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21. 发明授权

US06423404B1 Low-transmission transparent layered structure, production method thereof and display device using the layered structure 失效
标题翻译：低透明透明层状结构体及其制造方法以及使用层叠结构的显示装置
公开(公告)号：US06423404B1
公开(公告)日：2002-07-23
申请号：US09484543
申请日：2000-01-18
申请人： Yoshihiro Ohtsuka , Masaya Yukinobu
发明人： Yoshihiro Ohtsuka , Masaya Yukinobu
IPC分类号： B32B516
CPC分类号： H01J29/896 , C03C17/007 , C03C17/34 , C03C17/3411 , C03C2217/45 , C03C2217/475 , C03C2217/476 , C03C2217/485 , H01J29/868 , H01J2229/882 , H01J2229/8913 , Y10T428/256 , Y10T428/257
摘要： A low-transmission transparent layered structure made of a transparent substrate and a low-transmission transparent layer formed on the transparent substrate, wherein the low-transmission transparent layer is constituted of black pigment fine particles having a mean particle size of from 10 to 150 nm and a binder matrix as the main constituents, the black pigment fine particles are composite oxide fine particles of iron, manganese, and copper, or are carbon fine particles and black titanium compound fine particles, the visible light transmittance of the low-transmission transparent layer is from 40 to 90%, and the standard deviation of the transmittance of the low-transmission transparent layer in each wavelength every 5 nm of a visible light wavelength region (380 to 780 nm) is 5% or lower. The low-transmission transparent layer structure has a flat transmission profile, can impart a low reflectance and antistatic and electric field shielding functions, and is used for a display device.
摘要翻译：在透明基板上形成由透明基板和低透明透明层构成的低透明透明层状结构，其中低透明透明层由平均粒径为10〜150nm的黑色颜料微粒构成和粘合剂基质作为主要成分，黑色颜料微粒是铁，锰和铜的复合氧化物细颗粒，或是碳微细颗粒和黑色钛化合物微粒，低透明透明层的可见光透射率为40〜90％，可见光波长区域（380〜780nm）每5nm的各波长的透光性透明层的透射率的标准偏差为5％以下。低透明透明层结构具有平坦的透射轮廓，可以赋予低反射率和抗静电和电场屏蔽功能，并且用于显示装置。

22. 发明授权

US5820843A Raw material for producing powder of indium-tin oxide aciculae and method of producing the raw material, powder of indium-tin oxide aciculae and method of producing the powder, electroconductive paste and light-transmitting electroconductive film 失效
标题翻译：氧化铟锡粉末的制造原料及其制造方法，氧化铟锡粉末及其制造方法，导电性糊料和透光性导电膜
公开(公告)号：US5820843A
公开(公告)日：1998-10-13
申请号：US662145
申请日：1996-06-12
申请人： Masaya Yukinobu , Morikazu Kojima , Mitsuo Usuba
发明人： Masaya Yukinobu , Morikazu Kojima , Mitsuo Usuba
IPC分类号： C01G15/00 , C01G19/00 , C09D5/24 , H01B1/08 , H01B1/14 , H05K1/09
CPC分类号： C01G15/00 , C01G19/00 , C09D5/24 , H01B1/08 , H01B1/14 , C01P2002/10 , C01P2004/10 , H05K1/092
摘要： Disclosed are a powder of indium-tin oxide aciculae suitable as an electroconductive filler for an electroconductive ink to be used for forming a transparent electroconductive film, a method for producing a raw material to be used for producing the powder of indium-tin oxide aciculae, which has a major diameter of 5 .mu.m or more and a ratio of the major diameter to the minor diameter of 5 or more, an electroconductive paste capable of forming a light-transmitting electroconductive film having sufficient electroconductivity and light transmittance by printing, such as screen-printing, followed by high-temperature baking, and a light-transmitting electroconductive film to be formed from the paste. The raw material is produced by heating and concentrating an aqueous solution containing indium ions and nitrato ions to form a high-viscosity slurry followed by separating a powder of aciculae from the slurry. By calcining the raw material, a powder of indium-tin oxide aciculae is produced.
摘要翻译：公开了适合作为用于形成透明导电膜的导电油墨的导电填料的氧化铟锡粉末，用于生产氧化铟锡粉末的原料的制造方法，其直径为5μm以上，长径比与小直径的比例为5以上，能够形成具有足够的导电性的透光导电膜和通过印刷而具有透光性的导电浆，例如丝网印刷，然后进行高温烘烤，以及由该糊状物形成的透光导电膜。通过加热浓缩含有铟离子和硝酸根离子的水溶液来形成高粘度浆料，然后从浆料中分离出粉末的粉末来制备原料。通过煅烧原料，生成氧化铟锡粉末。

