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11. 发明申请

WO2015067583A1 PROCESS FOR PREPARING A HYDROTREATING CATALYST 审中-公开
标题翻译：制备氢化催化剂的方法
公开(公告)号：WO2015067583A1
公开(公告)日：2015-05-14
申请号：PCT/EP2014/073637
申请日：2014-11-04
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , SHELL OIL COMPANY
发明人： WINTER, Ferry , VAN WELSENES, Jan Arend , RIGUTTO, Marcello Stefano , GILTAY, Patricia Johanna Anne Maria , VAN VLAANDEREN, Johannes Jacobus Maria , AZGHAY, Ali
IPC分类号： B01J37/20 , B01J37/00 , B01J37/02 , B01J27/19 , C10G45/08 , B01J23/883 , B01J37/28 , B01J35/10 , B01J35/00 , B01J31/04
CPC分类号： B01J27/19 , B01J21/04 , B01J23/883 , B01J31/0202 , B01J31/04 , B01J35/0006 , B01J35/0026 , B01J35/026 , B01J35/1019 , B01J35/1061 , B01J37/0018 , B01J37/0201 , B01J37/0203 , B01J37/0205 , B01J37/0207 , B01J37/0215 , B01J37/0236 , B01J37/024 , B01J37/08 , B01J37/086 , B01J37/088 , B01J37/20 , B01J37/28 , B01J2523/00 , C10G45/08 , B01J2523/31 , B01J2523/51 , B01J2523/68 , B01J2523/845 , B01J2523/847
摘要： Process for preparing a hydrotreating catalyst comprising of from 5 wt% to 50 wt% of molybdenum, of from 0.5 wt% to 20 wt% of cobalt, and of from 0 to 5 wt% of phosphorus, all based on total dry weight of catalyst, which process comprises (a) treating a nickel containing carrier with molybdenum, cobalt and of from 1to 60 %wt of gluconic acid, based on weight of carrier, and optionally phosphorus, (b) optionally drying the treated carrier at a temperature of from 40 to 200 °C, and (c) calcining the treated and optionally dried carrier at a temperature of from 200 to 650 ºC to obtain the calcined treated carrier.
摘要翻译：制备加氢处理催化剂的方法，所述加氢处理催化剂包含5重量％至50重量％的钼，0.5重量％至20重量％的钴和0至5重量％的磷，均基于催化剂的总干重，该方法包括（a）基于载体的重量和任选的磷，用钼，钴和1至60重量％的葡萄糖酸处理含镍载体，（b）任选地将处理的载体在 40至200℃，和（c）在200至650℃的温度下煅烧经处理和任选干燥的载体，以获得经煅烧处理的载体。

12. 发明申请

WO2013092806A1 PROCESS FOR PREPARING HYDROCRACKING CATALYST 审中-公开
标题翻译：制备水解催化剂的方法
公开(公告)号：WO2013092806A1
公开(公告)日：2013-06-27
申请号：PCT/EP2012/076292
申请日：2012-12-20
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , SHELL OIL COMPANY
发明人： OUWEHAND, Cornelis , RIGUTTO, Marcello Stefano , VAN WELSENES, Jan Arend
IPC分类号： B01J21/12 , B01J23/883 , B01J37/02 , C10G47/12
CPC分类号： B01J31/04 , B01J21/12 , B01J23/883 , B01J23/888 , B01J27/049 , B01J27/19 , B01J29/061 , B01J31/0204 , B01J31/34 , B01J35/023 , B01J37/0036 , B01J37/0203 , B01J37/0236 , B01J37/18 , B01J37/20 , B01J37/32 , B01J2229/42 , C10G47/12 , C10G65/00
摘要： Process for preparing a sulphided hydrocracking catalyst comprising the steps of (a) treating an amorphous silica alumina carrier with one or more Group VIB metal components, one or more Group VIII metal components and a C 3 -C 12 polyhydric compound, (b) drying the treated catalyst carrier at a temperature of at most 200 °C to form an impregnated carrier, and (c) sulphiding the impregnated carrier to obtain a sulphided catalyst.
摘要翻译：制备硫化加氢裂化催化剂的方法，包括以下步骤：（a）用一种或多种VIB族金属组分，一种或多种VIII族金属组分和C 3 -C 12多羟基化合物处理无定形二氧化硅氧化铝载体，（b）催化剂载体在至多200℃的温度下形成浸渍的载体，和（c）硫化浸渍的载体以获得硫化催化剂。

