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21. 发明申请

WO2013087523A1 ABTRENNUNG VON 5-HYDROXYMETHYLFURFURAL (HMF) AUS REAKTIONSLÖSUNGEN DURCH WASSERDAMPF-DESTILLATION 审中-公开
标题翻译：通过蒸汽蒸馏从反应液的5-羟甲基糠醛（HMF）分离
公开(公告)号：WO2013087523A1
公开(公告)日：2013-06-20
申请号：PCT/EP2012/074737
申请日：2012-12-07
申请人： BASF SE , BÖHLING, Ralf , BLANK, Benoit , KINDLER, Alois , FELDNER, Carmen , UMLAUF, Sandra , BASF SCHWEIZ AG
发明人： BÖHLING, Ralf , BLANK, Benoit , KINDLER, Alois , FELDNER, Carmen , UMLAUF, Sandra
IPC分类号： C07D307/46
CPC分类号： C07D307/46
摘要： Verfahren zur Herstellung von Lösungen, welche 5-Hydroxymethylfurfural (HMF) enthalten und einen verminderten Gehalt an Ausgangsstoffen der HMF-Synthese oder einen verminderten Gehalt an Nebenprodukten der HMF-Synthese aufweisen (im Nachfolgenden Produkt-Lösung genannt), dadurch gekennzeichnet, dass Lösungen, welche - HMF - Ausgangsstoffe oder Nebenprodukte der HMF-Synthese und - ein organisches Lösemittel mit mindestens zwei Ethergruppen (kurz Polyether) enthalten (im Nachfolgenden Ausgangs-Lösung genannt), in einem Verdampfer mit Wasserdampf behandelt werden.
摘要翻译：一种用于容纳5-羟甲基糠醛（HMF）和HMF合成或副产品HMF合成的包括（以下称产物溶液）含量降低的起始材料的含量降低了溶液的制备方法，其特征在于解其中 - HMF - 起始原料或副产物HMF合成的，和 - 具有至少两个醚基团（短聚醚）含有（以下称为初始溶液）的有机溶剂中与水蒸汽的蒸发器进行处理。

22. 发明申请

WO2013010971A1 PROCESS FOR A CONTINUOUS PRODUCTION OF POLYETHEROLS 审中-公开
标题翻译：连续生产聚醚的方法
公开(公告)号：WO2013010971A1
公开(公告)日：2013-01-24
申请号：PCT/EP2012/063866
申请日：2012-07-16
申请人： BASF SE , CHILEKAR, Vinit , BEY, Oliver , BRODHAGEN, Andreas , LÖFFLER, Achim , AHMADNIAN, Fatemeh , BÖHLING, Ralf , GROßMANN, Christoph , KAMMEL, Ulrich , ADELMANN, Ronald , OSTROWSKI, Thomas , JOSHI, Milind , WATERS, Gerrit , MECKELNBURG, Dirk
发明人： CHILEKAR, Vinit , BEY, Oliver , BRODHAGEN, Andreas , LÖFFLER, Achim , AHMADNIAN, Fatemeh , BÖHLING, Ralf , GROßMANN, Christoph , KAMMEL, Ulrich , ADELMANN, Ronald , OSTROWSKI, Thomas , JOSHI, Milind , WATERS, Gerrit , MECKELNBURG, Dirk
IPC分类号： C08G65/00
CPC分类号： C08G65/2609 , C08G65/2696
摘要： The invention relates to a process for a continuous production of polyetherols comprising the steps of reacting of an alcohol (3) with a starter (5) or an alkoxylated precursor to give a mixture comprising an alcoholate and water, removing the water from the mixture by distillation,if appropriate feeding the alcoholate into a bubble column (23), having an inclination of from 0 to 90 to the horizontal, the bubble column (23)being divided into at least two compartments (25), wherein the compartments (25) are divided from each other by a dividing wall (27), the dividing wall (27) having a height, that liquid can flow over the dividing wall (27) from one compartment (25) into an adjacent compartment, feeding of alkylene oxide into at least one compartment (25) at the bottom of the compartment such that the alkylene oxide rises in the alcoholate, reacting of the alkylene oxide with the alcoholate or a secondary product being formed by the reaction of the alcoholate with alkylene oxide to give the polyetherol, discharging the reaction product from the bubble column (23).
摘要翻译：本发明涉及一种连续生产聚醚醚的方法，包括以下步骤：使醇（3）与起始物（5）或烷氧基化前体反应，得到包含醇化物和水的混合物，通过蒸馏，如果适当地将醇化物进料到气泡塔（23）中，其具有0至90°相对于水平面的倾斜度，气泡塔（23）被分成至少两个室（25），其中隔室（25）通过分隔壁（27）彼此分开，分隔壁（27）具有高度，液体可以在分隔壁（27）上从一个隔室（25）流到相邻的隔室中，将烯化氧进料到在室的底部的至少一个隔间（25），使得烯化氧在醇化物中升高，烯化氧与醇化物的反应或通过醇化物与烯化氧的反应形成的次级产物至gi 然后将聚合物从气泡塔（23）排出。

