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11. 发明授权

US09314759B2 Apparatus and method for hydroconversion 有权
标题翻译：加氢转化装置和方法
公开(公告)号：US09314759B2
公开(公告)日：2016-04-19
申请号：US14168099
申请日：2014-01-30
申请人： Steven Xuqi Song , Donald Leroy Kuehne , Abdenour Kemoun , Bruce Edward Reynolds
发明人： Steven Xuqi Song , Donald Leroy Kuehne , Abdenour Kemoun , Bruce Edward Reynolds
IPC分类号： B01J8/00 , B01J8/02 , B01J19/00 , B01J19/24 , B01J19/30 , B01J8/06 , B01J8/22 , B01J8/44 , C10G45/02 , C10G45/16 , C10G45/22 , C10G47/26 , C10G49/12 , B01J8/18 , C10G45/00 , C10G47/00 , C01G49/00
CPC分类号： B01J8/06 , B01J8/005 , B01J8/007 , B01J8/1827 , B01J8/22 , B01J8/226 , B01J8/44 , B01J2208/00176 , B01J2208/00929 , B01J2208/025 , B01J2208/026 , B01J2219/0004 , C10G45/02 , C10G45/16 , C10G45/22 , C10G47/26 , C10G49/12
摘要： An apparatus is disclosed for the hydroconversion of hydrocarbon feedstock with a hydrogen gas at elevated temperature and pressure with the use of a catalyst. The apparatus is a reactor vessel with a grid plate distributor for improved gas liquid distribution. The distributor comprises a grid plate and a bubble cap assembly with a plurality of tubular risers extending through the grid plate. Each tubular riser has an upper section above the grid plate and a lower section below the grid plate, the lower section terminated with an open bottom end for ingress of the hydrogen gas and hydrocarbon feedstock, the upper section having a closed top terminated with a housing cap. Each tubular riser has at least a vertical slot and a least a laterally placed opening sufficiently sized such that in operation, the liquid level in the zone below the grid plate is above the vertical slot and below the laterally placed opening.
摘要翻译：公开了一种使用催化剂在升高的温度和压力下用氢气加氢转化烃原料的装置。该装置是具有用于改善气体液体分布的格栅分配器的反应器容器。分配器包括格栅板和气泡盖组件，其具有延伸穿过格栅板的多个管状立管。每个管状提升管具有在格栅板上方的上部部分和在格栅板下方的下部分，下部部分终止于用于进入氢气和烃原料的开口底端，上部部分具有封闭的顶部，其与壳体帽。每个管状提升管具有至少一个垂直狭槽和至少一个横向放置的开口，其尺寸足够大，使得在操作中，格栅板下方的区域中的液位高于垂直槽并在横向放置的开口下方。

12. 发明授权

US09079141B2 Vortex-type mixing device for a down-flow hydroprocessing reactor 有权
标题翻译：用于下流加氢反应器的涡旋式混合装置
公开(公告)号：US09079141B2
公开(公告)日：2015-07-14
申请号：US13663570
申请日：2012-10-30
申请人： Craig Boyak , Abdenour Kemoun , Ralph Evans Killen , Krishniah Parimi , Steven Xuqi Song
发明人： Craig Boyak , Abdenour Kemoun , Ralph Evans Killen , Krishniah Parimi , Steven Xuqi Song
IPC分类号： B01J8/04 , B01F3/04 , B01F5/00
CPC分类号： B01F3/04113 , B01F3/04503 , B01F5/0057 , B01J8/04 , B01J8/0453 , B01J8/0492 , B01J2208/00884 , B01J2208/00938
摘要： The present invention is directed to a vortex-type mixing device for a down-flow hydroprocessing reactor. In particular, the device improves the effectiveness of an existing mixing volume in mixing the gas phase and liquid phase of two-phase systems. According to the present invention, the mixing device helps create a highly arcuate flow to incoming effluents and a high degree of mixing within a constrained interbed space of a hydroprocessing reactor.
摘要翻译：本发明涉及一种用于下流加氢反应器的涡流式混合装置。特别地，该装置提高了混合两相系统的气相和液相时的现有混合体积的有效性。根据本发明，混合装置有助于在加氢处理反应器的受限制的间隙空间内为进入的流出物形成高度弧形的流动和高度的混合。