23. 发明申请

US20130101867A1 METHOD OF MANUFACTURING METAL OXIDE FILM, METAL OXIDE FILM, ELEMENT USING THE METAL OXIDE FILM, SUBSTRATE WITH METAL OXIDE FILM, AND DEVICE USING THE SUBSTRATE WITH METAL OXIDE FILM 有权
标题翻译：制造金属氧化物膜，金属氧化物膜，使用金属氧化物膜的元件，具有金属氧化物膜的衬底的方法，以及使用具有金属氧化物膜的衬底的器件
公开(公告)号：US20130101867A1
公开(公告)日：2013-04-25
申请号：US13261535
申请日：2011-06-08
申请人： Masaya Yukinobu , Yuki Murayama , Takahito Nagano , Yoshihiro Otsuka
发明人： Masaya Yukinobu , Yuki Murayama , Takahito Nagano , Yoshihiro Otsuka
IPC分类号： C01G41/02 , C01F17/00 , C01F7/02 , C01G39/02 , C01G23/047 , C01G33/00 , C01G31/02 , C01G27/02 , C01G25/02 , B05D3/00 , C01G35/00
CPC分类号： C01G41/02 , B05D3/007 , C01F7/02 , C01F17/0043 , C01G23/047 , C01G25/02 , C01G27/02 , C01G31/02 , C01G33/00 , C01G35/00 , C01G39/02 , C03C17/006 , C03C2217/212 , C03C2217/214 , C03C2217/218 , C03C2217/219 , C03C2217/22 , C03C2217/228 , C03C2217/42 , C03C2218/116 , C03C2218/119 , H01L21/02565 , H01L21/02628
摘要： Provided is a method of manufacturing a metal oxide film to be formed through the following processes: a coating process of forming a coating film on a substrate by using a coating liquid for forming metal oxide film containing any of various organometallic compounds; a drying process of making the coating film into a dried coating film; and a heating process of forming an inorganic film from the dried coating film under an oxygen-containing atmosphere having a dew-point temperature equal to or lower than −10° C.
摘要翻译：提供一种通过以下方法制造金属氧化物膜的方法：通过使用用于形成含有各种有机金属化合物的金属氧化物膜的涂布液在基板上形成涂膜的涂布方法; 使涂膜成为干燥涂膜的干燥工序; 以及在露点温度等于或低于-10℃的含氧气氛下从干燥的涂膜形成无机膜的加热方法。

24. 发明授权

US08388871B2 Translucent conductive film forming coating liquid, translucent conductive film, and dispersive type electroluminescent device 失效
标题翻译：半透明导电膜形成涂布液，半透明导电膜和分散型电致发光器件
公开(公告)号：US08388871B2
公开(公告)日：2013-03-05
申请号：US11783107
申请日：2007-04-05
申请人： Kenji Kato , Masaya Yukinobu
发明人： Kenji Kato , Masaya Yukinobu
IPC分类号： H01B1/12
CPC分类号： H01B1/22 , H01B1/08 , Y10T428/12451 , Y10T428/256 , Y10T428/257 , Y10T428/2982
摘要： A translucent conductive film-forming coating liquid that can form a translucent conductive film having excellent translucency and conductivity together with organic solvent resistance includes conductive oxide acicular powder dispersed in a solvent containing a binder resin, the glass transition point (Tg) of the binder resin being 120° C. or more.
摘要翻译：可以形成具有优异的半透明性和导电性的半透明导电膜以及有机耐溶剂性的半透明导电膜形成涂布液包括分散在含有粘合剂树脂的溶剂中的导电氧化物针状粉末，粘合剂树脂的玻璃化转变点（Tg）为120℃以上。

