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21. 发明授权

US06828465B2 Method for producing bisphenols 有权
标题翻译：生产双酚的方法
公开(公告)号：US06828465B2
公开(公告)日：2004-12-07
申请号：US10239544
申请日：2002-12-16
申请人： Rainer Neumann , Rolf Lanze , Frieder Heydenreich , Michael Bödiger , Michael Prein
发明人： Rainer Neumann , Rolf Lanze , Frieder Heydenreich , Michael Bödiger , Michael Prein
IPC分类号： C07C3768
CPC分类号： C07C37/84 , C07C37/685 , C07C39/16
摘要： The present invention provides crystals of an adduct of a bisphenol and a phenol and methods of producing those crystals. The crystals may find use in preparing bisphenols.
摘要翻译：本发明提供了双酚和苯酚的加成物的晶体和制备这些晶体的方法。晶体可能用于制备双酚。

22. 发明授权

US06395864B1 Polycarbonates with a low yellowness index 失效
标题翻译：黄色指数低的聚碳酸酯
公开(公告)号：US06395864B1
公开(公告)日：2002-05-28
申请号：US09868826
申请日：2001-06-20
申请人： Steffen Kühling , Rolf Lanze , Michael Prein , Rainer Neumann , Hermann Kauth , Christian Kords , Frieder Heydenreich , Tony van Osselaer , Wilfried Haese
发明人： Steffen Kühling , Rolf Lanze , Michael Prein , Rainer Neumann , Hermann Kauth , Christian Kords , Frieder Heydenreich , Tony van Osselaer , Wilfried Haese
IPC分类号： C08G6400
CPC分类号： G11B7/2534 , C08G64/24 , Y10T428/31507
摘要： A process for the preparation of polycarbonate resins having a low yellowness index is described. The process involves converting phosgene with a sodium bisphenolate solution by means of a phase interface process performed with the exclusion of oxygen. The sodium bisphenolate solution used in the process has a dissolved oxygen content of
摘要翻译：描述了一种制备低黄度指数的聚碳酸酯树脂的方法。该方法涉及通过用排除氧气进行的相界面方法用双酚钠溶液转化光气。该方法中使用的双酚钠溶液的溶解氧含量<150ppb。还描述了由本发明的聚碳酸酯制备的光学数据存储介质。

23. 发明授权

US06291630B1 Method for producing a liquid formulation of tetraphenylphosphonium phenolate 有权
标题翻译：苯酚四苯基膦液体制剂的制备方法
公开(公告)号：US06291630B1
公开(公告)日：2001-09-18
申请号：US09623635
申请日：2000-09-06
申请人： Annett König , Michael Prein
发明人： Annett König , Michael Prein
IPC分类号： C08G6400
CPC分类号： C08G64/307 , B01J31/0268 , B01J2231/14 , B01J2231/40 , B01J2231/49 , C07C39/235 , C07F9/5442
摘要： A catalyst formulation that is liquid at room temperature and that comprise tetraphenylphosphonium phenolate and phenol is disclosed. The catalyst formulation is suitable as a transesterification catalyst and most especially in the preparation of thermoplastic solvent-free polycarbonates.
摘要翻译：公开了一种在室温下为液体并且包含苯酚四苯基苯酚和苯酚的催化剂制剂。催化剂配方适合作为酯交换催化剂，最特别是在制备无溶剂的聚碳酸酯中。

24. 发明授权

US08410184B2 Regeneration of acidic ion exchangers 失效
标题翻译：酸性离子交换剂的再生
公开(公告)号：US08410184B2
公开(公告)日：2013-04-02
申请号：US12784870
申请日：2010-05-21
申请人： Michael Prein , Christian Münnich , Ulrich Blaschke
发明人： Michael Prein , Christian Münnich , Ulrich Blaschke
IPC分类号： B01J38/60 , B01J38/62
CPC分类号： B01J31/10 , B01J31/4007 , B01J2231/347 , C07C37/20 , Y02P20/584 , C07C39/16
摘要： The invention relates to a method for regenerating acidic cation exchangers, which are used as catalysts in the reaction of phenols with aldehydes or ketones to give bisphenols, in particular to give bisphenol A, with acids, with the proviso that, in the method according to the invention, these cation exchangers experience very little mechanical damage due to swelling processes during the regeneration process.
摘要翻译：本发明涉及一种用于再生酸性阳离子交换剂的方法，其用作苯酚与醛或酮反应的催化剂，以产生双酚，特别是产生双酚A与酸，条件是在根据在本发明中，这些阳离子交换剂在再生过程中由于溶胀过程而经历很少的机械损伤。

