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21. 发明授权

US5149889A Composition for use in organolithium synthesis reactions 失效
标题翻译：用于有机锂合成反应的组合物
公开(公告)号：US5149889A
公开(公告)日：1992-09-22
申请号：US605742
申请日：1990-10-30
申请人： Jurgen Deberitz , Wilfried Weiss
发明人： Jurgen Deberitz , Wilfried Weiss
IPC分类号： C07F1/02
CPC分类号： C07F1/02
摘要： A process is disclosed for the preparation of tertiary alcohols, alpha-alkyl substituted nitriles, alkyl-substituted imines or tertiary amines by alkylation of a starting material that is a carbonyl compound or a nitrile followed by hydrolysis wherein the alkylation is carried out with the aid of a reaction system formed by suspending a mixture of:substantially 15 to 25% by weight of methyllithium or ethyllithium;substantially 35 to 45% by weight of an inorganic compound selected from the group which consists of at least one metal oxide selected from the group which consists of SiO.sub.2, Al.sub.2 O.sub.3, and CaO, and synthetic anhydrous aluminum silicate; andsubstantially 35 to 45% by weight of a paraffin oil or wax; in an organic solvent selected from the group which consists of:C.sub.5 to C.sub.10 saturated aliphatic hydrocarbons, C.sub.5 to C.sub.10 cycloaliphatic hydrocarbons, aromatic hydrocarbons selected from the group which consists of benzene, toluene, and xylene, and aliphatic or cycloaliphatic ethers selected from the group which consists of diisopropyl ether, di-n-butyl ether, tert-butylether, tetrahydrofuran and dioxane.
摘要翻译：公开了制备叔醇，α-烷基取代的腈，烷基取代的亚胺或叔胺的方法，该方法是通过羰基化合物或腈的原料烷基化，然后进行水解，其中烷基化是借助于通过将基本上为15至25重量％的甲基锂或乙基锂的混合物悬浮而形成的反应体系; 基本上为35〜45重量％的选自由选自由SiO 2，Al 2 O 3和CaO组成的组中的至少一种金属氧化物组成的组的无机化合物和合成的无水硅酸铝; 和基本上35至45重量％的石蜡油或蜡; 在选自以下的有机溶剂中：C5至C10饱和脂族烃，C5至C10脂环族烃，选自苯，甲苯和二甲苯组成的组的芳族烃和选自以下的脂族或脂环族醚：其由二异丙醚，二正丁基醚，叔丁基醚，四氢呋喃和二恶烷组成。

22. 发明授权

US09045701B2 Method of hydrotreating feeds from renewable sources with indirect heating 有权
标题翻译：从间接加热的可再生能源加氢处理饲料的方法
公开(公告)号：US09045701B2
公开(公告)日：2015-06-02
申请号：US12912214
申请日：2010-10-26
申请人： Wilfried Weiss , Laurent Bournay , Thierry Chapus
发明人： Wilfried Weiss , Laurent Bournay , Thierry Chapus
IPC分类号： C10G65/02 , C10G3/00 , C10G65/04
CPC分类号： C10G3/48 , C10G3/46 , C10G3/50 , C10G65/04 , C10G2300/1014 , C10G2300/1018 , C10G2300/4006 , C10G2300/4018 , C10G2300/4081 , C10G2400/04 , C10G2400/08 , Y02P30/20
摘要： The invention describes a method of treating feeds from renewable sources comprising: a hydrotreatment stage a) comprising at least two catalytic zones in which the entry stream comprising said feed mixed with at least a part of a hydrotreated liquid effluent from stage b) is introduced into the first catalytic zone at a temperature comprised between 150 and 260° C., and the effluent from the first catalytic zone is then introduced, mixed with at least a part of a hydrotreated liquid effluent from stage b) and preheated, into the following catalytic zone or zones at a temperature comprised between 260 and 320° C., a stage b) of separation of the effluent from the hydrotreatment stage a) permitting the separation of a gaseous effluent and of a hydrotreated liquid effluent of which at least a part is recycled upstream from each catalytic zone of stage a).
摘要翻译：本发明描述了一种处理来自可再生来源的饲料的方法，包括：加氢处理阶段a）包括至少两个催化区，其中将包含所述进料的进料与至少一部分来自阶段b）的加氢处理的液体流出物混合引入第一催化剂区域在150-260℃的温度下，然后引入来自第一催化区域的流出物，与来自步骤b）的加氢处理的液体流出物的至少一部分混合并预热到下面的催化剂区域或区域，温度为260至320℃，阶段b）将流出物与加氢处理阶段分离a）允许将气态流出物和至少部分为至少一部分的加氢处理液体流出物分离在阶段a）的每个催化区上游再循环。