13. 发明授权

US07964153B2 Reactor having a downcomer producing improved gas-liquid separation and method of use 有权
标题翻译：具有降液管的反应器产生改进的气液分离和使用方法
公开(公告)号：US07964153B2
公开(公告)日：2011-06-21
申请号：US12002770
申请日：2007-12-19
申请人： Abdenour Kemoun
发明人： Abdenour Kemoun
IPC分类号： B01J8/20 , B01J8/22
CPC分类号： B01J19/006 , B01D19/0057 , B01J19/246 , C10G49/12
摘要： In an upflow reactor for reacting heavy hydrocarbons with hydrogen gas in a liquefied catalyst slurry, that mixture is recirculated down through a downcomer having an upper degassing section which includes a frusto-conical upper surface. The mixture is caused to flow along that surface in a downward helical path, such that heavier components are centrifugally urged outwardly, and lighter components, e.g., gas, migrate inwardly. The gas bubbles can thus coalesce such that small bubbles become bigger bubbles having a greater tendency to rise out of the downcomer. Baffles placed on the upper surface can maximize the residence time of the mixture in the degassing section.
摘要翻译：在用于在液化催化剂浆液中使重质烃与氢气反应的上流式反应器中，该混合物向下循环通过具有上部脱气部分的降液管，该脱水部分包括截头圆锥形的上表面。使混合物沿着该表面沿向下的螺旋路径流动，使得较重的组分被离心地向外推动，较轻的组分（例如气体）向内迁移。气泡因此可以聚结，使得小气泡变得更大的气泡具有从降液管中升出的倾向。放置在上表面上的挡板可以最大化混合物在脱气部分中的停留时间。

14. 发明申请

US20090166257A1 Ionic liquid catalyzed alkylation process employing nozzles and system implementing such process 有权
标题翻译：使用喷嘴的离子液体催化烷基化方法和实施这种方法的系统
公开(公告)号：US20090166257A1
公开(公告)日：2009-07-02
申请号：US12003574
申请日：2007-12-28
申请人： Huping Luo , Abdenour Kemoun , Hye-Kyung Timken
发明人： Huping Luo , Abdenour Kemoun , Hye-Kyung Timken
IPC分类号： C10G55/06
CPC分类号： C10G29/205 , C10G50/00 , C10G2300/1081 , C10G2300/1088 , C10G2300/1092 , C10G2400/02
摘要： A process for a liquid/liquid reaction employs a nozzle dispersion whereby liquid reactants and liquid catalyst are injected through at least one nozzle into a reaction zone to effect a reaction. The reaction can be alkylation of at least one isoparaffin with at least one olefin in the presence of an ionic liquid catalyst. The at least one nozzle provides intimate contact between the phases for greater product control and reaction control.
摘要翻译：液/液反应的方法采用喷嘴分散体，其中液体反应物和液体催化剂通过至少一个喷嘴注入反应区以进行反应。反应可以在离子液体催化剂存在下用至少一种烯烃烷基化至少一种异链烷烃。至少一个喷嘴提供相之间的紧密接触，以实现更大的产品控制和反应控制。

15. 发明申请

US20130082125A1 MULTIPHASE CONTACT AND DISTRIBUTION APPARATUS FOR HYDROPROCESSING 有权
标题翻译：多相接触和分配装置用于水力发电
公开(公告)号：US20130082125A1
公开(公告)日：2013-04-04
申请号：US13686304
申请日：2012-11-27
申请人： Zackory S. Akin , Craig R. Boyak , Abdenour Kemoun , Ralph Evan Killen , Krishniah Parimi , Steven Xuqi Song , Steven Alden Souers
发明人： Zackory S. Akin , Craig R. Boyak , Abdenour Kemoun , Ralph Evan Killen , Krishniah Parimi , Steven Xuqi Song , Steven Alden Souers
IPC分类号： B05B1/14
CPC分类号： B05B1/14 , B01J8/0453 , B01J8/0492 , B01J2208/00884 , B01J2208/00902 , B01J2208/0092 , B01J2208/00929
摘要： Systems and apparatus for mixing, cooling, and distributing multiphase fluid mixtures within a reactor, wherein reactor internal apparatus of the present invention provides not only improved fluid mixing and distribution to each underlying catalyst bed surface, but also offers other advantages including: decreased mixing tray height; easier maintenance, assembly and disassembly; and decreased amounts of fabrication material. In an embodiment, fluid may be evenly distributed to a catalyst bed from a fluid distribution unit comprising a nozzle tray including a plurality of nozzles, wherein the nozzles include at least one liquid inlet disposed tangentially to an inner surface of the nozzle.
摘要翻译：用于在反应器内混合，冷却和分配多相流体混合物的系统和装置，其中本发明的反应器内部装置不仅提供了改进的流体混合和分配到每个下面的催化剂床表面，而且还提供了其它优点，包括：减少的混合托盘高度; 更容易维护，组装和拆卸; 并减少制造材料的数量。在一个实施例中，流体可以从包括包括多个喷嘴的喷嘴托盘的流体分配单元均匀地分布到催化剂床，其中喷嘴包括与喷嘴的内表面相切地设置的至少一个液体入口。

