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11. 发明授权

US4243613A Process for the manufacture of mixtures of formaldehyde and methanol by partial oxidation of methane 失效
标题翻译：通过部分氧化甲烷制造甲醛和甲醇的混合物的方法
公开(公告)号：US4243613A
公开(公告)日：1981-01-06
申请号：US945397
申请日：1978-09-25
申请人： Rudolf Brockhaus , Hans-Jurgen Franke
发明人： Rudolf Brockhaus , Hans-Jurgen Franke
IPC分类号： C07C47/04 , C07C29/50 , C07C31/04 , C07C45/33 , C07C47/048 , C07C47/48 , C07C27/14
CPC分类号： C07C29/50 , C07C45/33
摘要： A continuous process for the partial oxidation of methane to produce mixtures of formaldehyde and methanol wherein methane and an oxidizing gas are reacted in a reaction zone in the form of a flame and the resulting reaction mixture is cooled followed by separation of the resulting products, is further improved by controlling the velocity of the oxidizing gas so that it is 50 to 300 meters per second higher than the methane gas with the methane gas being introduced in a velocity of from 1 to 15 meters per second. Also, the stream of methane gas has a volume that is 3 to 100 times greater than the volume of the stream of oxidizing gas introduced into the reaction zone.
摘要翻译：用于部分氧化甲烷以产生甲醛和甲醇的混合物的连续方法，其中甲烷和氧化气体在火焰形式的反应区中反应，并将所得反应混合物冷却，然后分离得到的产物，是通过控制氧化气体的速度进一步改善，使得其比甲烷气体高50至300米/秒，甲烷气体以每秒1至15米的速度被引入。此外，甲烷气体的流量比引入反应区域的氧化气体流的体积大3至100倍。

12. 发明授权

US4075238A Polyhalobenzylic disulfooxonium compounds 失效
标题翻译：多卤苄基二氧化硫化合物
公开(公告)号：US4075238A
公开(公告)日：1978-02-21
申请号：US607326
申请日：1975-08-25
申请人： Victor Mark , Leon R. Zengierski
发明人： Victor Mark , Leon R. Zengierski
IPC分类号： C07C381/00 , C07C141/14 , C07C47/48 , C07C141/16
CPC分类号： C07C381/00
摘要： Polyhalobenzylic disulfooxonium compounds are produced by the reaction of aromatic methyl, halomethyl or hydroxymethyl substituents with sulfur trioxide. The disulfooxonium salts are readily converted to alcohols by hydrolysis to provide monomers for the production of fire resistant polymers and additives for polymers. Likewise, the disulfooxonium compounds of this invention present chemical intermediates for a wide range of useful products such as halogenated pesticides.
摘要翻译：通过芳族甲基，卤代甲基或羟甲基取代基与三氧化硫的反应制备多卤苄基二氧化氮化合物。通过水解容易地将二氧化硫鎓盐转化为醇，以提供用于生产耐火聚合物的单体和用于聚合物的添加剂。同样地，本发明的二氧化氮化合物为各种有用的产物如卤化农药提供化学中间体。

13. 发明授权

US4052461A Hydroformylation process 失效
标题翻译：氢化工艺
公开(公告)号：US4052461A
公开(公告)日：1977-10-04
申请号：US565167
申请日：1975-04-04
申请人： Harold Burnham Tinker , Donald E. Morris
发明人： Harold Burnham Tinker , Donald E. Morris
IPC分类号： B01J31/16 , B01J31/18 , B01J31/20 , B01J31/24 , C07C45/49 , C07C45/50 , C07C47/48 , B01J21/02
CPC分类号： B01J31/2404 , B01J31/1895 , B01J31/20 , B01J31/24 , C07C45/49 , C07C45/50 , B01J2231/321 , B01J2531/822
摘要： The invention relates to a process for the preparation of aldehydes by the hydroformylation of olefinically unsaturated compounds using a rhodium catalyst which catalyst is provided by (1) introducing rhodium into the reaction solution in the form of an ionic rhodium compound, the said ionic compound consisting of (a) a rhodium-containing cation having rhodium complexed with ligands other than halide, and (b) a non-coordinating anion; and (2) furnishing to the reaction solution at least two moles of a modifying ligand per mole of ionic rhodium compound where the modifying ligand is furnished either pre-coordinated in the said ionic rhodium compound or as a free compound, and where the modifying ligand is a tertiary organo phosphorous compound having from 3 to 90 carbon atoms, or a tertiary organo arsenic compound having from 3 to 90 carbon atoms, or a tertiary organo antimony compound having from 3 to 90 carbon atoms.The process is especially useful for the production of aldehydes from olefinically unsaturated compounds having from 2 to 30 carbon atoms, carbon monoxide, and hydrogen at a total pressure of from 4.6 to 142 kg/cm.sup.2 (50 to 2,000 psig), and at a temperature of from about 60.degree. C to about 180.degree. C.A preferred embodiment of the invention utilizes the modifying ligand at a molar concentration in excess of that required stoichiometrically by the ionic rhodium compound. Another preferred embodiment of this invention employs the modifying ligand as the solvent for the reaction system.