23. 发明申请

WO2008095931A2 FLÜSSIGKEITGETRÄNKTES SCHAUMSTOFFFORMTEIL AUF BASIS EINES AMINOPLASTEN UND DESSEN VERWENDUNGEN 审中-公开
标题翻译：液体浸泡发泡成型基于氨基塑料及其用途
公开(公告)号：WO2008095931A2
公开(公告)日：2008-08-14
申请号：PCT/EP2008/051400
申请日：2008-02-05
申请人： BASF SE , QUADBECK-SEEGER, Hans-Jürgen , ALTEHELD, Armin , HAHN, Klaus , SCHERZER, Dietrich , MÖCK, Christof , VATH, Bernhard , BODE, Andreas , BÖHLING, Ralf
发明人： QUADBECK-SEEGER, Hans-Jürgen , ALTEHELD, Armin , HAHN, Klaus , SCHERZER, Dietrich , MÖCK, Christof , VATH, Bernhard , BODE, Andreas , BÖHLING, Ralf
IPC分类号： C08J9/40 , C09K5/06 , F28D20/02
CPC分类号： C09K5/063 , C08J9/40 , C08J2201/038 , C08J2205/05 , C08J2361/28 , F28D20/023 , Y02E60/145 , Y10T428/249995 , Y10T428/249997
摘要： Ein flüssigkeitgetränktes Schaumstoffformteil, bestehend aus a) 1 bis 10 Vol.-%. eines offenzelligen Schaumstoffes auf Basis eines Aminoplasten und b) 90 bis 99 Vol.-% einer bei 25°C flüssigen Komponente, wie aromatischer oder aliphatische Kohlenwasserstoffe, Alkohole, Ketone, Wasser oder wässrige Dispersionen, sowie dessen Verwendungen zum Transportieren oder Dosieren von Flüssigkeiten, zur Gefriersprengung, zur Energieabsorption von Geschossen oder als latente Wärmespeicher.
摘要翻译：一种液体浸渍的发泡成型，包括a）1至10体积％。基于氨基塑料，和b）90至99体积百分比的液体％在25℃下成分，例如芳族或脂族烃，醇，酮，水或水分散体的开孔泡沫，以及它们的用途用于输送或流体的计量，到冷冻爆炸，射弹的或作为潜热蓄热的能量吸收。

24. 发明公开

EP1483230A1 VERFAHREN ZUR HERSTELLUNG VON ETHYLDIMETHYLAMIN UND TRIETHYLAMIN 审中-公开
标题翻译：工艺用于生产和乙基二 - 三乙胺
公开(公告)号：EP1483230A1
公开(公告)日：2004-12-08
申请号：EP03711916.1
申请日：2003-03-03
申请人： BASF AKTIENGESELLSCHAFT
发明人： BÖHLING, Ralf , STEINBRENNER, Ulrich , FUNKE, Frank , MÜLLER, Günter , GAUS, Günter , BENISCH, Christoph
IPC分类号： C07C209/60
CPC分类号： C07C209/60 , C07C211/05 , C07C211/08
摘要： The invention relates to a method for producing ethyldimethylamine and triethylamine, comprising the steps of (i) reacting a mixture from diethylamine and dimethylamine with ethylene in the presence of a catalyst from the group of the alkalimetal dimethylamides, alkalimetal diethylamides and alkalimetal hydrides, (ii) removing the catalyst, (iii) separating by distillation the obtained mixture into triethylamine and ethyldimethylamine and optionally diethylamine and dimethylamine, (iv) optionally returning the catalyst and the educt amines to the reaction. The inventive method allows the coupled production of ethyldimethylamine and diethylamine in a simple process.

