开(公告)号：US5112507A
公开(公告)日：1992-05-12
申请号：US414993
申请日：1989-09-29
申请人： James J. Harrison
发明人： James J. Harrison
IPC分类号： C07C57/13 , C08F8/00 , C08F210/00 , C10L1/14 , C10L1/16 , C10L1/18 , C10L1/22 , C10L1/26 , C10L1/30 , C10M129/93 , C10M129/95 , C10M133/52 , C10M145/16 , C10M149/06 , F02F7/00
CPC分类号： C10M149/06 , C07C57/13 , C08F210/00 , C08F255/10 , C08F8/00 , C08F8/32 , C08F8/42 , C10M129/93 , C10M129/95 , C10M133/52 , C10M145/16 , C08F2800/10 , C08F2810/20 , C10L1/143 , C10L1/1608 , C10L1/1616 , C10L1/1824 , C10L1/221 , C10L1/238 , C10L1/2383 , C10L1/2387 , C10L1/2683 , C10L1/303 , C10M2207/123 , C10M2207/129 , C10M2207/22 , C10M2207/287 , C10M2209/086 , C10M2215/04 , C10M2215/26 , C10M2217/024 , C10M2217/046 , C10M2217/06 , C10N2270/02 , F02F7/006
摘要： Novel copolymers of unsaturated acidic reactants and high molecular weight olefins wherein at least 20 percent of the total high molecular weight olefin comprises the alkylvinylidene isomer are useful as dispersants in lubricating oils and fuels and also may be used to prepare polysuccinimides and other post-treated additives useful in lubricating oils and fuels.
摘要翻译：不饱和酸性反应物和高分子量烯烃的新型共聚物，其中至少20％的总高分子量烯烃包含烷基亚乙烯基异构体可用作润滑油和燃料中的分散剂，也可用于制备聚琥珀酰亚胺和其他后处理添加剂可用于润滑油和燃料。

27. 发明授权

US4711969A Oligomerization of ethylene in methanol and water 失效
标题翻译：乙烯在甲醇和水中的低聚
公开(公告)号：US4711969A
公开(公告)日：1987-12-08
申请号：US900204
申请日：1986-08-25
申请人： David L. Beach , James J. Harrison
发明人： David L. Beach , James J. Harrison
IPC分类号： C07B61/00 , B01J23/755 , B01J31/18 , B01J31/22 , B01J31/24 , C07C1/00 , C07C2/30 , C07C2/32 , C07C2/36 , C07C11/02 , C07C67/00 , C08F4/00 , C08F4/06 , C08F4/26 , C08F4/60 , C08F8/00 , C08F10/02
CPC分类号： B01J31/226 , B01J31/18 , B01J31/2247 , B01J31/2295 , B01J31/2404 , C07C2/32 , C07C2/36 , B01J2231/20 , B01J2531/847 , B01J2531/96 , C07C2531/22 , C07C2531/24 , Y02P20/52
摘要： A process for oligomerizing ethylene using a nickel ylide catalyst substituted with a sulfonato group, wherein the oligomerization is carried out in the presence of methanol and water.
摘要翻译：使用被磺酰基取代的内酯化催化剂使乙烯低聚的方法，其中低聚反应在甲醇和水的存在下进行。

28. 发明授权

US4573534A Cement compositions and method of cementing casing in a well 失效
标题翻译：水泥组合物和井筒固井方法
公开(公告)号：US4573534A
公开(公告)日：1986-03-04
申请号：US650071
申请日：1984-06-12
申请人： Wilford S. Baker , James J. Harrison
发明人： Wilford S. Baker , James J. Harrison
IPC分类号： C04B24/38 , C04B28/02 , C09K8/42 , C09K8/46 , C04B24/04 , E21B33/14
CPC分类号： C04B28/02 , C04B24/383 , C04B28/04 , C09K8/42 , C09K8/46 , C09K8/467 , C04B2103/0028 , C04B2103/0036
摘要： A novel cement composition comprising (1) cement, (2) at least one polysaccharide, and (3) a viscosity modifying amount of a 1,2-dicarbonyl; aqueous slurries prepared from these novel cement compositions and a method of cementing casing in the borehole of a well using such novel aqueous cement slurries.
摘要翻译：一种新型水泥组合物，其包含（1）水泥，（2）至少一种多糖，和（3）粘度调节量的1,2-二羰基; 由这些新型水泥组合物制备的水性浆料以及使用这种新型水性水泥浆料将套管固定在井眼中的方法。