23. 发明申请

US20110094148A1 METHOD OF HYDROTREATING FEEDS FROM RENEWABLE SOURCES WITH INDIRECT HEATING 有权
标题翻译：从具有间接加热的可再生能源加氢饲料的方法
公开(公告)号：US20110094148A1
公开(公告)日：2011-04-28
申请号：US12912214
申请日：2010-10-26
申请人： Wilfried WEISS , Laurent BOURNAY , Thierry CHAPUS
发明人： Wilfried WEISS , Laurent BOURNAY , Thierry CHAPUS
IPC分类号： C10L1/188
CPC分类号： C10G3/48 , C10G3/46 , C10G3/50 , C10G65/04 , C10G2300/1014 , C10G2300/1018 , C10G2300/4006 , C10G2300/4018 , C10G2300/4081 , C10G2400/04 , C10G2400/08 , Y02P30/20
摘要： The invention describes a method of treating feeds from renewable sources comprising: a hydrotreatment stage a) comprising at least two catalytic zones in which the entry stream comprising said feed mixed with at least a part of a hydrotreated liquid effluent from stage b) is introduced into the first catalytic zone at a temperature comprised between 150 and 260° C., and the effluent from the first catalytic zone is then introduced, mixed with at least a part of a hydrotreated liquid effluent from stage b) and preheated, into the following catalytic zone or zones at a temperature comprised between 260 and 320° C., a stage b) of separation of the effluent from the hydrotreatment stage a) permitting the separation of a gaseous effluent and of a hydrotreated liquid effluent of which at least a part is recycled upstream from each catalytic zone of stage a).
摘要翻译：本发明描述了一种处理来自可再生来源的饲料的方法，包括：加氢处理阶段a）包括至少两个催化区，其中将包含所述进料的进料与至少一部分来自阶段b）的加氢处理的液体流出物混合引入第一催化剂区域在150-260℃的温度下，然后引入来自第一催化区域的流出物，与来自步骤b）的加氢处理的液体流出物的至少一部分混合并预热到下面的催化剂区域或区域，温度为260至320℃，阶段b）将流出物与加氢处理阶段分离a）允许将气态流出物和至少部分为至少一部分的加氢处理液体流出物分离在阶段a）的每个催化区上游再循环。

24. 发明申请

US20070187847A1 Process for the preparation of pure aryllithium compounds and their use 有权
标题翻译：纯芳基锂化合物的制备方法及其用途
公开(公告)号：US20070187847A1
公开(公告)日：2007-08-16
申请号：US11725614
申请日：2007-03-20
申请人： Ute Emmel , Wilfried Weiss , Ulrich Wietelmann , Dirk Dawidowski
发明人： Ute Emmel , Wilfried Weiss , Ulrich Wietelmann , Dirk Dawidowski
IPC分类号： C07F1/02
CPC分类号： C07F1/02
摘要： A process is described for preparing aryllithium compounds by reaction of metallic lithium in an ether-containing solvent with an aryl halide, wherein prior to or at the beginning of the reaction a catalyst is added, the catalyst containing a halogen-free, polynuclear aromatic (aryl catalyst) or consisting of such a compound.
摘要翻译：描述了通过在含醚溶剂中的金属锂与芳基卤化物反应来制备芳基锂化合物的方法，其中在反应之前或开始时加入催化剂，所述催化剂含有无卤素的多核芳族（芳基催化剂）或由这种化合物组成。

25. 发明授权

US07175784B2 Method for the production of alkyl lithium compounds by using reduced pressure 有权
标题翻译：通过减压生产烷基锂化合物的方法
公开(公告)号：US07175784B2
公开(公告)日：2007-02-13
申请号：US10498186
申请日：2002-12-10
申请人： Wilfried Weiss , Eike Dolling , Bernd Schneider
发明人： Wilfried Weiss , Eike Dolling , Bernd Schneider
IPC分类号： C07F1/02
CPC分类号： C07F1/02
摘要： Disclosed is a method for producing Alkyllithium compounds by reacting metallic lithium with an Alkyl halide in a solvent. The reaction is performed at a reduced pressure at the boiling point of the solvent.
摘要翻译：公开了通过在溶剂中使金属锂与烷基卤化物反应制备烷基锂化合物的方法。该反应在溶剂沸点的减压下进行。

26. 发明申请

US20050051911A1 Method for the production of alkyllithium compounds by using reduced pressure 有权
标题翻译：通过减压生产烷基锂化合物的方法
公开(公告)号：US20050051911A1
公开(公告)日：2005-03-10
申请号：US10498186
申请日：2002-12-10
申请人： Wilfried Weiss , Eike Dolling , Bernd Schneider
发明人： Wilfried Weiss , Eike Dolling , Bernd Schneider
IPC分类号： C07F1/02
CPC分类号： C07F1/02
摘要： Disclosed is a method for producing Alkyllithium compounds by reacting metallic lithium with an Alkyl halide in a solvent. The reaction is performed at a reduced pressure at the boiling point of the solvent.
摘要翻译：公开了通过在溶剂中使金属锂与烷基卤化物反应制备烷基锂化合物的方法。该反应在溶剂沸点的减压下进行。

