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11. 发明授权

US08092709B2 Stabilizers for the stabilization of unsaturated hydrocarbon-based precursor 有权
标题翻译：用于稳定不饱和烃类前体的稳定剂
公开(公告)号：US08092709B2
公开(公告)日：2012-01-10
申请号：US13109488
申请日：2011-05-17
申请人： Steven Gerard Mayorga , Kelly Ann Chandler
发明人： Steven Gerard Mayorga , Kelly Ann Chandler
IPC分类号： C09K3/00 , C09K15/00 , C09K15/16 , C09K15/22 , C07D211/00 , C07D295/00
CPC分类号： C07C7/20 , C07C2602/42 , C07C13/39
摘要： A stabilized composition consists essentially of unsaturated hydrocarbon-based materials, and a stabilizer selected from the group consisting of a hydroxybenzophenone and a nitroxyl radical based stabilizer. A method for stabilizing unsaturated hydrocarbon-based precursor material against the polymerization comprises providing a stabilizer selected from the group consisting of a hydroxybenzophenone and a nitroxyl radical based stabilizer.
摘要翻译：稳定化的组合物基本上由不饱和烃基材料和选自羟基二苯甲酮和基于硝酰基的稳定剂组成的组中的稳定剂组成。稳定不饱和烃基前体材料以抗聚合的方法包括提供选自羟基二苯甲酮和基于硝酰基的稳定剂的稳定剂。

12. 发明申请

US20100018849A1 Removal of Trace Arsenic Impurities from Triethylphosphate (TEPO) 失效
标题翻译：从三乙基磷酸盐（TEPO）去除痕量砷杂质
公开(公告)号：US20100018849A1
公开(公告)日：2010-01-28
申请号：US12179979
申请日：2008-07-25
申请人： Steven Gerard Mayorga , Heather Regina Bowen , Kelly Ann Chandler
发明人： Steven Gerard Mayorga , Heather Regina Bowen , Kelly Ann Chandler
IPC分类号： B01D3/34
CPC分类号： C07F9/11 , C07F9/025
摘要： A method of removing trace levels of arsenic-containing impurities from raw triethylphosphate (TEPO) is disclosed. The method uses adsorption, or adsorption followed by a flash distillation. The method comprises contacting raw triethylphosphate (TEPO) with an adsorbent which selectively adsorbs the arsenic-containing impurities in the raw triethylphosphate (TEPO). The adsorbent is a base promoted alumina containing adsorbent represented by a formula: ZxWy; where x is the weight percentage of Z in the adsorbent ranging from 30% to 99.999%; y is the weight percentage of W in the adsorbent, and x+y=100%; Z is selected from the group consisting of alumina (Al2O3), magnesium-alumina based layered double hydroxide (MgO—Al2O3), alumina-zeolite, and mixtures thereof; and W is selected from the group consisting of at least one basic metal oxide, at least one basic metal carbonate, and mixtures thereof. The method will result in a final triethylphosphate (TEPO) with a few ppb to less than 1 ppb arsenic containing impurities.
摘要翻译：公开了从原料三乙基磷酸盐（TEPO）中除去痕量砷含量杂质的方法。该方法使用吸附或吸附，然后进行快速蒸馏。该方法包括将原料三乙基磷酸盐（TEPO）与选择性吸附原料三乙基磷酸盐（TEPO）中的含砷杂质的吸附剂接触。吸附剂是由式ZxWy表示的碱性促进氧化铝的吸附剂。其中x是吸附剂中Z的重量百分数，范围为30％至99.999％; y是吸附剂中W的重量百分数，x + y = 100％; Z选自氧化铝（Al2O3），镁 - 氧化铝基层状双氢氧化物（MgO-Al 2 O 3），氧化铝 - 沸石及其混合物; W选自至少一种碱金属氧化物，至少一种碱金属碳酸盐及其混合物。该方法将产生具有几ppb至少于1ppb含砷杂质的最终三乙基磷酸酯（TEPO）。

