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21. 发明授权

US08936767B2 Oxidation system with sidedraw secondary reactor 有权
标题翻译：具有侧面二次反应器的氧化系统
公开(公告)号：US08936767B2
公开(公告)日：2015-01-20
申请号：US12957730
申请日：2010-12-01
申请人： Ashfaq Shaikh , Alan George Wonders , David Lange
发明人： Ashfaq Shaikh , Alan George Wonders , David Lange
IPC分类号： B01J8/18 , B01J8/22 , B01J10/00 , B01J8/00 , B01J19/00 , B01J19/24 , B01J35/00 , B01J35/02 , C07C51/00 , C07C51/16 , C07C51/21 , C07C51/255 , C07C51/265
CPC分类号： B01J8/228 , B01J8/22 , B01J10/00 , B01J2208/00274 , B01J2208/003 , C07C51/265 , C07C63/26
摘要： Disclosed are process and apparatus for vertical splitting of the oxygen supply to a post-oxidation reactor. Further disclosed are process and apparatus for supplying reaction medium to a post-oxidation reactor at a mid-level inlet. Such apparatus and process can assist in reducing oxygen pinch throughout the post-oxidation reactor.
摘要翻译：公开了用于将氧气供应垂直分离到后氧化反应器的方法和装置。还公开了用于在中级入口向后氧化反应器供应反应介质的方法和装置。这种设备和方法可以帮助减少整个后氧化反应器中的氧气。

22. 发明授权

US07910071B2 Optimized liquid-phase oxidation 有权
公开(公告)号：US07910071B2
公开(公告)日：2011-03-22
申请号：US12548475
申请日：2009-08-27
申请人： Alan George Wonders , Howard Wood Jenkins, Jr. , Lee Reynolds Partin , Wayne Scott Strasser , Marcel de Vreede
发明人： Alan George Wonders , Howard Wood Jenkins, Jr. , Lee Reynolds Partin , Wayne Scott Strasser , Marcel de Vreede
IPC分类号： B01J19/24 , B01J19/00 , F27B15/08 , C07C65/00 , C07C51/00 , C07C51/16 , C07C51/255
CPC分类号： B01J8/226 , B01J8/1818 , B01J8/1872 , B01J8/222 , B01J19/006 , B01J2219/0004 , C07C51/265 , C07C63/26
摘要： Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.

23. 发明授权

US07902396B2 Optimized liquid-phase oxidation 有权
公开(公告)号：US07902396B2
公开(公告)日：2011-03-08
申请号：US12490441
申请日：2009-06-24
申请人： Alan George Wonders , Gino Georges Lavoie , Charles Edwan Sumner, Jr.
发明人： Alan George Wonders , Gino Georges Lavoie , Charles Edwan Sumner, Jr.
IPC分类号： C07C51/16
CPC分类号： C07C51/265 , C07C63/26
摘要： Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.

24. 发明授权

US07884232B2 Optimized liquid-phase oxidation 有权
公开(公告)号：US07884232B2
公开(公告)日：2011-02-08
申请号：US11365441
申请日：2006-03-01
申请人： Alan George Wonders , Thomas Young Lightfoot , Thomas Earl Woodruff , Charles Helton Hitchcock , David Lee Denton , Carl Norman McCurry
发明人： Alan George Wonders , Thomas Young Lightfoot , Thomas Earl Woodruff , Charles Helton Hitchcock , David Lee Denton , Carl Norman McCurry
IPC分类号： C07C51/16
CPC分类号： C07C51/265 , C07C63/26
摘要： Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.

