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11. 发明授权

US5726340A Method of producing aromatic carbonate 失效
标题翻译：芳香族碳酸酯的制造方法
公开(公告)号：US5726340A
公开(公告)日：1998-03-10
申请号：US796673
申请日：1997-03-04
申请人： Masatoshi Takagi , Katsufumi Kujira , Takahiro Yoneyama , Yuji Ohgomori
发明人： Masatoshi Takagi , Katsufumi Kujira , Takahiro Yoneyama , Yuji Ohgomori
IPC分类号： B01J27/135 , B01J31/26 , C07B61/00 , C07C68/00 , C07C69/96
CPC分类号： C07C68/005 , Y10T307/729 , Y10T307/944 , Y10T307/951
摘要： The present invention relates to a method of producing an aromatic carbonate by reacting an aromatic hydroxy compound, carbon monoxide, and oxygen, wherein the reaction is carried out in the presence of a catalyst comprising: (A) at least one selected from palladium and palladium compounds; (B) at least one lead compound; (C) at least one cobalt compound; and, (D) at least one halide. According to this method an aromatic carbonate which produces only a small amount of impurities and has excellent selectivity can be produced.
摘要翻译：本发明涉及通过使芳族羟基化合物，一氧化碳和氧气反应制备芳族碳酸酯的方法，其中反应在催化剂存在下进行，所述催化剂包含：（A）至少一种选自钯和钯化合物（B）至少一种铅化合物; （C）至少一种钴化合物; 和（D）至少一种卤化物。根据该方法，可以生产仅产生少量杂质并具有优异选择性的芳族碳酸酯。

12. 发明授权

US5498789A Method of producing aromatic carbonate 失效
标题翻译：芳香族碳酸酯的制造方法
公开(公告)号：US5498789A
公开(公告)日：1996-03-12
申请号：US348116
申请日：1994-11-28
申请人： Masatoshi Takagi , Hidekazu Miyagi , Yuji Ohgomori , Hiroshi Iwane
发明人： Masatoshi Takagi , Hidekazu Miyagi , Yuji Ohgomori , Hiroshi Iwane
IPC分类号： C07C68/00 , C07C69/96
CPC分类号： C07C68/005
摘要： The present invention relates to a method of producing an aromatic carbonate by reacting an aromatic hydroxy compound, carbon monoxide and oxygen using a catalyst system for suppressing the production of aryl aromatic o-hydroxycarboxylate as a by-product. The catalyst system consists of the following compounds:(A) at least one selected from palladium and palladium compounds;(B) at least one selected from lead compounds; and(C) at least one halide selected from quaternary ammonium halides and quaternary phosphonium halides; and if required,(D) at least one selected from copper and copper compounds.The method of the present invention can increase the yield of an aromatic carbonate per palladium (the turnover number of palladium).
摘要翻译：本发明涉及通过芳香族羟基化合物，一氧化碳和氧气的反应来制造芳香族碳酸酯的方法，该催化剂体系用于抑制作为副产物的芳基芳族邻羟基羧酸酯的生产。催化剂体系由以下化合物组成：（A）选自钯和钯化合物中的至少一种; （B）选自铅化合物中的至少一种; 和（C）选自季铵卤化物和季鏻卤化物的至少一种卤化物; 如果需要，（D）选自铜和铜化合物中的至少一种。本发明的方法可以提高每钯的芳族碳酸酯的收率（钯的转换数）。

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