13. 发明申请

US20090159844A1 Stabilizers for the Stabilization of Unsaturated Hydrocarbon-based Precursor 有权
公开(公告)号：US20090159844A1
公开(公告)日：2009-06-25
申请号：US12128381
申请日：2008-05-28
申请人： Steven Gerard Mayorga , Kelly Ann Chandler , Mary Kathryn Haas , Mark Leonard O'Neill , Dino Sinatore
发明人： Steven Gerard Mayorga , Kelly Ann Chandler , Mary Kathryn Haas , Mark Leonard O'Neill , Dino Sinatore
IPC分类号： C09K3/00
CPC分类号： C07C7/20 , C07C2602/42 , C07C13/39
摘要： A stabilized composition consists essentially of unsaturated hydrocarbon-based materials, and a stabilizer selected from the group consisting of a hydroxybenzophenone and a nitroxyl radical based stabilizer.A stabilized composition consists essentially of unsaturated hydrocarbon-based materials, at least one polar liquid and a stabilizer selected from the group consisting of a hydroxybenzophenone, a nitroxyl radical based stabilizer and a hydroquinone based stabilizer.A method for stabilizing unsaturated hydrocarbon-based precursor material against the polymerization comprises providing a stabilizer selected from the group consisting of a hydroxybenzophenone and a nitroxyl radical based stabilizer.A method for stabilizing a mixture of unsaturated hydrocarbon-based precursor material with at lease one polar liquid against the polymerization comprises adding to the mixture, a stabilizer selected from the group consisting of a hydroxybenzophenone and a nitroxyl radical based stabilizer.

14. 发明授权

US08173213B2 Process stability of NBDE using substituted phenol stabilizers 有权
标题翻译：使用取代苯酚稳定剂的NBDE工艺稳定性
公开(公告)号：US08173213B2
公开(公告)日：2012-05-08
申请号：US12470002
申请日：2009-05-21
申请人： Steven Gerard Mayorga , Mary Kathryn Haas , Mark Leonard O'Neill , Dino Sinatore
发明人： Steven Gerard Mayorga , Mary Kathryn Haas , Mark Leonard O'Neill , Dino Sinatore
IPC分类号： C09K15/08 , C10L1/183 , C23C16/40 , H01L21/00
CPC分类号： C07C7/20 , C07C13/64 , C07C39/06 , C07C13/00 , C07C15/00
摘要： A stabilized cyclic alkene composition comprising one or more cyclic alkenes, and at least one stabilizer compound having the Formula (I), R1,R2,R3,R4,R5(C6)OH Formula (I) wherein R′ through R5 can each independently be H, OH, C1-C8 linear, branched, or cyclic alkyl, C1-C8 linear, branched, or cyclic alkoxy or substituted or unsubstituted aryl, and wherein the stabilizer compound is present in an amount greater than 200 ppm up to 20,000 ppm and has a boiling point lower than 265° C. A method for forming a layer of carbon-doped silicon oxide on a substrate, which uses the stabilized alkene composition and a silicon containing compound.
摘要翻译：包含一种或多种环状烯烃的稳定化环烯烃组合物和至少一种具有式（I），R 1，R 2，R 3，R 4，R 5（C 6）OH式（I）的稳定剂化合物，其中R'至R 5可各自独立地是H，OH，C1-C8直链，支链或环状烷基，C1-C8直链，支链或环状烷氧基或取代或未取代的芳基，其中稳定剂化合物的存在量大于200ppm至高达20,000ppm 并且具有低于265℃的沸点。使用稳定的烯烃组合物和含硅化合物在基材上形成碳掺杂氧化硅层的方法。

15. 发明申请

US20110295033A1 LOW-IMPURITY ORGANOSILICON PRODUCT AS PRECURSOR FOR CVD 有权
标题翻译：低成本有机硅产品作为CVD的前身
公开(公告)号：US20110295033A1
公开(公告)日：2011-12-01
申请号：US13205015
申请日：2011-08-08
申请人： Steven Gerard Mayorga , Mark Leonard O'Neill , Kelly A. Chandler
发明人： Steven Gerard Mayorga , Mark Leonard O'Neill , Kelly A. Chandler
IPC分类号： C07F7/02
CPC分类号： C07F7/20 , C07F7/1804
摘要： The present invention provides an organosilicon composition comprising diethoxymethylsilane, a concentration of dissolved residual chloride, and a concentration of dissolved residual chloride scavenger that does not yield unwanted chloride salt precipitate when combined with another composition comprising diethoxymethylsilane.
摘要翻译：本发明提供一种包含二乙氧基甲基硅烷的有机硅组合物，溶解的残留氯化物的浓度以及溶解的残余氯化物清除剂的浓度，当与包含二乙氧基甲基硅烷的另一种组合物组合时，其不产生不需要的氯化物盐沉淀物。