25. 发明申请

US20100087675A1 Dicarboxylic Acid Production with Minimal Wastewater Generation 有权
标题翻译：以最少的废水生成的二羧酸生产
公开(公告)号：US20100087675A1
公开(公告)日：2010-04-08
申请号：US12556096
申请日：2009-09-09
申请人： Raymond Elbert Fogle, III , Ronald Buford Sheppard , Timothy Alan Upshaw , Alan George Wonders
发明人： Raymond Elbert Fogle, III , Ronald Buford Sheppard , Timothy Alan Upshaw , Alan George Wonders
IPC分类号： C07C51/255
CPC分类号： C07C51/265 , C07C63/24 , C07C63/26 , C07C63/15
摘要： The invention provides improved energy content in and shaft power recovery from off-gas from xylene oxidation reactions while at the same time minimizing wastewater treatment cost. More shaft power is produced using off-gas than is required to drive the main air compressor, even with preferred, relatively low oxidation temperatures. Simultaneously, an amount of wastewater greater than byproduct water from oxidation of xylene is kept in vapor form and treated along with off-gas pollutants in a self-sustaining (self-fueling) gas-phase thermal oxidative destruction unit. Optionally, off-gas is combined from multiple xylene oxidation reactors, comprising primary and/or secondary oxidation reactors and forming TPA and/or IPA. Optionally, air compressor condensate and caustic scrubber blowdown are used in a TPA process or as utility water, effectively eliminating normal flow of liquid wastewater effluent from a TPA plant. Optionally, PET off-gas containing the water of PET formation is treated in a shared thermal oxidative destruction unit, effectively eliminating normal flow of liquid wastewater effluent from a combined pX-to-TPA-to-PET plant.
摘要翻译：本发明提供了来自二甲苯氧化反应的废气的改进的能量含量和轴功率回收，同时使废水处理成本最小化。即使使用优选的相对低的氧化温度，也可以使用除了驱动主空气压缩机所需的废气以外的更多的轴功率。同时，大量来自二氧化碳氧化的副产物水的废水保持蒸气形式，并在自持（自燃）气相热氧化破坏装置中与废气污染物一起处理。任选地，废气从包括初级和/或二级氧化反应器并形成TPA和/或IPA的多个二甲苯氧化反应器组合。任选地，空气压缩机冷凝物和苛性碱洗涤器排污用于TPA方法或作为效用水，有效地消除了来自TPA设备的液体废水流出物的正常流动。任选地，在共同的热氧化破坏单元中处理含有PET形成水的PET废气，有效地消除了从组合的pX到TPA到PET植物的液体废水流出物的正常流动。

26. 发明授权

US07568361B2 Optimized liquid-phase oxidation 有权
公开(公告)号：US07568361B2
公开(公告)日：2009-08-04
申请号：US11154218
申请日：2005-06-16
申请人： Alan George Wonders , Robert Lin , Marcel de Vreede , Lee Reynolds Partin
发明人： Alan George Wonders , Robert Lin , Marcel de Vreede , Lee Reynolds Partin
IPC分类号： C07C51/16
CPC分类号： B01J8/1818 , B01J4/002 , B01J8/1872 , B01J8/22 , B01J8/226 , B01J2208/0084 , B01J2219/00006 , B01J2219/0004 , C07C51/265 , C07C63/26
摘要： Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.

27. 发明授权

US07420082B2 Polycarboxylic acid production system employing hot liquor removal downstream of oxidative digestion 有权
标题翻译：聚羧酸生产系统采用热液除去氧化消解下游
公开(公告)号：US07420082B2
公开(公告)日：2008-09-02
申请号：US11365258
申请日：2006-03-01
申请人： Alan George Wonders , Ronald Buford Sheppard , Martin De Boer
发明人： Alan George Wonders , Ronald Buford Sheppard , Martin De Boer
IPC分类号： C07C61/00 , C07C51/23
CPC分类号： C07C51/265 , C07C51/42 , C07C63/26
摘要： Disclosed is an optimized system for more efficiently and economically producing terephthalic acid. The system includes an optimized post-digestion cooling stage that provides a TPA product having enhanced purity, while minimizing costs associated with removing impurities from recycled solvent.
摘要翻译：公开了一种更有效和经济地生产对苯二甲酸的优化系统。该系统包括优化的消化后冷却阶段，其提供具有增强的纯度的TPA产物，同时最小化从再循环溶剂中除去杂质所涉及的成本。