14. 发明授权

US3520934A Hydrogenation of cinnamaldehyde 失效
标题翻译：辛酰胺的氢化反应
公开(公告)号：US3520934A
公开(公告)日：1970-07-21
申请号：US3520934D
申请日：1968-07-15
申请人： UNIVERSAL OIL PROD CO
发明人： DUNKEL MORRIS , ECKHARDT DANIEL J , STERN ALFRED
IPC分类号： B01J23/58 , C07C45/62 , C07C47/48
CPC分类号： B01J23/58 , C07C45/62

15. 发明授权

US4187319A Substituted benzaldehyde hypolipidemic agents 失效
标题翻译：取代苯甲醛降血脂药
公开(公告)号：US4187319A
公开(公告)日：1980-02-05
申请号：US802853
申请日：1977-06-02
申请人： Thomas R. Blohm , J. Martin Grisar , Roger A. Parker
发明人： Thomas R. Blohm , J. Martin Grisar , Roger A. Parker
IPC分类号： A61K31/11 , C07C47/575 , C07C47/48
CPC分类号： C07C323/00 , A61K31/11 , C07C45/41
摘要： Substituted benzaldehydes of the following general structure are useful as hypolipidemic agents: ##STR1## wherein Y is selected from oxygen and divalent sulfur; R is selected from a straight or branched saturated hydrocarbon chain having from 10 to 20 carbon atoms and a straight or branched unsaturated hydrocarbon chain having from 10 to 20 carbon atoms and from 1 to 4 double bonds.
摘要翻译：具有以下通用结构的取代的苯甲醛可用作降血脂剂：其中Y选自氧和二价硫; R选自具有10至20个碳原子的直链或支链饱和烃链和具有10至20个碳原子和1至4个双键的直链或支链不饱和烃链。

16. 发明授权

US4187247A 9-Substituted phenyl-3,7-dimethyl-nona 2,4,6,8-tetraene compounds 失效
标题翻译： 9-取代的苯基-3,7-二甲基 - 非2,4,6,8-四烯化合物
公开(公告)号：US4187247A
公开(公告)日：1980-02-05
申请号：US019025
申请日：1979-03-08
申请人： Werner Bollag , Rudolf Ruegg , Gottlieb Ryser
发明人： Werner Bollag , Rudolf Ruegg , Gottlieb Ryser
IPC分类号： C07C37/045 , C07C205/22 , C07C205/37 , C07F9/54 , C07C47/48 , C07C41/00 , C07C41/52
CPC分类号： C07F9/5456 , C07C205/22 , C07C205/37 , C07C37/045 , C07C41/16 , C07C41/30
摘要： Novel 9-substituted phenyl-3,7-dimethyl-nona-2,4,6,8-tetraene derivatives useful as anti-tumor agents.
摘要翻译：用作抗肿瘤剂的新型9-取代苯基-3,7-二甲基 - 非 - 2,4,6,8-四烯衍生物。

