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21. 发明公开

EP1899292A1 IMPROVED PROCESS FOR SYNTHESIZING ALKYLATED ARYLAMINES 审中-公开
标题翻译：改进方法合成烷基化的芳基胺
公开(公告)号：EP1899292A1
公开(公告)日：2008-03-19
申请号：EP06771345.3
申请日：2006-05-30
申请人： ALBEMARLE CORPORATION
发明人： ELNAGAR, Hassan, Y. , GATTO, Vince, J. , BOONE, James, E. , LO, Joyce , COURY, Joseph, E., Ph., D. , SAKAHARA, Brett
IPC分类号： C07C209/68 , B01J31/14 , B01J27/10 , B01J35/00
CPC分类号： B01J31/14 , B01J31/122 , B01J37/24 , C07C209/68 , C07C211/55
摘要： An improved process and novel catalyst system for alkylating arylamines generally comprising the combination of an arylamine and an alkylating agent in the presence of a trialkyl aluminum compound and a hydrogen halide. The improved process and new catalyst system allows for higher total conversion of the arylamine feedstock without sacrificing substitution product selectivity and also allows for the reaction of recycled alkylene feedstock.

22. 发明公开

EP1250327A2 PROCESS FOR PRODUCING N-HALOGENATED ORGANIC COMPOUNDS 无效
标题翻译：用于生产有机n卤代化合物
公开(公告)号：EP1250327A2
公开(公告)日：2002-10-23
申请号：EP01906581.2
申请日：2001-01-17
申请人： ALBEMARLE CORPORATION
发明人： ELNAGAR, Hassan, Y. , PETERS, Bruce, C. , SPIELMAN, Edgar, E., Jr. , THOMAS, Dustin, H.
IPC分类号： C07D233/82 , C07D251/36
CPC分类号： C07D233/82
摘要： The process enables highly effective N-halogenation of a compound having one or more halogenatable amido or imido functional groups in the molecule. The process involves, for example, concurrently feeding into a reactor (i) water, inorganic base, and the compound to be N-halogenated, e.g., a hydantoin, and a feed of (ii) a brominating agent and/or a chlorinating agent. The proportions of these feeds are such that the pH is kept within the range of ca. 5.5-8.5 (preferably 6.5-8.5, and most preferably 6.8-7.2) and one or more of the amido or imido nitrogen atoms is substituted by a bromine or chlorine atom. A feature of the processs is that it can be conducted at elevated temperatures as high as about 90 °C without appreciable thermal decomposition of reactants or product. The resultant product continuously precipitates in high yield and purity. Moreover, products can be produced that are very pale yellow to almost pure white in appearance. Further, the process has been found capable of producing 1,3-dibromo-5,5-dimethylhydantoin with far larger particle sizes than previously produced on a commercial basis.

23. 发明授权

EP0822927B1 A PROCESS FOR THE PREPARATION OF TETRABROMOBISPHENOL-A 失效
标题翻译：用于生产四溴双酚A
公开(公告)号：EP0822927B1
公开(公告)日：2002-08-28
申请号：EP96916430.0
申请日：1996-04-18
申请人： ALBEMARLE CORPORATION
发明人： McKINNIE, Bonnie, G. , HOLUB, Richard, A. , ELNAGAR, Hassan, Y.
IPC分类号： C07C37/62 , C07C39/367
CPC分类号： C07C37/62 , C07C39/367
摘要： This invention relates to a process for the production of tetrabromobisphenol-A by the bromination of bisphenol-A, which process features the addition of bisphenol-A to a reaction mass containing unreacted Br2 and 30 to 85 wt.% water and an alcohol solvent, the reaction mass being at a relatively high temperature.

24. 发明公开

EP1086069A1 A PROCESS FOR THE PREPARATION OF TETRABROMOBISPHENOL-A 有权
标题翻译：一种制备四溴双酚-A的方法
公开(公告)号：EP1086069A1
公开(公告)日：2001-03-28
申请号：EP99922906.5
申请日：1999-05-10
申请人： ALBEMARLE CORPORATION
发明人： HOLUB, Richard, A. , ALFERI, Steven, R. , McKINNIE, Bonnie, G. , ELNAGAR, Hassan, Y.
IPC分类号： C07C39/367 , C07C37/62
CPC分类号： C07C37/62 , C07C39/367
摘要： This invention relates to a process for the production of tetrabromobisphenol-A by the bromination of bisphenol-A, which process features: (a) feeding to a reaction mass (i) bisphenol-A and (ii) a stream of gaseous bromine, the gaseous stream having a Reynold's number ≥ 40,000; (b) the reaction mass containing from 50 to 20,000 ppm unreacted bromine and less than 20 wt.% HBr; and (c) the reaction mass having precipitated there form tetrabromobisphenol-A, all of (a)(ii); (b) and (c) occurring during the bisphenol-A feed.
摘要翻译：本发明涉及一种通过溴化双酚-A生产四溴双酚-A的方法，该方法的特征在于：（a）将反应物料（i）加入到双酚-A和（ii）气态溴物流中，雷诺数≥40,000的气流; （b）含有50至20,000ppm未反应溴和少于20重量％HBr的反应物料; 和（c）在那里沉淀的反应物质形成四溴双酚-A，全部（a）（ii）; （b）和（c）在双酚A进料过程中发生。