16. 发明授权

US07820120B2 Device for a reactor and method for distributing a multi-phase mixture in a reactor 有权
标题翻译：用于反应器的装置和在反应器中分配多相混合物的方法
公开(公告)号：US07820120B2
公开(公告)日：2010-10-26
申请号：US12002769
申请日：2007-12-19
申请人： Abdenour Kemoun
发明人： Abdenour Kemoun
IPC分类号： B01J19/00
CPC分类号： B01F3/0446 , B01F5/0421 , B01F5/0428 , B01J4/002 , B01J19/246
摘要： An up-flow reactor includes a reaction chamber, and a distributor device disposed in the reaction chamber for distributing a multi-phase mixture therein. The distributor device includes a first pipe adapted for conducting a gas phase, and including first discharge ports, a second pipe adapted for conducting a slurry or a liquid phase, and including second discharge ports, and a plurality of nozzles. Each nozzle communicates a pair of the first and second discharge ports with a venturi outlet of the nozzle, such that pressurized gas phase from the first discharge port passing through the venturi outlet creates a negative pressure for drawing-in the slurry or the liquid phase to be mixed with the gas phase in the venturi outlet.
摘要翻译：上流式反应器包括反应室和设置在反应室中用于在其中分配多相混合物的分配器装置。分配器装置包括适于导入气相的第一管，包括第一排出口，适于导入浆液或液相的第二管，以及包括第二排出口和多个喷嘴。每个喷嘴将一对第一和第二排出口与喷嘴的文氏管出口连通，使得通过文氏管出口的来自第一排出口的加压气相产生用于将浆料或液相吸入的负压与文氏管出口中的气相混合。

17. 发明申请

US20090159499A1 Process and apparatus for separating gas from a multi-phase mixture being recycled in a reactor 有权
标题翻译：用于从反应器中再循环的多相混合物中分离气体的方法和装置
公开(公告)号：US20090159499A1
公开(公告)日：2009-06-25
申请号：US12002772
申请日：2007-12-19
申请人： Abdenour Kemoun
发明人： Abdenour Kemoun
IPC分类号： C10G45/00 , B01J19/00
CPC分类号： C10G49/12 , B01J8/004 , B01J8/008 , B01J8/226 , B01J8/228 , B01J2208/00752
摘要： A reactor in which a multi-phase mixture, including gas and a catalyst slurry or liquid, is to be conducted. The reactor includes a reaction chamber having a substantially unencumbered center portion through which the multi-phase mixture is conducted upwardly. A downcomer arrangement is disposed laterally outwardly of the center portion and adjacent to an inner surface of the reaction chamber. An external pump communicates with a lower portion of the reaction chamber for circulating components of the mixture downward from an upper end of the downcomer arrangement to a lower end thereof. A collection chamber is disposed below the reaction chamber into which the components exiting the downcomer arrangement are introduced and where the gas is separated from the remainder of the components. The separated gas can be reintroduced into the reaction chamber.
摘要翻译：将要进行包括气体和催化剂浆液或液体在内的多相混合物的反应器。反应器包括具有基本上未受阻的中心部分的反应室，多相混合物通过该中心部向上传导。降液装置横向设置在中心部分的外侧并与反应室的内表面相邻。外部泵与反应室的下部连通，用于将混合物的组分从降液管装置的上端向下循环到其下端。收集室设置在反应室下方，离开降液管装置的部件被引入该收集室，并且气体与其余部件分离。分离的气体可以重新引入反应室。