16. 发明授权

US08039658B2 Removal of trace arsenic impurities from triethylphosphate (TEPO) 失效
标题翻译：从磷酸三乙酯（TEPO）去除痕量砷杂质
公开(公告)号：US08039658B2
公开(公告)日：2011-10-18
申请号：US12179979
申请日：2008-07-25
申请人： Steven Gerard Mayorga , Heather Regina Bowen , Kelly Ann Chandler
发明人： Steven Gerard Mayorga , Heather Regina Bowen , Kelly Ann Chandler
IPC分类号： C07F9/09
CPC分类号： C07F9/11 , C07F9/025
摘要： A method of removing trace levels of arsenic-containing impurities from raw triethylphosphate (TEPO) is disclosed. The method uses adsorption, or adsorption followed by a flash distillation. The method comprises contacting raw triethylphosphate (TEPO) with an adsorbent which selectively adsorbs the arsenic-containing impurities in the raw triethylphosphate (TEPO). The adsorbent is a base promoted alumina containing adsorbent represented by a formula: ZxWy; where x is the weight percentage of Z in the adsorbent ranging from 30% to 99.999%; y is the weight percentage of W in the adsorbent, and x+y=100%; Z is selected from the group consisting of alumina (Al2O3), magnesium-alumina based layered double hydroxide (MgO—Al2O3), alumina-zeolite, and mixtures thereof; and W is selected from the group consisting of at least one basic metal oxide, at least one basic metal carbonate, and mixtures thereof. The method will result in a final triethylphosphate (TEPO) with a few ppb to less than 1 ppb arsenic containing impurities.
摘要翻译：公开了从原料三乙基磷酸盐（TEPO）中除去痕量砷含量杂质的方法。该方法使用吸附或吸附，然后进行快速蒸馏。该方法包括将原料三乙基磷酸盐（TEPO）与选择性吸附原料三乙基磷酸盐（TEPO）中的含砷杂质的吸附剂接触。吸附剂是由式ZxWy表示的碱性促进氧化铝的吸附剂。其中x是吸附剂中Z的重量百分数，范围为30％至99.999％; y是吸附剂中W的重量百分数，x + y = 100％; Z选自氧化铝（Al2O3），镁 - 氧化铝基层状双氢氧化物（MgO-Al 2 O 3），氧化铝 - 沸石及其混合物; W选自至少一种碱金属氧化物，至少一种碱金属碳酸盐及其混合物。该方法将产生具有几ppb至少于1ppb含砷杂质的最终三乙基磷酸酯（TEPO）。

17. 发明授权

US07968001B2 Stabilizers for the stabilization of unsaturated hydrocarbon-based precursor 有权
标题翻译：用于稳定不饱和烃类前体的稳定剂
公开(公告)号：US07968001B2
公开(公告)日：2011-06-28
申请号：US12038409
申请日：2008-02-27
申请人： Steven Gerard Mayorga , Kelly Ann Chandler
发明人： Steven Gerard Mayorga , Kelly Ann Chandler
IPC分类号： C09K3/00 , C09K15/00 , C09K15/16 , C09K15/22 , C07D211/00 , C07D295/00
CPC分类号： C07C7/20 , C07C2602/42 , C07C13/39
摘要： A stabilized composition consists essentially of unsaturated hydrocarbon-based materials, and a stabilizer selected from the group consisting of hydroxybenzophenone and a nitroxyl radical based stabilizer. A method for stabilizing unsaturated hydrocarbon-based precursor material against the polymerization comprises providing a stabilizer selected from the group consisting of a hydroxybenzophenone and a nitroxyl radical based stabilizer.
摘要翻译：稳定化的组合物基本上由不饱和烃基材料和选自羟基二苯甲酮和基于硝酰基的稳定剂组成的组中的稳定剂组成。稳定不饱和烃基前体材料以抗聚合的方法包括提供选自羟基二苯甲酮和基于硝酰基的稳定剂的稳定剂。