25. 发明授权

US08269416B2 Film with transparent conductive layer, flexible functional element and flexible dispersion-type electroluminescent element, and method for producing the same and electronic device by the use thereof 有权
标题翻译：具有透明导电层，柔性功能元件和柔性分散型电致发光元件的薄膜及其制造方法及其使用的电子器件
公开(公告)号：US08269416B2
公开(公告)日：2012-09-18
申请号：US11992933
申请日：2006-06-26
申请人： Yuki Murayama , Masaya Yukinobu
发明人： Yuki Murayama , Masaya Yukinobu
IPC分类号： H01J1/62 , H05K1/00 , B32B29/04 , B29C63/02
CPC分类号： H05B33/28 , H01L51/5206 , H01L2227/326 , H01L2251/5338
摘要： A compressed multilayered film for a flexible functional element includes a base film, a transparent conductive layer coated on one side of the base film, and a support layer with a low adhesion layer liner on an opposite side of the base film. The support layer is separable from the base film. The base film has a thickness of 3 to 25 μm, and the transparent conductive layer is composed mainly of conductive oxide microparticles and a binder matrix. The multilayered film is compressed to increase the filling density of the conductive microparticles in the transparent conductive layer.
摘要翻译：用于柔性功能元件的压缩多层膜包括基膜，涂覆在基膜的一侧上的透明导电层和在基膜的相对侧上具有低粘附层衬垫的支撑层。支撑层可与基膜分离。基膜的厚度为3〜25μm，透明导电层主要由导电性氧化物微粒和粘合剂基体构成。多层膜被压缩以增加透明导电层中导电微粒的填充密度。

26. 发明授权

US08040042B2 Transparent electroconductive layered structure, organic electroluminescent device using the same layered structure, method for producing the same layered structure, and method for producing the same device 有权
标题翻译：透明导电层状结构体，使用相同分层结构的有机电致发光元件，制造相同分层结构的方法及其制造方法
公开(公告)号：US08040042B2
公开(公告)日：2011-10-18
申请号：US10570801
申请日：2004-09-08
申请人： Masaya Yukinobu
发明人： Masaya Yukinobu
IPC分类号： H01J1/62 , H01J63/04
CPC分类号： H01L51/442 , H01L51/5088 , H01L51/5206 , H01L51/5212 , H01L51/5259 , H01L2227/326 , Y02E10/549 , Y02P70/521
摘要： Disclosed is an organic EL device comprising a transparent electroconductive anode layer which is formed by a simple coating method that enables film formation at a low temperature, which organic EL device is free from electrical short circuit between the transparent electroconductive anode layer and a cathode layer. Also disclosed is a transparent electroconductive layered structure used for manufacturing such an organic EL device. The transparent electroconductive layered structure is characterized by comprising a flat and smooth substrate, a transparent electroconductive anode layer which is formed on the substrate by a coating method and mainly composed of conductive particles, and a transparent substrate joined to the transparent electroconductive anode layer via an adhesive layer. The transparent electroconductive layered structure is also characterized in that the flat and smooth substrate can be separated from the transparent electroconductive anode layer.
摘要翻译：公开了一种有机EL器件，其包括通过简单的涂覆方法形成的透明导电阳极层，其能够在低温下成膜，该有机EL器件在透明导电阳极层和阴极层之间没有电短路。还公开了用于制造这种有机EL器件的透明导电层状结构。透明导电层状结构的特征在于包括平坦且光滑的基板，通过涂覆方法形成在主要由导电颗粒构成的基板上的透明导电阳极层和透明基板，该透明基板经由透明导电阳极层粘合剂层。透明导电层状结构的特征还在于，平坦且光滑的衬底可以与透明导电阳极层分离。