25. 发明申请

US20110112240A1 POLYCARBONATES HAVING IMPROVED TRANSMISSION 审中-公开
标题翻译：具有改进传输的聚碳酸酯
公开(公告)号：US20110112240A1
公开(公告)日：2011-05-12
申请号：US12940431
申请日：2010-11-05
申请人： Berit Krauter , Michael Prein
发明人： Berit Krauter , Michael Prein
IPC分类号： C08L69/00 , B29C45/00
CPC分类号： C08L69/00 , C08L71/02 , C08L2666/22
摘要： The present invention relates to a composition containing polycarbonate and 0.01 wt. % to less than 0.30 wt. % of polyol, polyether polyol, or combinations thereof.
摘要翻译：本发明涉及含有聚碳酸酯和0.01wt。％至小于0.30重量％％的多元醇，聚醚多元醇或其组合。

26. 发明授权

US07763757B2 Crystallization processes for producing bisphenols 有权
标题翻译：生产双酚的结晶过程
公开(公告)号：US07763757B2
公开(公告)日：2010-07-27
申请号：US11971268
申请日：2008-01-09
申请人： Christian Münnich , Ulrich Blaschke , Rob Eek , Michael Prein , Raymond Audenaert , Gert Tytgat
发明人： Christian Münnich , Ulrich Blaschke , Rob Eek , Michael Prein , Raymond Audenaert , Gert Tytgat
IPC分类号： C07C37/84 , C07C39/16
CPC分类号： C07C37/20 , C07C37/84 , C07C39/16
摘要： Processes for producing bisphenols (e.g., bisphenol A (BPA)) having a purity greater than 99.7% are described, such processes including reacting a phenol and acetone in the presence of an acidic catalyst to form a product mixture comprising a bisphenol; removing at least a portion of the bisphenol from the product mixture in the form of a bisphenol/phenol adduct by crystallization, filtration and washing to provide bisphenol/phenol adduct crystals; and removing at least a portion of the phenol from the bisphenol/phenol adduct crystals to provide the bisphenol having a purity of more than 99.7%; wherein the crystallization comprises continuous suspension crystallization and is carried out in at least three crystallization devices arranged such that the product mixture is first cooled in a first stage of the crystallization to a temperature of 50 to 70° C. in a first crystallization device and a second crystallization device connected in parallel, and subsequently cooled in a second stage of the crystallization to a temperature of 40 to 50° C. in a third crystallization device connected downstream in series to the first and second crystallization devices, and wherein a total dwell time of the product mixture in the crystallization is more than 4 hours.
摘要翻译：描述了用于生产纯度大于99.7％的双酚（例如双酚A（BPA））的方法，包括在酸性催化剂存在下使苯酚和丙酮反应以形成包含双酚的产物混合物; 通过结晶，过滤和洗涤从双酚/苯酚加合物的形式从产物混合物中除去至少一部分双酚以提供双酚/苯酚加合物晶体; 并从双酚/苯酚加合物晶体中除去至少一部分苯酚，得到纯度大于99.7％的双酚; 其中所述结晶包括连续悬浮液结晶，并且在至少三个结晶装置中进行，所述结晶装置被排列成使得产物混合物在结晶的第一阶段首先在第一结晶装置中冷却至50至70℃，第二结晶装置并联连接，随后在结晶的第二阶段中在与第一和第二结晶装置串联下游的第三结晶装置中冷却至40至50℃的温度，并且其中总停留时间的产物混合物在结晶中超过4小时。

27. 发明申请

US20090137709A1 POLYOL-CONTAINING, FLAME-RESISTANT POLYCARBONATES, PROCESSES FOR PREPARING THE SAME AND PRODUCTS CONTAINING THE SAME 审中-公开
标题翻译：含多元醇，耐火聚碳酸酯，其制备方法和含有该聚合物的产品
公开(公告)号：US20090137709A1
公开(公告)日：2009-05-28
申请号：US12262346
申请日：2008-10-31
申请人： Berit Krauter , Wolfgang Ebert , Michael Prein , Michael Wagner
发明人： Berit Krauter , Wolfgang Ebert , Michael Prein , Michael Wagner
IPC分类号： C08K5/42 , C08K5/435
CPC分类号： C08L69/00 , C08K5/42 , C08K5/43 , C08L71/02 , C08L79/08 , C08L2205/03 , C08L2666/22 , C08L2666/14
摘要： Flame-resistant compositions comprising: a polycarbonate; 0.01 to
摘要翻译：耐火组合物，包含：聚碳酸酯; 0.01〜<0.3wt。％的多元醇; 和0.01〜0.8重量％选自碱金属，碱土金属及其混合物的金属盐，以及选自磺酸，磺酰胺，磺酰亚胺及其混合物的化合物的盐; 制备方法及其制备的产品。