28. 发明申请

US20080194864A1 Optimized liquid-phase oxidation 有权
公开(公告)号：US20080194864A1
公开(公告)日：2008-08-14
申请号：US12105389
申请日：2008-04-18
申请人： Alan George Wonders , Lee Reynolds Partin , Wayne Scott Strasser , Marcel de Vreede , Puneet Gupta
发明人： Alan George Wonders , Lee Reynolds Partin , Wayne Scott Strasser , Marcel de Vreede , Puneet Gupta
IPC分类号： C07C51/265
CPC分类号： B01J8/22 , B01J4/002 , B01J8/1818 , B01J8/1872 , B01J8/222 , B01J2208/00079 , B01J2208/003 , B01J2219/00006 , B01J2219/0004 , C07C51/265 , C07C63/26
摘要： Disclosed is an optimized process and apparatus for more efficiently and economically carrying out the liquid-phase oxidation of an oxidizable compound. Such liquid-phase oxidation is carried out in a bubble column reactor that provides for a highly efficient reaction at relatively low temperatures. When the oxidized compound is para-xylene and the product from the oxidation reaction is crude terephthalic acid (CTA), such CTA product can be purified and separated by more economical techniques than could be employed if the CTA were formed by a conventional high-temperature oxidation process.

29. 发明申请

US20070219393A1 Polycarboxylic acid production system with enhanced residence time distribution for oxidative digestion 有权
标题翻译：聚羧酸生产体系具有增强的氧化消化停留时间分布
公开(公告)号：US20070219393A1
公开(公告)日：2007-09-20
申请号：US11366004
申请日：2006-03-01
申请人： Robert Lin , Ruairi Seosamh O'Meadhra , Alan George Wonders , Thomas Michael Pell
发明人： Robert Lin , Ruairi Seosamh O'Meadhra , Alan George Wonders , Thomas Michael Pell
IPC分类号： C07C51/16 , C07C51/255 , F01N3/10
CPC分类号： C07C51/265 , C07C63/26
摘要： Disclosed is an optimized system for more efficiently and economically producing terephthalic acid. The system includes an oxidative digestion reactor/zone configured to provide optimized residence time distribution for the solid and liquid phases of the reaction medium processed therein.
摘要翻译：公开了一种更有效和经济地生产对苯二甲酸的优化系统。该系统包括氧化消化反应器/区域，其构造成为其中处理的反应介质的固相和液相提供优化的停留时间分布。

30. 发明授权

US06417296B2 Process for producing polyolefins 有权
标题翻译：生产聚烯烃的方法
公开(公告)号：US06417296B2
公开(公告)日：2002-07-09
申请号：US09818327
申请日：2001-03-27
申请人： Randal Ray Ford , Kenneth Alan Dooley , Jeffrey James Vanderbilt , Roxanna Lea Whitfield , Alan George Wonders
发明人： Randal Ray Ford , Kenneth Alan Dooley , Jeffrey James Vanderbilt , Roxanna Lea Whitfield , Alan George Wonders
IPC分类号： C08F234
CPC分类号： C08F10/00 , C08F210/16 , Y10S526/901 , C08F2/002 , C08F4/6294 , C08F4/6293 , C08F210/08 , C08F2500/12 , C08F210/06 , C08F210/14
摘要： A novel process for producing homopolymers and interpolymers of olefins which involves contacting an olefin and/or an olefin and at least one or more other olefin(s) under polymerization conditions with a Ziegler-Natta catalyst comprising at least one transition metal compound and at least one organometallic co-catalyst compound and tetrahydrofuran in amounts sufficient to reduce the electrostatic charge in the polymerization medium. Also disclosed is a process for reducing electrostatic charge in an olefin polymerization medium.
摘要翻译：一种制备烯烃的均聚物和共聚体的新方法，其包括在聚合条件下使烯烃和/或烯烃与至少一种或多种其它烯烃与包含至少一种过渡金属化合物的齐格勒 - 纳塔催化剂和至少一种有机金属助催化剂化合物和四氢呋喃，其量足以减少聚合介质中的静电电荷。还公开了一种减少烯烃聚合介质中的静电荷的方法。

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