25. 发明公开

EP0822927A1 A PROCESS FOR THE PREPARATION OF TETRABROMOBISPHENOL-A 失效
标题翻译：用于生产四溴双酚A
公开(公告)号：EP0822927A1
公开(公告)日：1998-02-11
申请号：EP96916430.0
申请日：1996-04-18
申请人： ALBEMARLE CORPORATION
发明人： McKINNIE, Bonnie, G. , HOLUB, Richard, A. , ELNAGAR, Hassan, Y.
IPC分类号： C07C , C07C37 , C07C39
CPC分类号： C07C37/62 , C07C39/367
摘要： This invention relates to a process for the production of tetrabromobisphenol-A by the bromination of bisphenol-A, which process features the addition of bisphenol-A to a reaction mass containing unreacted Br2 and 30 to 85 wt.% water and an alcohol solvent, the reaction mass being at a relatively high temperature.

26. 发明公开

EP1778645A2 PROCESS FOR PRODUCING N-HALOGENATED ORGANIC COMPOUNDS 审中-公开
标题翻译：方法生产N-卤化有机化合物
公开(公告)号：EP1778645A2
公开(公告)日：2007-05-02
申请号：EP05771462.8
申请日：2005-07-12
申请人： ALBEMARLE CORPORATION
发明人： ELNAGAR, Hassan, Y. , PETERS, Bruce, C , SPIELMAN, Edge, E., Jr. , THOMAS, Dustin, H.
IPC分类号： C07D233/82
CPC分类号： C07D233/82
摘要： The process enables highly effective N-halogenation of a compound having one or more halogenatable amido or imido functional groups in the molecule. The process involves, for example, concurrently feeding into a reactor (i) water, inorganic base, and the compound to be N-halogenated, e.g., a hydantoin, and a feed of (ii) a brominating agent and/or a chlorinating agent. The proportions of these feeds are such that the pH is kept at 5 or below or within a specified range e.g., 5.5-8.5 and one or more of the amido or imido nitrogen atoms is substituted by a bromine or chlorine atom. A feature of the process is that it can be conducted at elevated temperatures as high as about 90°C without appreciable thermal decomposition of reactants or product. The resultant product continuously precipitates in high yield and purity. Moreover, products can be produced that are very pale yellow to almost pure white in appearance. Further, the process has been found capable of producing 1,3-dibromo-5,5-dimethylhydantoin with far larger particle sizes than previously produced on a commercial basis.

27. 发明公开

EP1730097A1 PREPARATION OF STERICALLY HINDERED HYDROXYPHENYLCARBOXYLIC ACID ESTERS 有权转让
标题翻译：经过稀释的羟基苯甲酸甲酯的制备
公开(公告)号：EP1730097A1
公开(公告)日：2006-12-13
申请号：EP05713643.4
申请日：2005-02-10
申请人： ALBEMARLE CORPORATION
发明人： GATTO, Vincent, J. , ELNAGAR, Hassan, Y. , CHENG, Chi-Hung , ADAMS, J. Robert
IPC分类号： C07C69/732 , C07C67/347 , C07C67/60 , C09K15/08 , C10M129/76
CPC分类号： C10M177/00 , C07C67/03 , C07C67/347 , C07C67/60 , C09K15/08 , C10M129/76 , C10M2207/026 , C10M2207/289 , C10N2230/10 , C10N2270/00 , C07C69/732
摘要： A novel manufacturing process is described for producing hindered phenolic alkyl esters, which may be useful as antioxidants. This process simplifies catalyst neutralization and removal during the preparation of hindered phenolic esters. Compositions that comprise the hindered phenolic esters produced according to these methods are also described.
摘要翻译：描述了一种用于生产受阻酚类烷基酯的新型制造方法，其可用作抗氧化剂。该过程简化了受阻酚酯制备过程中催化剂的中和和去除。还描述了包含根据这些方法制备的受阻酚酯的组合物。

