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21. 发明申请

US20140155659A1 PROCESS FOR THE MANUFACTURE OF 2-CHLORO-3,3,3-TRIFLUOROPROPENE (HCFO 1233xf) BY LIQUID PHASE FLUORINATION OF PENTACHLOROPROPANE 审中-公开
标题翻译：通过液相色谱法制备2-氯代-3,3,3-三氟乙烯（HCFO 1233xf）的方法
公开(公告)号：US20140155659A1
公开(公告)日：2014-06-05
申请号：US13885470
申请日：2010-11-15
申请人： Laurent Wendlinger , Anne Pigamo , Phillipe Bonnet
发明人： Laurent Wendlinger , Anne Pigamo , Phillipe Bonnet
IPC分类号： C07C17/20
CPC分类号： C07C17/206 , C07C17/25 , C07C17/383 , C07C21/18
摘要： Process of catalytic fluorination in liquid phase of product 1,1,1,2,3-pentachloropropane or/and 1,1,2,2,3-pentachloropropane into product 2-chloro-3,3,3-trifluoropropene in presence of a catalyst.
摘要翻译：在产物1,1,1,2,3-五氯丙烷或/和1,1,2,2,3-五氯丙烷的液相中催化氟化的方法在产物2-氯-3,3,3-三氟丙烯的存在下，催化剂

22. 发明授权

US08680346B2 Process for the preparation of trifluorinated and tetrafluorinated compounds 有权
标题翻译：制备三氟化四氟化合物的方法
公开(公告)号：US08680346B2
公开(公告)日：2014-03-25
申请号：US13063079
申请日：2009-09-11
申请人： Anne Pigamo , Michel Devic , Laurent Wendlinger
发明人： Anne Pigamo , Michel Devic , Laurent Wendlinger
IPC分类号： C07C17/00
CPC分类号： C07C21/18 , C07C17/04 , C07C17/087 , C07C17/206 , C07C17/25 , C07C51/12 , C07C19/10
摘要： The subject of the invention is a process for the preparation of 2,3-dichloro-1,1,1-trifluoropropane by chlorination of 3,3,3-trifluoropropene at a pressure greater than 2 bar. Application in the synthesis of 1234yf.
摘要翻译：本发明的主题是通过在大于2巴的压力下氯化3,3,3-三氟丙烯来制备2,3-二氯-1,1,1-三氟丙烷的方法。应用于1234yf的合成。

23. 发明申请

US20140039228A1 CATALYTIC GAS PHASE FLUORINATION 有权
标题翻译：催化气相氟化
公开(公告)号：US20140039228A1
公开(公告)日：2014-02-06
申请号：US13980665
申请日：2011-01-21
申请人： Anne Pigamo , Nicolas Doucet , Laurent Wendlinger
发明人： Anne Pigamo , Nicolas Doucet , Laurent Wendlinger
IPC分类号： C07C17/20
CPC分类号： C07C17/206 , B01J21/04 , B01J21/20 , B01J23/06 , B01J23/34 , B01J23/75 , B01J23/755 , B01J23/86 , B01J23/864 , B01J23/866 , B01J23/90 , B01J23/94 , B01J27/125 , B01J37/0201 , B01J37/14 , B01J37/26 , B01J38/12 , C07C17/25 , Y02P20/584 , C07C21/18 , C07C19/08
摘要： The present invention relates to a fluorination process, comprising: an activation stage comprising contacting a fluorination catalyst with an oxidizing agent-containing gas flow for at least one hour; and at least one reaction stage comprising reacting a chlorinated compound with hydrogen fluoride in gas phase in the presence of the fluorination catalyst, so as to produce a fluorinated compound.
摘要翻译：本发明涉及一种氟化方法，包括：活化阶段，包括使含氟化催化剂与含氧化剂气流接触至少1小时; 以及至少一个反应阶段，包括在氟化催化剂存在下，使气相中的氯化化合物与氟化氢反应，从而制备氟化物。