18. 发明申请

US20090297711A1 Process Stability of NBDE Using Substituted Phenol Stabilizers 有权
标题翻译：使用取代苯酚稳定剂的NBDE工艺稳定性
公开(公告)号：US20090297711A1
公开(公告)日：2009-12-03
申请号：US12470002
申请日：2009-05-21
申请人： Steven Gerard Mayorga , Mary Kathryn Haas , Mark Leonard O'Neill , Dino Sinatore
发明人： Steven Gerard Mayorga , Mary Kathryn Haas , Mark Leonard O'Neill , Dino Sinatore
IPC分类号： C23C16/22 , C07C13/39 , B32B9/00
CPC分类号： C07C7/20 , C07C13/64 , C07C39/06 , C07C13/00 , C07C15/00
摘要： A stabilized cyclic alkene composition comprising one or more cyclic alkenes, and at least one stabilizer compound having the Formula (I), R1,R2,R3,R4,R5(C6)OH Formula (I) wherein R1 through R5 can each independently be H, OH, C1-C8 linear, branched, or cyclic alkyl, C1-C8 linear, branched, or cyclic alkoxy or substituted or unsubstituted aryl, and wherein the stabilizer compound is present in an amount greater than 200 ppm up to 20,000 ppm and has a boiling point lower than 265° C.A method for forming a layer of carbon-doped silicon oxide on a substrate, which uses the stabilized alkene composition and a silicon containing compound.
摘要翻译：包含一种或多种环状烯烃的稳定化环烯烃组合物和至少一种具有式（I），R1，R2，R3，R4，R5（C6）OH式（Ⅰ）的稳定剂化合物，其中R1至R5各自独立地为 H，OH，C1-C8直链，支链或环状烷基，C1-C8直链，支链或环状烷氧基或取代或未取代的芳基，其中稳定剂化合物的存在量大于200ppm至20,000ppm，具有低于265℃的沸点。在使用稳定的烯烃组合物和含硅化合物的基底上形成碳掺杂氧化硅层的方法。

19. 发明授权

US08440099B2 Stabilizers for the stabilization of unsaturated hydrocarbon-based precursor 有权
标题翻译：用于稳定不饱和烃类前体的稳定剂
公开(公告)号：US08440099B2
公开(公告)日：2013-05-14
申请号：US12128381
申请日：2008-05-28
申请人： Steven Gerard Mayorga , Kelly Ann Chandler , Mary Kathryn Haas , Mark Leonard O'Neill , Dino Sinatore
发明人： Steven Gerard Mayorga , Kelly Ann Chandler , Mary Kathryn Haas , Mark Leonard O'Neill , Dino Sinatore
IPC分类号： C09K3/00 , C09K15/20
CPC分类号： C07C7/20 , C07C2602/42 , C07C13/39
摘要： A stabilized composition consists essentially of unsaturated hydrocarbon-based materials, and a stabilizer selected from the group consisting of a hydroxybenzophenone and a nitroxyl radical based stabilizer.A stabilized composition consists essentially of unsaturated hydrocarbon-based materials, at least one polar liquid and a stabilizer selected from the group consisting of a hydroxybenzophenone, a nitroxyl radical based stabilizer and a hydroquinone based stabilizer.A method for stabilizing unsaturated hydrocarbon-based precursor material against the polymerization comprises providing a stabilizer selected from the group consisting of a hydroxybenzophenone and a nitroxyl radical based stabilizer.A method for stabilizing a mixture of unsaturated hydrocarbon-based precursor material with at lease one polar liquid against the polymerization comprises adding to the mixture, a stabilizer selected from the group consisting of a hydroxybenzophenone and a nitroxyl radical based stabilizer.
摘要翻译：稳定化的组合物基本上由不饱和烃基材料和选自羟基二苯甲酮和基于硝酰基的稳定剂组成的组中的稳定剂组成。稳定化的组合物基本上由不饱和烃基材料，至少一种极性液体和选自羟基二苯甲酮，基于硝酰基的稳定剂和氢醌基稳定剂的稳定剂组成。稳定不饱和烃基前体材料以抗聚合的方法包括提供选自羟基二苯甲酮和基于硝酰基的稳定剂的稳定剂。用于使不饱和烃类前体材料与至少一种极性液体的混合物与聚合反应的方法包括向混合物中加入选自羟基二苯甲酮和基于硝酰基的稳定剂的稳定剂。

20. 发明授权

US08329933B2 Low-impurity organosilicon product as precursor for CVD 有权
标题翻译：低杂质有机硅产品作为CVD的前体
公开(公告)号：US08329933B2
公开(公告)日：2012-12-11
申请号：US13205015
申请日：2011-08-08
申请人： Steven Gerard Mayorga , Mark Leonard O'Neill , Kelly Ann Chandler
发明人： Steven Gerard Mayorga , Mark Leonard O'Neill , Kelly Ann Chandler
IPC分类号： C07F7/04
CPC分类号： C07F7/20 , C07F7/1804
摘要： The present invention provides an organosilicon composition comprising diethoxymethylsilane, a concentration of dissolved residual chloride, and a concentration of dissolved residual chloride scavenger that does not yield unwanted chloride salt precipitate when combined with another composition comprising diethoxymethylsilane.
摘要翻译：本发明提供一种包含二乙氧基甲基硅烷的有机硅组合物，溶解的残留氯化物的浓度以及溶解的残余氯化物清除剂的浓度，当与包含二乙氧基甲基硅烷的另一种组合物组合时，其不产生不需要的氯化物盐沉淀物。

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