13. 发明申请

WO2013090534A1 A TITANIA-BOUND ZSM-12 ZEOLITE COMPOSITION AND METHOD OF MAKING AND USING SUCH COMPOSITION 审中-公开
标题翻译： TITANIA-BOUND ZSM-12沸石组合物及其制备和使用这种组合物的方法
公开(公告)号：WO2013090534A1
公开(公告)日：2013-06-20
申请号：PCT/US2012/069438
申请日：2012-12-13
申请人： SHELL OIL COMPANY , SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V.
发明人： RIGUTTO, Marcello Stefano , JONGKIND, Hermanus , PELGRIM, Bart , GEERINCK, Peter
IPC分类号： B01J37/00 , B01J37/02 , B01J37/04 , C10G73/02 , B01J21/06 , B01J29/70
CPC分类号： B01J29/06 , B01J21/063 , B01J23/44 , B01J29/7034 , B01J29/7469 , B01J35/0006 , B01J35/0026 , B01J35/023 , B01J35/1014 , B01J35/1023 , B01J37/0009 , B01J37/0201 , B01J2229/16 , B01J2229/37 , B01J2229/42 , C10G47/20
摘要： Presented is a composition useful in the catalytic dewaxing of a waxy hydrocarbon feedstock. The composition includes a mixture of ZSM-12 zeolite and titania and may further include a noble metal. The ZSM-12 zeolite preferably has a high silica-to-alumina ratio within its framework. The mixture may be dealuminated either by acid leaching using a fluorosilicate salt or by steam treating.
摘要翻译：提出了可用于蜡质烃原料的催化脱蜡的组合物。组合物包括ZSM-12沸石和二氧化钛的混合物，并且还可以包括贵金属。在其框架内，ZSM-12沸石优选具有高的二氧化硅与氧化铝的比例。混合物可以通过使用氟硅酸盐的酸浸或通过蒸汽处理脱铝。

14. 发明申请

WO2021185721A1 A METHOD OF PREPARING A HYDROCRACKING CATALYST 审中-公开
公开(公告)号：WO2021185721A1
公开(公告)日：2021-09-23
申请号：PCT/EP2021/056455
申请日：2021-03-15
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , SHELL OIL COMPANY
发明人： COOPER, David Allen , DEN BREEJEN, Johan Peter , HUGHES, James , OUWEHAND, Cornelis , RIGUTTO, Marcello Stefano
IPC分类号： B01J29/08 , B01J29/16 , B01J37/00 , B01J37/08 , B01J35/10 , C10G47/20 , B01J35/00 , B01J37/02 , B01J35/02 , B01J37/20
摘要： The present invention provides a method of preparing a supported catalyst, preferably a hydrocracking catalyst, the method at least comprising the steps of: a) providing a zeolite Y having a bulk silica to alumina ratio (SAR) of at least 10; b) mixing the zeolite Y provided in step a) with a base, water and a surfactant, thereby obtaining a slurry of the zeolite Y; c) reducing the water content of the slurry obtained in step b) thereby obtaining solids with reduced water content, wherein the reducing of the water content in step c) involves the addition of a binder; d) shaping the solids with reduced water content obtained in step c) thereby obtaining a shaped catalyst carrier; e) calcining the shaped catalyst carrier obtained in step d) at a temperature above 300°C in the presence of the surfactant of step b), thereby obtaining a calcined catalyst carrier; f) impregnating the catalyst carrier calcined in step e) with a hydrogenation component thereby obtaining a supported catalyst; wherein no heat treatment at a temperature of above 500°C takes place between the mixing of step b) and the shaping of step d).