24. 发明申请

US20130267740A1 PROCESS FOR THE PREPARATION OF 2,3,3,3 TETRAFLUOROPROPENE 有权
标题翻译：制备2,3,3,3-四氯丙烯的方法
公开(公告)号：US20130267740A1
公开(公告)日：2013-10-10
申请号：US13879435
申请日：2010-10-22
申请人： Laurent Wendlinger , Philippe Bonnet , Anne Pigamo , Nicolas Doucet
发明人： Laurent Wendlinger , Philippe Bonnet , Anne Pigamo , Nicolas Doucet
IPC分类号： C07C17/20
CPC分类号： C07C17/25 , C07C17/206 , C07C17/383 , C07C17/42 , C07C21/18
摘要： The present invention provides a process for preparing 2,3,3,3-tetrafluoropropene, comprising the following steps: (a) catalytic reaction of 1,1,1,2,3-pentachloropropane and/or 1,1,2,2,3-pentachloropropane with HF into product 2-chloro-3,3,3-trifluoropropene; (b) catalytic reaction of the thus-obtained 2-chloro-3,3,3-trifluoropropene into 2,3,3,3-tetrafluoropropene.
摘要翻译：本发明提供一种制备2,3,3,3-四氟丙烯的方法，包括以下步骤：（a）1,1,1,2,3-五氯丙烷和/或1,1,2,2 与HF的3-五氯丙烷反应制成2-氯-3,3,3-三氟丙烯; （b）将由此得到的2-氯-3,3,3-三氟丙烯催化反应成2,3,3,3-四氟丙烯。

25. 发明授权

US08536386B2 Process for the preparation of fluoroolefin compounds 有权
标题翻译：氟烯烃化合物的制备方法
公开(公告)号：US08536386B2
公开(公告)日：2013-09-17
申请号：US12602705
申请日：2009-08-18
申请人： Anne Pigamo , Michel Devic , Laurent Wendlinger
发明人： Anne Pigamo , Michel Devic , Laurent Wendlinger
IPC分类号： C07C17/00
CPC分类号： C07C17/25 , C07C21/18
摘要： A subject-matter of the invention is a process for the preparation of fluoroolefin compounds. It relates more particularly to a process for the manufacture of a compound of formula (I) CF3—CF═CHX in which X represents a hydrogen or fluorine atom, comprising at least one stage of dehydrofluorination of a compound of formula (II) CF3—CHF—CHFX during which the compound of formula (II) is brought into contact with a mixture composed of water and of potassium hydroxide in which the potassium hydroxide is present in an amount of between 58 and 86% by weight.
摘要翻译：本发明的主题是制备氟烯烃化合物的方法。更具体地涉及制备式（I）化合物的方法，其中X表示氢或氟原子，包括式（II）化合物的至少一个脱氟化氢阶段CF 3 - CHF-CHFX，其中使式（II）化合物与由氢和氢氧化钾组成的混合物接触，其中氢氧化钾的存在量为58至86重量％。

26. 发明申请

US20110190554A1 PROCESS FOR THE PREPARATION OF FLUORINATED COMPOUNDS 有权
标题翻译：制备氟化合物的方法
公开(公告)号：US20110190554A1
公开(公告)日：2011-08-04
申请号：US12602707
申请日：2009-08-19
申请人： Anne Pigamo , Michel Devic , Laurent Wendlinger
发明人： Anne Pigamo , Michel Devic , Laurent Wendlinger
IPC分类号： C07C17/23
CPC分类号： C07C17/25 , C07C17/354 , C07C21/18 , Y02P20/582 , C07C19/08
摘要： A subject-matter of the invention is a process for the preparation of 2,3,3,3-tetrafluoro-1-propene which comprises the following stages: (i) hydrogenation of hexafluoropropylene to give 1,1,1,2,3,3-hexafluoropropane; (ii) dehydrofluorination of the 1,1,1,2,3,3-hexafluoropropane obtained in the preceding stage to give 1,2,3,3,3-pentafluoro-1-propene; (iii) hydrogenation of the 1,2,3,3,3-pentafluoro-1-propene obtained in the preceding stage to give 1,1,1,2,3-pentafluoropropane; and (iv) dehydrofluorination of the 1,1,1,2,3-pentafluoropropane obtained in the preceding stage to give 2,3,3,3-tetrafluoro-1-propene. Stages (ii) and (iv) are carried out using a water and potassium hydroxide mixture with the potassium hydroxide representing between 58 and 86% by weight of the mixture and at a temperature of between 110 and 180° C.
摘要翻译：本发明的主题是制备2,3,3,3-四氟-1-丙烯的方法，其包括以下步骤：（i）六氟丙烯的氢化，得到1,1,1,2,3 ，3-六氟丙烷; （ii）前段得到的1,1,1,2,3,3-六氟丙烷的脱氟化氢，得到1,2,3,3,3-五氟-1-丙烯; （iii）在前一阶段获得的1,2,3,3,3-五氟-1-丙烯的氢化，得到1,1,1,2,3-五氟丙烷; 和（iv）前一阶段获得的1,1,1,2,3-五氟丙烷的脱氟化氢，得到2,3,3,3-四氟-1-丙烯。阶段（ii）和（iv）使用氢氧化钾与氢氧化钾混合物的比例为混合物的58-86％（重量）和在110和180℃之间的温度下进行。