27. 发明授权

US06756024B2 Method for preparing lithium amide 失效
标题翻译：制备氨基化锂的方法
公开(公告)号：US06756024B2
公开(公告)日：2004-06-29
申请号：US10091383
申请日：2002-03-05
申请人： Wilfried Weiss , Dirk Dawidowski
发明人： Wilfried Weiss , Dirk Dawidowski
IPC分类号： C01B2100
CPC分类号： C01B21/0926
摘要： A method for preparing lithium amide is described in which in a first method step lithium metal is reacted with ammonia to form lithium bronze and in a second method step the lithium bronze is reacted with a 1,3-diene or an arylolefin in the presence of a solvent.
摘要翻译：描述了一种制备氨基化锂的方法，其中在第一种方法步骤中，使锂金属与氨反应形成青铜青铜，并且在第二种方法步骤中，将青铜与1,3-二烯或芳基烯烃在溶剂。

28. 发明授权

US5677543A Dissolved methyllithium-containing composition for use in synthesis reactions 失效
标题翻译：用于合成反应使用溶解含甲基的组合物
公开(公告)号：US5677543A
公开(公告)日：1997-10-14
申请号：US499547
申请日：1995-07-07
申请人： Wilfried Weiss , Peter Rittmeyer , Ute Emmel
发明人： Wilfried Weiss , Peter Rittmeyer , Ute Emmel
IPC分类号： C07F1/02 , C09K3/00
CPC分类号： C07F1/02
摘要： Disclosed is a dissolved methyllithium-containing composition for use in synthesis reactions (synthesis composition) and processes of preparing the composition. In the sythesis composition the methyllithium is contained in a solvent of the general formula (I) ##STR1## wherein independently R.sup.1 and R.sup.2 are a hydrogen, methyl or ethyl residue and R.sup.3 and R.sup.4 are a methyl or ethyl residue. To prepare the methyllithium-containing synthesis composition of the invention lithium powder or granular lithium is dispersed in a solvent having the general formula I, methyl halide is added at a controlled rate, the reaction temperature is maintained in the range of from 0.degree. to 60.degree. C., and the resulting lithium halide is separated from the methyllithium solution.
摘要翻译：公开了用于在合成反应（合成组合物）以及制备所述组合物的过程中使用的溶解含甲基的组合物。在合成组合物中，甲基锂包含在通式（I）的溶剂中（I），其中独立地R 1和R 2是氢，甲基或乙基残基，且R 3和R 4是甲基或乙基残基。为了制备本发明的含甲基锂的合成组合物，将锂粉末或颗粒状锂分散在具有通式I的溶剂中，以受控的速率加入甲基卤，反应温度保持在0〜60℃ 并将所得卤化锂与甲基锂溶液分离。

29. 发明授权

US5019214A Twin-wire former for the production of a web of paper 失效
标题翻译：用于生产纸张的双线成型机
公开(公告)号：US5019214A
公开(公告)日：1991-05-28
申请号：US451818
申请日：1989-12-15
申请人： Albrecht Meinecke , Dieter Egelhof , Wilfried Weiss
发明人： Albrecht Meinecke , Dieter Egelhof , Wilfried Weiss
IPC分类号： D21F9/00
CPC分类号： D21F9/003
摘要： A twin-wire former for the production of a web of paper from a fiber suspension. An upper endless loop of wire belt having a lower horizontal run and a lower endless loop wire belt having an upper horizontal run. Guide rolls support the wire belts to define a twin-wire zone. The upstream inlet wedge of the twin-wire zone is disposed at the outlet from a head box. The initial part of the path of the twin-wire zone has a gradual curvature convexly with respect to the lower wire belt, and in that initial portion are positioned guide tables, suction boxes and dewatering elements. This curved initial part is followed by a forming roll within the loop of the upper wire belt. The twin-wires wrap an arcuate sector of the lower region of the forming roll. A support roll follows the forming roll. The support roll is upraised sufficiently to wrap the twin-wires around the bottom of the forming roll and over an arcuate sector at the top of the support roll. Following the support roll, the upper wire separates from the lower wire. In the continuing generally horizontal, slightly descending path of the lower wire with the web on it are disposed a plurality of suction boxes and a lower wire suction roll to define a final dewatering path after the twin-wire zone.
摘要翻译：一种用于从纤维悬浮液生产纸幅的双线成型机。具有较低水平行程的电线带的上部无限循环和具有上部水平行程的下部无端环线缆带。导辊支撑钢丝绳带以限定双线区域。双线区域的上游入口楔设置在头箱的出口处。双线区域的路径的初始部分相对于下部电缆带呈凸起的渐变曲线，并且在该初始部分中定位有引导台，抽吸箱和脱水元件。该弯曲的初始部分之后是在上部线带的环内的成形辊。双丝缠绕成形辊的下部区域的弓形部分。支撑辊跟随成型辊。支撑辊被充分地升高以将双网包裹在成形辊的底部周围并且在支撑辊的顶部的弓形部分上方。在支撑辊之后，上部电线与下部电线分离。在其上具有腹板的下部丝线的连续大致水平的稍微下降的路径中设置有多个抽吸盒和下部线抽吸辊，以在双网区域之后限定最终脱水路径。

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