25. 发明授权

EP1530559B1 VERFAHREN UND VORRICHTUNG ZUR HERSTELLUNG VON AMEISENSAUREN FORMIATEN UND DEREN VERWENDUNG 有权
标题翻译：方法和装置生成酸甲及其用途
公开(公告)号：EP1530559B1
公开(公告)日：2007-11-21
申请号：EP03790832.4
申请日：2003-07-30
申请人： BASF Aktiengesellschaft
发明人： ADAMI, Christoph , KARL, Jörn , HAUK, Alexander , BÖHLING, Ralf , PASTRE, Jörg , LENZ, Robert
IPC分类号： C07C51/09 , C07C53/02 , C07C53/06
CPC分类号： C07C51/412 , C07C53/06
摘要： The invention relates to a method for producing formic acid formates, whereby (a) formic acid methyl ester is partially hydrolysed with water; (b) formic acid methyl ester and methanol are separated by distillation from the reaction mixture obtained in step (a), forming a current containing formic acid and water; (c) the current obtained in step (b), containing the formic acid methyl ester and optionally methanol, is converted into a current containing formate and water, by (i) reaction with a basic compound having a pKa value of the corresponding acid of the corresponding dissociation step of = 3, measured at 25 °C in an aqueous solution, in the presence of water, and (ii) separation by distillation of the methanol; and (d) the current obtained in step (b), containing formic acid and water, and the current obtained in step (c), containing formate and water, are combined to form a mixture containing the formic acid formate and water. The invention also relates to a device for producing said formic acid formates and to the use of the same.

26. 发明公开

EP1682475A1 VERFAHREN ZUR HERSTELLUNG VON N-BUTYRALDEHYD 审中-公开
标题翻译：用于生产正丁醛
公开(公告)号：EP1682475A1
公开(公告)日：2006-07-26
申请号：EP04790844.7
申请日：2004-10-26
申请人： BASF Aktiengesellschaft
发明人： STEINBRENNER, Ulrich , BENISCH, Christoph , BÖHLING, Ralf , FUNKE, Frank
IPC分类号： C07C45/42 , C07C45/51 , C07C47/02
CPC分类号： C07C45/42 , C07C47/02
摘要： The invention relates to a method for producing n-butyraldehyde from 1,3-butadiene comprising the following steps: a) provision of a mixture A containing a 2-butenylamine of general formula (II) and a 3-butenylamine of general formula (III); b) addition of an amine (IV) and an alkali metal to mixture A and in situ production of an alkali metal amide of general formula (V), or addition of an alkali metal amide (Va) to mixture A and isomerisation of 2-butenylamine (II) and 3-butenylamine (III) to 1-butenylamine of general formula (I), whereby the alkali metal amide (V) or (Va) acts as an isomerisation catalyst and a mixture B containing 1-butenylamine (I), 2-butenylamine (II) and 3-butenylamine (III) is obtained; c) addition of butadiene and hydroamination of the butadiene with the amine (IV) to form 2-butenylamine (II) and 3-butenylamine (III), whereby the alkali metal amide (V) or (Va) acts as a hydroamination catalyst and a mixture C containing 1-butenylamine (I), 2-butenylamine (II) and 3-butenylamine (III) is obtained; d) addition of water to mixture C, which permits butyraldehyde and the amine (IV) to be released from the 1-butenylamine and a hydrolysate D containing 2-butenylamine (II), 3-butenylamine (III), amine (IV) and butyraldehyde to be obtained; e) extraction of the butyraldehyde, amine (IV), 2-butenylamine (II) and 3-butenylamine (III) from the hydrolysate D; f) recycling of 2-butenylamine (II), 3-butenylamine (III) and amine (IV) to step a).

27. 发明公开

EP1448510A1 VERFAHREN ZUR HERSTELLUNG VON ETHYLAMIN UND BUTYLAMIN 审中-公开
标题翻译：用于生产乙胺和丁胺
公开(公告)号：EP1448510A1
公开(公告)日：2004-08-25
申请号：EP02787642.4
申请日：2002-11-12
申请人： BASF AKTIENGESELLSCHAFT
发明人： STEINBRENNER, Ulrich , FUNKE, Frank , BÖHLING, Ralf
IPC分类号： C07C209/60 , C07C209/22 , C07C209/26 , C07C211/07 , C07C211/08
CPC分类号： C07C211/07 , C07C211/04 , C07C211/08 , Y02P20/582
摘要： The invention concerns a method for producing ethylamines and butylamines and ethylamine and butylamine mixtures. Said method comprises the following steps: (i) hydroamination of butadiene and ethylene with a monoalkylamine and/or dialkylamine, alkyl may be substituted by ethyl and/or butyl, in the presence of an alkali metal amide as catalyst; (ii) isomerization of the amine obtained during hydroamination (i), optionally after (iia) separating into specific fractions and/or (iib) in hydrogenation conditions and/or (iic) in the presence of ammonia; (iii) separating the product mixture obtained, isolating the desired amine produced and recycling to step (i) the appropriate amine as educt.