27. 发明授权

US09340473B2 Catalytic gas phase fluorination 有权
标题翻译：催化气相氟化
公开(公告)号：US09340473B2
公开(公告)日：2016-05-17
申请号：US13980665
申请日：2011-01-21
申请人： Anne Pigamo , Nicolas Doucet , Laurent Wendlinger
发明人： Anne Pigamo , Nicolas Doucet , Laurent Wendlinger
IPC分类号： C07C17/25 , C07C17/20 , B01J23/90 , B01J23/92 , B01J23/94 , B01J23/26 , B01J23/78 , B01J23/84 , B01J23/882 , B01J23/883 , B01J23/843 , B01J23/847 , B01J23/86 , B01J37/14 , B01J37/26 , B01J38/12 , B01J27/125 , B01J37/02
CPC分类号： C07C17/206 , B01J21/04 , B01J21/20 , B01J23/06 , B01J23/34 , B01J23/75 , B01J23/755 , B01J23/86 , B01J23/864 , B01J23/866 , B01J23/90 , B01J23/94 , B01J27/125 , B01J37/0201 , B01J37/14 , B01J37/26 , B01J38/12 , C07C17/25 , Y02P20/584 , C07C21/18 , C07C19/08
摘要： The present invention relates to a fluorination process, comprising: an activation stage comprising contacting a fluorination catalyst with an oxidizing agent-containing gas flow for at least one hour; and at least one reaction stage comprising reacting a chlorinated compound with hydrogen fluoride in gas phase in the presence of the fluorination catalyst, so as to produce a fluorinated compound.
摘要翻译：本发明涉及一种氟化方法，包括：活化阶段，包括使含氟化催化剂与含氧化剂气流接触至少1小时; 以及至少一个反应阶段，包括在氟化催化剂存在下，使气相中的氯化化合物与氟化氢反应，从而制备氟化物。

28. 发明授权

US09302961B2 Catalytic gas phase fluorination 有权
标题翻译：催化气相氟化
公开(公告)号：US09302961B2
公开(公告)日：2016-04-05
申请号：US13980672
申请日：2011-01-21
申请人： Anne Pigamo , Laurent Wendlinger , Nicolas Doucet
发明人： Anne Pigamo , Laurent Wendlinger , Nicolas Doucet
IPC分类号： C07C17/25 , C07C17/20 , B01J23/90 , B01J23/92 , B01J23/94 , B01J23/26 , B01J23/78 , B01J23/84 , B01J23/882 , B01J23/883 , B01J23/843 , B01J23/847 , B01J23/86 , B01J37/14 , B01J37/26 , B01J38/12 , B01J27/125
CPC分类号： C07C17/206 , B01J23/866 , B01J23/90 , B01J23/92 , B01J23/94 , B01J27/125 , B01J37/14 , B01J37/26 , B01J38/12 , C07C17/20 , C07C17/25 , Y02P20/584 , C07C21/18
摘要： The invention relates to a fluorination process, alternately comprising reaction stages and regeneration stages, wherein the reaction stages comprise reacting a chlorinated compound with hydrogen fluoride in gas phase in the presence of a fluorination catalyst to produce a fluorinated compound, and the regeneration stages comprise contacting the fluorination catalyst with an oxidizing agent-containing gas flow.
摘要翻译：本发明涉及氟化方法，交替包括反应阶段和再生阶段，其中反应步骤包括在氟化催化剂存在下使气相中的氯化化合物与氟化氢反应以产生氟化化合物，并且再生阶段包括接触含有含氧化剂气体的氟化催化剂。