28. 发明申请

US20080200734A1 CRYSTALLIZATION PROCESSES FOR PRODUCING BISPHENOLS 有权
标题翻译：生产双酚的结晶方法
公开(公告)号：US20080200734A1
公开(公告)日：2008-08-21
申请号：US11971268
申请日：2008-01-09
申请人： Christian Munnich , Ulrich Blaschke , Rob Eek , Michael Prein , Raymond Audenaert , Gert Tytgat
发明人： Christian Munnich , Ulrich Blaschke , Rob Eek , Michael Prein , Raymond Audenaert , Gert Tytgat
IPC分类号： C07C39/04
CPC分类号： C07C37/20 , C07C37/84 , C07C39/16
摘要： Processes for producing bisphenols (e.g., bisphenol A (BPA)) having a purity greater than 99.7% are described, such processes including reacting a phenol and acetone in the presence of an acidic catalyst to form a product mixture comprising a bisphenol; removing at least a portion of the bisphenol from the product mixture in the form of a bisphenol/phenol adduct by crystallization, filtration and washing to provide bisphenol/phenol adduct crystals; and removing at least a portion of the phenol from the bisphenol/phenol adduct crystals to provide the bisphenol having a purity of more than 99.7%; wherein the crystallization comprises continuous suspension crystallization and is carried out in at least three crystallization devices arranged such that the product mixture is first cooled in a first stage of the crystallization to a temperature of 50 to 70° C. in a first crystallization device and a second crystallization device connected in parallel, and subsequently cooled in a second stage of the crystallization to a temperature of 40 to 50° C. in a third crystallization device connected downstream in series to the first and second crystallization devices, and wherein a total dwell time of the product mixture in the crystallization is more than 4 hours.
摘要翻译：描述了用于生产纯度大于99.7％的双酚（例如双酚A（BPA））的方法，包括在酸性催化剂存在下使苯酚和丙酮反应以形成包含双酚的产物混合物; 通过结晶，过滤和洗涤从双酚/苯酚加合物的形式从产物混合物中除去至少一部分双酚以提供双酚/苯酚加合物晶体; 并从双酚/苯酚加合物晶体中除去至少一部分苯酚，得到纯度大于99.7％的双酚; 其中所述结晶包括连续悬浮液结晶，并且在至少三个结晶装置中进行，所述结晶装置被排列成使得产物混合物在结晶的第一阶段首先在第一结晶装置中冷却至50至70℃，第二结晶装置并联连接，随后在结晶的第二阶段中在与第一和第二结晶装置串联下游的第三结晶装置中冷却至40至50℃的温度，并且其中总停留时间的产物混合物在结晶中超过4小时。

29. 发明授权

US07071283B2 Reactive rectification 失效
标题翻译：反应整顿
公开(公告)号：US07071283B2
公开(公告)日：2006-07-04
申请号：US10344965
申请日：2001-08-10
申请人： Gerald John , Edmund Dikow , Christine Mendoza-Frohn , Georg Ronge , Rolf Bachmann , Lutz Gottschalk , Michael Prein
发明人： Gerald John , Edmund Dikow , Christine Mendoza-Frohn , Georg Ronge , Rolf Bachmann , Lutz Gottschalk , Michael Prein
IPC分类号： C08G64/00
CPC分类号： C08G64/205 , B01D3/009 , C08G64/307 , Y02P20/127 , Y10T428/24273
摘要： The invention relates to a method for producing polycarbonate according to the method for the transesterification of molten mass whereby bis-(hydroxyaryl) compounds (bisphenols) and diaryl carbonates are reacted by means of reactive rectification.
摘要翻译：本发明涉及一种根据熔融物质酯交换法制备聚碳酸酯的方法，其中双（（羟基芳基）化合物（双酚）和碳酸二芳基酯通过无功整流反应。

30. 发明授权

US06906227B2 Bisphenol phenol adducts 有权
标题翻译：双酚酚加合物
公开(公告)号：US06906227B2
公开(公告)日：2005-06-14
申请号：US10149905
申请日：2000-12-07
申请人： Rainer Neumann , Rolf Lanze , Frieder Heydenreich , Michael Bödiger , Michael Prein
发明人： Rainer Neumann , Rolf Lanze , Frieder Heydenreich , Michael Bödiger , Michael Prein
IPC分类号： B01D33/06 , B01D9/02 , C07C37/70 , C07C37/82 , C07C37/84 , C07C39/16
CPC分类号： C07C37/70 , C07C37/82 , C07C39/16
摘要： The application relates to a process for producing high-purity bis(4-hydroxyaryl)alkanes from adducts of bis(4-hydroxyaryl)alkanes and aromatic hydroxy compounds, which are obtained by acid-catalysed reaction of the aromatic hydroxy compounds with ketones.
摘要翻译：本申请涉及通过芳族羟基化合物与酮的酸催化反应获得的由双（4-羟基芳基）烷烃和芳族羟基化合物的加合物生产高纯度双（4-羟基芳基）烷烃的方法。

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