27. 发明申请

US20110229737A1 METHOD FOR PRODUCING TRANSPARENT CONDUCTIVE FILM, TRANSPARENT CONDUCTIVE FILM, TRANSPARENT CONDUCTIVE SUBSTRATE AND DEVICE COMPRISING THE SAME 有权
标题翻译：透明导电薄膜，透明导电薄膜，透明导电基板及其装置的制造方法
公开(公告)号：US20110229737A1
公开(公告)日：2011-09-22
申请号：US12998767
申请日：2009-12-01
申请人： Masaya Yukinobu , Yoshihiro Otsuka
发明人： Masaya Yukinobu , Yoshihiro Otsuka
IPC分类号： B32B9/00 , B05D5/12 , B05D3/02 , H01B1/02
CPC分类号： H01L31/1884 , C23C18/1216 , C23C18/1275 , C23C18/1279 , C23C18/1283 , G02F1/13439 , H01L33/42 , H01L2924/0002 , Y02E10/50 , H01L2924/00
摘要： Provided is a method for producing a transparent conductive film which is formed via a coating step, a drying step and a baking step, wherein the baking step is characterized in that the dried coating film containing the organic metal compound as the main component is baked by being heated to a baking temperature or higher, at which at least the inorganic component is crystallized, under an oxygen-containing atmosphere having a dewpoint of −10° C. or lower, whereby an organic component contained in the dried coating film is removed therefrom by a heat decomposition, a combustion or the combination thereof to thereby form a conductive oxide microparticle layer densely filled with conductive oxide microparticles containing the metal oxide as a main component.
摘要翻译：提供一种通过涂布步骤，干燥步骤和烘烤步骤形成的透明导电膜的制造方法，其特征在于，将含有有机金属化合物作为主要成分的干燥涂膜以在露点为-10℃以下的含氧气氛下，加热至至少无机成分结晶的烧成温度以上，由此除去干燥后的涂膜中含有的有机成分通过热分解，燃烧或其组合，从而形成密封地填充有以金属氧化物为主要成分的导电性氧化物微粒的导电性氧化物微粒层。

28. 发明申请

US20090302756A1 Film with Transparent Conductive Layer, Flexible Functional Element and Flexible Dispersion-Type Electroluminescent Element, and Method for Producing the Same and Electronic Device by the Use Thereof 有权
标题翻译：具有透明导电层的膜，柔性功能元件和柔性分散型电致发光元件及其制造方法及其使用的电子器件
公开(公告)号：US20090302756A1
公开(公告)日：2009-12-10
申请号：US11992933
申请日：2006-06-26
申请人： Yuki Murayama , Masaya Yukinobu
发明人： Yuki Murayama , Masaya Yukinobu
IPC分类号： H01J1/62 , H05K1/00 , B32B29/04 , B29C63/02
CPC分类号： H05B33/28 , H01L51/5206 , H01L2227/326 , H01L2251/5338
摘要： An object of the present invention is to provide various flexible functional elements such as a film with a transparent conductive layer which is excellent in flexibility, more specifically, a film with the transparent conductive layer formed on a thin and flexible base film, and a flexible functional element selected from any of a liquid crystal display element, an organic EL element, and an electronic paper element as well as a flexible dispersion-type EL element, using the film with the transparent conductive layer, and a method for producing the same.There is provided a film with a transparent conductive layer, the layer being formed on a base film by a coating method, characterized in that the base film side of the film with the transparent conductive layer is lined with a support film having a low adhesive layer separable at an interface with the base film, the base film having a thickness of 3 to 25 μm, and that the transparent conductive layer is composed mainly of conductive oxide microparticles and a binder matrix, and a compression treatment is given thereto.
摘要翻译：本发明的目的是提供各种柔性功能元件，例如具有柔性优异的透明导电层的膜，更具体地说，具有形成在薄且柔性基膜上的透明导电层的膜，以及柔性从液晶显示元件，有机EL元件和电子纸元件中选择的功能元件以及使用具有透明导电层的膜的柔性分散型EL元件及其制造方法。提供具有透明导电层的膜，该层通过涂布方法形成在基膜上，其特征在于，具有透明导电层的膜的基膜侧衬有具有低粘合层的支撑膜在与基膜的界面处可分离，基膜的厚度为3〜25μm，透明导电层主要由导电性氧化物微粒和粘合剂基质构成，并进行压缩处理。