28. 发明公开

EP0889896A1 SYNTHESIS OF CYCLOALKYLDIARYLPHOSPHINES 失效
标题翻译：环烷基二芳基磷杂环戊二烯的合成
公开(公告)号：EP0889896A1
公开(公告)日：1999-01-13
申请号：EP97916918.0
申请日：1997-03-24
申请人： ALBEMARLE CORPORATION
发明人： SENARATNE, K., Pushpananda, A. , MALCOLM, Arcelio, J. , ORIHUELA, Felix, M. , ELNAGAR, Hassan, Y.
IPC分类号： C07F9
CPC分类号： C07F9/5077
摘要： Partially sterically-hindered cycloalkyl chlorides are reacted with lithium diarylphosphides in inert liquid hydrocarbon reaction media to form cycloalkyldiarylphosphines. Aryl lithium is coproduced. The process makes it possible to avoid, or at least substantially eliminate, the interaction with or cleavage of cyclic ether reaction media such as tetrahydrofuran, previously the solvent of choice for conducting this type of reaction. Also during the conduct of the present process the chloro-substituted cycloalkane does not undergo any appreciable reaction with the coproduced aryl lithium as it is formed. Thus improvements both in yield and quality of the cycloalkyldiarylphosphine product are made possible. A comprehensive three-step process for converting triarylphosphine to cycloalkyldiarylphosphine is also described.
摘要翻译：部分空间位阻的环烷基氯化物与锂二芳基磷化物在惰性液体烃反应介质中反应形成环烷基二芳基膦。芳基锂是联产的。该方法可以避免或者至少基本上消除环醚反应介质如四氢呋喃与预先用于进行这类反应的溶剂的相互作用或裂解。在进行本发明方法的过程中，氯取代的环烷烃在形成时与联产生的芳基锂不发生明显的反应。因此，环烷基二芳基膦产物的收率和质量的改善成为可能。还描述了将三芳基膦转化为环烷基二芳基膦的综合三步法。

29. 发明授权

EP2034837B1 BIOFILM CONTROL 有权
标题翻译： BIOFILMSTEUERUNG
公开(公告)号：EP2034837B1
公开(公告)日：2011-03-09
申请号：EP07812494.8
申请日：2007-06-29
申请人： Albemarle Corporation
发明人： SAUER, Joe, D. , NALEPA, Christopher, J. , PICKRELL, William, S. , STARRETT, Richmond, M. , ELNAGAR, Hassan, Y. , COOK, George, W., Jr. , MOORE, Robert, M., Jr.
IPC分类号： A01N43/50
CPC分类号： A01N43/50
摘要： Compositions and methods suitable for killing bacteria and controlling biofilms comprising one or more microorganisms are provided wherein molecules capable of emulating cell-to-cell signal molecules of the microorganisms are utilized.

30. 发明公开

EP1250049A1 1,3-DIBROMO-5,5-DIMETHYLHYDANTOIN OF ENHANCED PROPERTIES 有权
标题翻译： 1,3-二溴-5,5-二DIMETHYLHYDRANTOIN具有改进的性能
公开(公告)号：EP1250049A1
公开(公告)日：2002-10-23
申请号：EP01942511.5
申请日：2001-01-17
申请人： ALBEMARLE CORPORATION
发明人： ELNAGAR, Hassan, Y. , HOWARTH, Jonathan, N. , PETERS, Bruce, C. , SPIELMAN, Edgar, E., Jr. , THOMAS, Dustin, H.
IPC分类号： A01N59/00 , C07D233/82
CPC分类号： C07D233/82 , A01N59/00 , Y10S514/951 , A01N25/34 , A01N25/12 , A01N2300/00
摘要： Among the enhanced properties of the 1,3-dibromo-5,5-dimethylhydantoins described are their larger average particle sizes, their compactibility even though devoid of a binder, their excellent free-flowing and low-dust properties, and their more appealing aesthetic qualities, as compared to previously known 1,3-dibromo-5,5-dimethylhydantoins. These novel 1,3-dibromo-5,5-dimethyl-hydantoins can be produced, for example, by concurrently feeding (i) an aqueous solution or slurry formed from an inorganic base and 5,5-dimethylhydantoin, and (ii) a brominating agent, in proportions such that each nitrogen atom is substituted by a bromine atom, thereby forming product which precipitates in an aqueous reaction mixture. The pH of the reaction mixture is maintained in the range of 5.5 to 8.5.

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