29. 发明授权

US4462837A Cement composition and method of cement casing in a well 失效
标题翻译：水泥套管在井中的水泥组成和方法
公开(公告)号：US4462837A
公开(公告)日：1984-07-31
申请号：US466551
申请日：1983-02-15
申请人： Wilford S. Baker , James J. Harrison
发明人： Wilford S. Baker , James J. Harrison
IPC分类号： C04B24/38 , C09K8/46 , C09K8/487 , C04B7/353
CPC分类号： C04B24/383 , C09K8/46 , C09K8/487 , C04B2103/46
摘要： A novel cement composition for the preparation of a novel aqueous slurry useful in cementing casing in the borehole of a well comprising (1) cement, (2) (a) a hydroxyethylcellulose ether having a critical viscosity or (2) (b) a mixture of a hydroxyethylcellulose ether having a critical viscosity and of a hydroxypropylcellulose ether having a critical viscosity and (3) a dispersant.
摘要翻译：一种用于制备用于在井眼钻井中固井套管的新型含水浆料的新型水泥组合物，其包含（1）水泥，（2）（a）具有临界粘度的羟乙基纤维素醚或（2）（b）混合物具有临界粘度的羟乙基纤维素醚和具有临界粘度的羟丙基纤维素醚，和（3）分散剂。

30. 发明授权

US4382153A Process for the oligomerization of ethylene in methanol 失效
公开(公告)号：US4382153A
公开(公告)日：1983-05-03
申请号：US365291
申请日：1982-04-05
申请人： David L. Beach , James J. Harrison
发明人： David L. Beach , James J. Harrison
IPC分类号： C07C2/36 , C07C2/02
CPC分类号： C07C2/36 , C07C2531/24
摘要： Ethylene is oligomerizied by reacting ethylene under an elevated pressure greater than about 700 pounds per square inch gauge (4826 kPa) in methanol in contact with a nickel ylide defined by the following Formula: ##STR1## wherein R.sub.1, R.sub.2, R.sub.3, R.sub.4, R.sub.5, R.sub.6, R.sub.7 and R.sub.8 are either alike or different members selected from the group consisting of hydrogen, alkyl radicals having from about one to about 24 carbon atoms, preferably from about one to about 10 carbon atoms; aryl radicals having from about six to about 20 carbon atoms, preferably from about six to about 10 carbon atoms; alkenyl radicals having from about two to about 30 carbon atoms, preferably from about two to about 20 carbon atoms; cycloalkyl radicals having from about three to about 40 carbon atoms, preferably from about three to about 30 carbon atoms; aralkyl and alkaryl radicals having from about six to about 40 carbon atoms, preferably from about six to about 30 carbon atoms; a halogen radical selected from the group consisting of fluorine, chlorine, bromine and iodine, preferably chlorine; a hydroxyl group; an alkoxy or aryloxy group; and a hydrocarbyl group, such as defined above, carrying halogen, hydroxyl or alkoxy or aryloxy; provided that at least one, preferably from about one to about four, of each of R.sub.1 to R.sub.8 is a sulfonato group (--SO.sub.3.sup.-) or an alkyl, aryl, alkenyl, cycloalkyl, aralkyl or alkaryl group carrying a sulfonato group; M is sulfur or oxygen, preferably oxygen; E is phosphorus, arsenic, antimony or nitrogen, preferably phosphorus; and F is phosphorus, arsenic or antimony, preferably phosphorus. There is thus obtained a reaction product containing (A) a methanol phase having dissolved therein the nickel ylide catalyst and (B) an alpha-olefin phase. These two phases are then separated from each other to recover the alpha-olefin phase. The use of methanol as the solvent medium causes the reaction product to resolve itself into two phases: an upper phase containing most of the oligomer product, and a lower methanol phase carrying the catalyst dissolved therein. This permits easy separation of the product from the reaction mixture and also permits effective recycle of methanol with dissolved catalyst. The product obtained contains normal alpha-olefins having from about four to about 100 carbon atoms, generally from about four to about 50 carbon atoms.

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