18. 发明授权

US07473405B2 Fluid distribution apparatus for downflow multibed poly-phase catalytic reactor 有权
标题翻译：用于下流多相多相催化反应器的流体分配装置
公开(公告)号：US07473405B2
公开(公告)日：2009-01-06
申请号：US10965167
申请日：2004-10-13
申请人： Abdenour Kemoun , Krishniah Parimi , Duyen T. Nguyen
发明人： Abdenour Kemoun , Krishniah Parimi , Duyen T. Nguyen
IPC分类号： B01J8/02 , B01F3/04
CPC分类号： B01J4/002 , B01J8/1818 , B01J8/1845 , B01J8/1881 , B01J8/22 , B01J19/26
摘要： The invention in one embodiment is a nozzle device for coupling with a fluid distribution conduit for improving the distribution of an upward or downwardly flowing poly-phase mixture including at least one gas phase and at least one liquid phase, above at least one packed bed of granular solid or fluidized bed. The fluid distribution conduit for receiving liquid and gas phases has one or more lateral openings for flow over an upper portion of its height through which a gas phase can enter and has fluid distribution conduit having one or more lateral openings for flow over at least a lower portion of its height through which a liquid phase can enter the fluid distribution conduit. It also has at least one lower cross section for flow through which a mixture of gas and liquid communicate with a packed bed of granular solid or a fluidized bed. The nozzle device includes a venturi nozzle having an outer diameter not greater than an inner diameter of the lower cross section of the fluid distribution conduit, wherein the nozzle device may be fixedly coupled to and co-axially aligned with the lower cross section of the fluid distribution conduit. It is for accelerating and dispersing the liquid and gas phases passing out of the conduit.
摘要翻译：在一个实施方案中，本发明是用于与流体分配管连接的喷嘴装置，用于改善向上或向下流动的包含至少一个气相和至少一个液相的向上或向下流动的多相混合物在至少一个填充床粒状固体或流化床。用于接收液相和气相的流体分配管道具有一个或多个横向开口，用于在其高度的上部流动，气相可通过该开口进入，并且具有流体分配导管，该流体分配导管具有一个或多个横向开口，用于流过至少一个下部其高度的一部分通过液体相进入流体分配导管。它还具有用于流动的至少一个下部横截面，气体和液体的混合物通过该下部横截面与颗粒状固体或流化床的填充床连通。喷嘴装置包括文丘里喷嘴，其外径不大于流体分配管道的下横截面的内径，其中喷嘴装置可以固定地联接到流体的下部横截面并与其同轴对准分销渠道。用于加速和分散通过导管的液相和气相。

19. 发明申请

US20130064740A1 VORTEX-TYPE MIXING DEVICE FOR A DOWN-FLOW HYDROPROCESSING REACTOR 有权
标题翻译：用于下流式加氢反应器的VORTEX型混合装置
公开(公告)号：US20130064740A1
公开(公告)日：2013-03-14
申请号：US13663570
申请日：2012-10-30
申请人： Craig Boyak , Abdenour Kemoun , Ralph Evans Killen , Krishniah Parimi , Steven Xuqi Song
发明人： Craig Boyak , Abdenour Kemoun , Ralph Evans Killen , Krishniah Parimi , Steven Xuqi Song
IPC分类号： B01F3/04 , B01J8/04
CPC分类号： B01F3/04113 , B01F3/04503 , B01F5/0057 , B01J8/04 , B01J8/0453 , B01J8/0492 , B01J2208/00884 , B01J2208/00938
摘要： The present invention is directed to a vortex-type mixing device for a down-flow hydroprocessing reactor. In particular, the device improves the effectiveness of an existing mixing volume in mixing the gas phase and liquid phase of two-phase systems. According to the present invention, the mixing device helps create a highly arcuate flow to incoming effluents and a high degree of mixing within a constrained interbed space of a hydroprocessing reactor.
摘要翻译：本发明涉及一种用于下流加氢反应器的涡流式混合装置。特别地，该装置提高了混合两相系统的气相和液相时的现有混合体积的有效性。根据本发明，混合装置有助于在加氢处理反应器的受限制的间隙空间内为进入的流出物形成高度弧形的流动和高度的混合。

20. 发明授权

US07842262B2 Process and apparatus for separating gas from a multi-phase mixture being recycled in a reactor 有权
标题翻译：用于从反应器中再循环的多相混合物中分离气体的方法和装置
公开(公告)号：US07842262B2
公开(公告)日：2010-11-30
申请号：US12002772
申请日：2007-12-19
申请人： Abdenour Kemoun
发明人： Abdenour Kemoun
IPC分类号： C10G45/00
CPC分类号： C10G49/12 , B01J8/004 , B01J8/008 , B01J8/226 , B01J8/228 , B01J2208/00752
摘要： A reactor in which a multi-phase mixture, including gas and a catalyst slurry or liquid, is to be conducted. The reactor includes a reaction chamber having a substantially unencumbered center portion through which the multi-phase mixture is conducted upwardly. A downcomer arrangement is disposed laterally outwardly of the center portion and adjacent to an inner surface of the reaction chamber. An external pump communicates with a lower portion of the reaction chamber for circulating components of the mixture downward from an upper end of the downcomer arrangement to a lower end thereof. A collection chamber is disposed below the reaction chamber into which the components exiting the downcomer arrangement are introduced and where the gas is separated from the remainder of the components. The separated gas can be reintroduced into the reaction chamber.
摘要翻译：将要进行包括气体和催化剂浆液或液体在内的多相混合物的反应器。反应器包括具有基本上未受阻的中心部分的反应室，多相混合物通过该中心部向上传导。降液装置横向设置在中心部分的外侧并与反应室的内表面相邻。外部泵与反应室的下部连通，用于将混合物的组分从降液管装置的上端向下循环到其下端。收集室设置在反应室下方，离开降液管装置的部件被引入该收集室，并且气体与其余部件分离。分离的气体可以重新引入反应室。

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