17. 发明授权

US4111998A Process for the preparation of aromatic aldehydes 失效
标题翻译：芳香醛制备方法
公开(公告)号：US4111998A
公开(公告)日：1978-09-05
申请号：US489715
申请日：1974-07-18
申请人： Jean-Pierre Decor
发明人： Jean-Pierre Decor
IPC分类号： B01J23/00 , C07B61/00 , C07C45/00 , C07C45/41 , C07C47/228 , C07C47/52 , C07C67/00 , C07C47/48
CPC分类号： C07C45/41
摘要： A process is provided for the preparation of a juxtanuclear or extranuclear aromatic aldehyde, said process comprising effecting the catalytic reduction of the corresponding acid chloride using hydrogen in the presence of a palladium catalyst and a tertiary amide. The use of the tertiary amide increases the selectivity, activity and working life of the catalyst as compared with conventional processes and renders the use of catalyst regulators such as quinoline or sulphur-containing compounds unnecessary.
摘要翻译：提供了一种用于制备多核或非核芳香醛的方法，所述方法包括在钯催化剂和叔酰胺存在下，使用氢催化还原相应的酰氯。与常规方法相比，叔酰胺的使用增加了催化剂的选择性，活性和使用寿命，并且使得不需要使用催化剂调节剂如喹啉或含硫化合物。

18. 发明授权

US3754038A 2-phenyl-2-alkenals 失效
标题翻译： 2-PHENYL-2-ALKENALS
公开(公告)号：US3754038A
公开(公告)日：1973-08-21
申请号：US3754038D
申请日：1970-11-23
申请人： INT FLAVORS & FRAGRANCES INC
发明人： VAN PRAAG M , STEIN H
IPC分类号： A23L27/20 , C07C45/74 , C07C47/232 , C07C47/48
CPC分类号： C07C47/232 , A23L27/204 , C07C45/74
摘要： NOVEL UNSATURATED ALDEHYDES, PARTICULARLY 2-PHENYL-2ALKENALS, USEFUL FOR PREPARING FLAVORING COMPOSITIONS AND FOOD COMPOSITIONS, PARTICULARLY THOSE HAVING CHOCOLATE OR COCOA FLAVOR AAND/OR AROMA QUALITIES, FLAVORING AND FOOD COMPOSITIONS CONTAINING SUCH ALDEHYDES, AND METHODS FOR PREPARING SUCH ALDEHYDES AND COMPOSITIONS.

19. 发明授权

US3579589A Process for manufacturing a catalyst,resulting catalyst and process for manufacture of benzoic aldehyde from toluene in the presence of said catalyst 失效
标题翻译：催化剂制备方法，催化剂的制备及其在催化剂存在下从苯乙烯制备苯甲醛的方法
公开(公告)号：US3579589A
公开(公告)日：1971-05-18
申请号：US3579589D
申请日：1968-09-05
申请人： INST FRANCAIS DU PETROLE
发明人： DELMON BERNARD
IPC分类号： B01J23/24 , C07C45/36 , C07C51/265 , C07C47/48 , C07C47/52
CPC分类号： C07C45/36 , B01J23/24 , C07C51/265 , Y02P20/582 , C07C47/54 , C07C63/06
摘要： PROCESS FOR MANUFACTURING A CATALYST USED FOR OXIDIZING TOLUENE TO BENZALDEHYDE, WHICH PROCESS COMPISES ADMIXING AN URANIUM OXIDE OR SALT WITH A MOLYBDENUM OXIDE OR SALT IN THE PRESENCE OF SULFURIC ACID, DRYING AND CALCINATING THE RESULTING MIXTURE. OPTIONALLY, THERE CAN BE ADDED TO THE MIXTURE, BEFORE DRYING AND CALCINATING, AN ALKALINE OR ALKALINE-EARTH METAL COMPOUND AND/OR METALS OR COMPOUNDS OF METALS SUCH AS CHROMIUM, TUNGSTEN, SILVER COPPER, YTYTRIUM, CERIUM AND OTHER ELEMENTS FROM THE GROUP OF THE RARE EARTHS.

20. 发明授权

US3520935A Hydrogenation of cinnamic aldehyde 失效
标题翻译：加氢脱氢酶
公开(公告)号：US3520935A
公开(公告)日：1970-07-21
申请号：US3520935D
申请日：1969-05-01
申请人： UNIVERSAL OIL PROD CO
发明人： ARRIGO JOSEPH T , CHRISTENSEN NILS J , CHRYSLER RICHARD L , SPARKS ALLEN K
IPC分类号： B01J23/58 , C07C45/62 , C07C47/228 , C07C47/48
CPC分类号： C07C47/228 , B01J23/58 , C07C45/62

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