28. 发明授权

EP1446377B1 VERFAHREN ZUR HERSTELLUNG VON AMINEN DURCH OLEFINAMINIERUNG IN GEGENWART UNGESÄTTIGTER STICKSTOFFVERBINDUNGEN 有权
标题翻译：用于生产AMINES BY OLEFINAMINIERUNG不饱和中含氮化合物的存在
公开(公告)号：EP1446377B1
公开(公告)日：2005-11-09
申请号：EP02803007.0
申请日：2002-11-11
申请人： BASF Aktiengesellschaft
发明人： BÖHLING, Ralf , STEINBRENNER, Ulrich , FUNKE, Frank , DIER, Reinhard
IPC分类号： C07C209/60
CPC分类号： C07C209/60 , C07C211/05
摘要： The invention relates to a method for producing alkylamines (product amines) by reacting alkenes with amines (educt amines) in the presence of a metal hydride or a metal as a catalyst. Said reaction is carried out in the presence of a co-catalyst, the acidity of said co-catalyst being higher than that of the educt amine. The invention also relates to the use of said co-catalyst in the production of alkylamines (product amines) by reacting alkenes with amines (educt amines) in the presence of a metal hydride or a metal as a catalyst.

29. 发明公开

EP1530560A1 VERFAHREN UND VORRICHTUNG ZUR HERSTELLUNG VON AMEISENSAUREN FORMIATEN UND DEREN VERWENDUNG 审中-公开
公开(公告)号：EP1530560A1
公开(公告)日：2005-05-18
申请号：EP03793657.2
申请日：2003-07-30
申请人： BASF AKTIENGESELLSCHAFT
发明人： ADAMI, Christoph , KARL, Jörn , HAUK, Alexander , BÖHLING, Ralf , PASTRE, Jörg , LENZ, Robert
IPC分类号： C07C51/09 , C07C51/44 , C07C51/43 , C07C53/02 , C07C53/06 , A23K3/03 , A23L1/304 , A61L9/00
CPC分类号： C07C51/43 , C07C51/09 , C07C51/44 , C07C53/02 , C07C53/06
摘要： The invention relates to a method for producing formates according to which: (a) methyl formate is partially hydrolyzed with water; (b) methyl formate and methanol are separated by distillation from the reaction mixture obtained in step (a) while forming a stream containing formic acid and water, and; (c) the stream containing formic acid and water from step (b) is brought together with the corresponding formate while forming a mixture containing the formate and water. The invention also relates to a device for producing these formates and to the use thereof.
摘要翻译：本发明涉及一种生产甲酸盐的方法，其中：（a）甲酸甲酯用水部分水解; （b）通过蒸馏将甲酸甲酯和甲醇从步骤（a）中获得的反应混合物中分离出来，同时形成含有甲酸和水的物流; （c）将来自步骤（b）的含有甲酸和水的物流与相应的甲酸盐合并在一起，同时形成含有甲酸盐和水的混合物。本发明还涉及用于生产这些甲酸盐的装置及其用途。

30. 发明公开

EP1530559A1 VERFAHREN UND VORRICHTUNG ZUR HERSTELLUNG VON AMEISENSAUREN FORMIATEN UND DEREN VERWENDUNG 有权
标题翻译：方法和装置生成酸甲及其用途
公开(公告)号：EP1530559A1
公开(公告)日：2005-05-18
申请号：EP03790832.4
申请日：2003-07-30
申请人： BASF AKTIENGESELLSCHAFT
发明人： ADAMI, Christoph , KARL, Jörn , HAUK, Alexander , BÖHLING, Ralf , PASTRE, Jörg , LENZ, Robert
IPC分类号： C07C51/09 , C07C53/02 , C07C53/06
CPC分类号： C07C51/412 , C07C53/06
摘要： The invention relates to a method for producing formic acid formates, whereby (a) formic acid methyl ester is partially hydrolysed with water; (b) formic acid methyl ester and methanol are separated by distillation from the reaction mixture obtained in step (a), forming a current containing formic acid and water; (c) the current obtained in step (b), containing the formic acid methyl ester and optionally methanol, is converted into a current containing formate and water, by (i) reaction with a basic compound having a pKa value of the corresponding acid of the corresponding dissociation step of = 3, measured at 25 °C in an aqueous solution, in the presence of water, and (ii) separation by distillation of the methanol; and (d) the current obtained in step (b), containing formic acid and water, and the current obtained in step (c), containing formate and water, are combined to form a mixture containing the formic acid formate and water. The invention also relates to a device for producing said formic acid formates and to the use of the same.

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