29. 发明授权

US09255047B2 Process for the preparation of fluorinated compounds 有权
标题翻译：氟化合物的制备方法
公开(公告)号：US09255047B2
公开(公告)日：2016-02-09
申请号：US12602707
申请日：2009-08-19
申请人： Anne Pigamo , Michel Devic , Laurent Wendlinger
发明人： Anne Pigamo , Michel Devic , Laurent Wendlinger
IPC分类号： C07C17/354 , C07C17/25 , C07C21/18
CPC分类号： C07C17/25 , C07C17/354 , C07C21/18 , Y02P20/582 , C07C19/08
摘要： A subject-matter of the invention is a process for the preparation of 2,3,3,3-tetrafluoro-1-propene which comprises the following stages: (i) hydrogenation of hexafluoropropylene to give 1,1,1,2,3,3-hexafluoropropane; (ii) dehydrofluorination of the 1,1,1,2,3,3-hexafluoropropane obtained in the preceding stage to give 1,2,3,3,3-pentafluoro-1-propene; (iii) hydrogenation of the 1,2,3,3,3-pentafluoro-1-propene obtained in the preceding stage to give 1,1,1,2,3-pentafluoropropane; and (iv) dehydrofluorination of the 1,1,1,2,3-pentafluoropropane obtained in the preceding stage to give 2,3,3,3-tetrafluoro-1-propene. Stages (ii) and (iv) are carried out using a water and potassium hydroxide mixture with the potassium hydroxide representing between 58 and 86% by weight of the mixture and at a temperature of between 110 and 180° C.
摘要翻译：本发明的主题是制备2,3,3,3-四氟-1-丙烯的方法，其包括以下步骤：（i）六氟丙烯的氢化，得到1,1,1,2,3 ，3-六氟丙烷; （ii）前段得到的1,1,1,2,3,3-六氟丙烷的脱氟化氢，得到1,2,3,3,3-五氟-1-丙烯; （iii）在前一阶段获得的1,2,3,3,3-五氟-1-丙烯的氢化，得到1,1,1,2,3-五氟丙烷; 和（iv）前一阶段获得的1,1,1,2,3-五氟丙烷的脱氟化氢，得到2,3,3,3-四氟-1-丙烯。阶段（ii）和（iv）使用氢氧化钾与氢氧化钾混合物进行，其中氢氧化钾占混合物重量的58-86％，在110-180℃的温度下进行。

30. 发明授权

US08252964B2 Process for the purification of 2,3,3,3-tetrafluoro-1-propene (HFO-1234yf) 有权
标题翻译：纯化2,3,3,3-四氟-1-丙烯（HFO-1234yf）的方法
公开(公告)号：US08252964B2
公开(公告)日：2012-08-28
申请号：US13001663
申请日：2009-06-08
申请人： Michel Devic , Anne Pigamo , Laurent Wendlinger
发明人： Michel Devic , Anne Pigamo , Laurent Wendlinger
IPC分类号： C07C17/38
CPC分类号： C07C17/389 , C07C21/18
摘要： The subject of the invention is a process for the purification of 2,3,3,3-tetrafluoro-1-propene (HFO-1234yf). More particularly, it relates to a purification process in which 2,3,3,3-tetrafluoro-1-propene, comprising impurities based on halogen compounds, is brought into contact with an adsorbent, preferably molecular sieves and advantageously molecular sieves having a pore opening with an average diameter between 5 and 11 Å, preferably between 5 and 9 Å.
摘要翻译：本发明的主题是用于纯化2,3,3,3-四氟-1-丙烯（HFO-1234yf）的方法。更具体地说，本发明涉及一种纯化方法，其中将包含基于卤素化合物的杂质的2,3,3,3-四氟-1-丙烯与吸附剂，优选分子筛和有利的分子筛接触，所述分子筛具有孔平均直径在5和11埃之间，优选在5和9之间。

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