29. 发明申请

US20090256118A1 Fine Silver Particle Colloidal Dispersion, Coating Liquid for Silver Film Formation, Processes for Producing These, and Silver Film 有权
标题翻译：细银粒子胶体分散体，银膜形成用涂布液，制造方法和银膜
公开(公告)号：US20090256118A1
公开(公告)日：2009-10-15
申请号：US12085185
申请日：2005-12-08
申请人： Hiroyuki Tanaka , Kenji Kato , Masaya Yukinobu
发明人： Hiroyuki Tanaka , Kenji Kato , Masaya Yukinobu
IPC分类号： H01B1/22 , C09D1/00
CPC分类号： B22F9/24 , B01J13/0043 , B22F1/0022 , B22F2998/10 , B82Y30/00 , B22F1/0096
摘要： A process for producing a fine silver particle colloidal dispersion the fine silver particles of which have a larger average particle diameter than those in the conventional Carey-Lea process and also which has superior dispersion stability. An aqueous silver nitrate solution is allowed to react with a mixed solution of an aqueous iron(II) sulfate solution and an aqueous sodium citrate solution, and the resultant reaction fluid containing an agglomerate of fine silver particles is left at 0 to 100° C. to obtain an agglomerate of fine silver particles having grown into granular particles. Next, this agglomerate of fine silver particles having grown into granular particles is filtered, and, to the resultant cake of the agglomerate of fine silver particles, pure water is added to obtain a fine silver particle colloidal dispersion having an average particle diameter of 20 to 200 nm. This fine silver particle colloidal dispersion is concentrated and washed, further followed by addition of an organic solvent containing dimethyl sulfoxide, to obtain a coating liquid for silver film formation.
摘要翻译：一种制备细银粒子胶体分散体的方法，其细银粒子具有比常规Carey-Lea方法更大的平均粒径，并且其具有优异的分散稳定性。使硝酸银水溶液与硫酸铁水溶液和柠檬酸钠水溶液的混合溶液反应，将含有细银粒子附聚物的反应液保持在0〜100℃。以获得生长成粒状颗粒的细银粒子的附聚物。接下来，将生长成粒状颗粒的细银粒子附聚物过滤，向所得到的细银粒子附聚物的滤饼中加入纯水，得到平均粒径为20〜 200nm。将该细银粒子胶体分散体浓缩并洗涤，然后加入含有二甲基亚砜的有机溶剂，得到银膜形成用涂布液。

30. 发明申请

US20090184637A1 Dispersion-Type Electroluminescent Element and Method for Manufacturing the Same 失效
标题翻译：分散型电致发光元件及其制造方法
公开(公告)号：US20090184637A1
公开(公告)日：2009-07-23
申请号：US12308839
申请日：2006-06-26
申请人： Masaya Yukinobu , Yuki Murayama , Yasuo Tsukui
发明人： Masaya Yukinobu , Yuki Murayama , Yasuo Tsukui
IPC分类号： H01J1/62 , H01J9/00
CPC分类号： H05B33/10 , H05B33/22
摘要： A dispersion-type EL element is a dispersion-type electroluminescent element with at least a transparent coating layer, a transparent conductive layer, a phosphor layer, a dielectric layer and a rear electrode layer sequentially formed on a base film surface. The transparent coating layer can be peeled off the surface of the base film. The transparent conductive layer is formed by applying a coating liquid composed mainly of conductive oxide particles and a binder on a surface of the transparent coating layer, applying compression processing to the applied layer and then curing the compressed layer.
摘要翻译：分散型EL元件是在基膜表面上依次形成至少具有透明涂层，透明导电层，荧光体层，电介质层和后电极层的分散型电致发光元件。透明涂层可以从基膜的表面剥离。透明导电层通过在透明涂层的表面上涂覆主要由导电氧化物颗粒和粘合剂组成的涂布液，对涂布层进行压缩处理，然后固化压缩层而形成。

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