15. 发明申请

WO2015028677A1 PROCESS FOR PREPARING A CATALYST, CATALYST OBTAINED BY SUCH PROCESS, AND USE OF SUCH CATALYST 审中-公开
标题翻译：制备催化剂，通过这种方法获得的催化剂的方法，以及这些催化剂的使用
公开(公告)号：WO2015028677A1
公开(公告)日：2015-03-05
申请号：PCT/EP2014/068563
申请日：2014-09-02
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , SHELL OIL COMPANY
发明人： AZGHAY, Ali , ESPINOSA ALONSO, Leticia , FRANSSEN, Nicole Maria Gerarda , RIGUTTO, Marcello Stefano , SCHAVERIEN, Colin John
IPC分类号： B01J23/755 , B01J37/02 , C10G1/00 , C10G3/00
CPC分类号： B01J23/755 , B01J21/08 , B01J35/1014 , B01J35/1019 , B01J37/0018 , B01J37/0045 , B01J37/02 , B01J37/03 , C10G3/44 , C10G3/46 , C10G3/50 , C10G2300/1011 , Y02P30/20
摘要： Process for converting a biomass-derived pyrolysis oil comprising the following steps: i) preparing a catalyst, preferably containing one or more Group VIII metals in an amount of equal to or more than 30wt%, based on the total weight of the catalyst, by a method including - mixing one or more Group VIII metal components; a waterborne refractory oxide component comprising a refractory oxide selected from the Group consisting of titania, zirconia, silica and mixtures thereof; and a water-soluble base; in an aqueous solvent to prepare an metal-containing aqueous mixture; and - subjecting the metal-containing aqueous mixture to precipitation conditions; and ii) contacting a feed containing the biomass-derived pyrolysis oil with hydrogen at a temperature in the range from 50°C to 350°C in the presence of the catalyst.
摘要翻译：用于转化生物质衍生的热解油的方法，包括以下步骤：i）制备催化剂，优选含有基于催化剂总重量等于或大于30重量％的一种或多种第VIII族金属，通过一种方法，包括 - 混合一种或多种VIII族金属组分; 包含选自二氧化钛，氧化锆，二氧化硅及其混合物的耐火氧化物的水性难熔氧化物组分; 和水溶性碱; 在水性溶剂中制备含金属的水性混合物; 和 - 对含金属的含水混合物进行沉淀条件; 和ii）在催化剂存在下，将含有生物质衍生的热解油的进料与氢气在50℃至350℃的温度下接触。

16. 发明申请

WO2014001550A1 PROCESS TO PREPARE MIDDLE DISTILLATES AND BASE OILS 审中-公开
标题翻译：制备中间馏分和基础油的方法
公开(公告)号：WO2014001550A1
公开(公告)日：2014-01-03
申请号：PCT/EP2013/063734
申请日：2013-06-28
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , SHELL OIL COMPANY
发明人： KIEFFER, Eduard Philip , RIGUTTO, Marcello Stefano , SIETSMA, Jelle Rudolf Anne
IPC分类号： C10G65/12 , C10G65/04 , C10G73/02 , C10G73/44 , C10G45/62 , C10G45/64 , C10L1/08
CPC分类号： C10G67/02 , C10G45/62 , C10G45/64 , C10G65/00 , C10G65/043 , C10G65/12 , C10G65/16 , C10G73/02 , C10G73/44 , C10G2300/1022 , C10G2300/301
摘要： The present invention provides a process to prepare a first middle distillates fraction, a second middle distillates fraction and one or more base oils, which process at least comprises the following steps: (a) providing a Fischer-Tropsch product stream; (b) separating the Fischer-Tropsch product stream of step (a), thereby obtaining at least a low boiling fraction, boiling below a temperature in the range of from 300 to 450°C, and a high boiling fraction, boiling above a temperature in the range of from 300 to 450°C; (c) subjecting the high boiling fraction of step (b) to a hydrocracking/hydroisomerization step to obtain an at least partially isomerised product stream; (d) separating the product stream of step (c), thereby obtaining a first middle distillates fraction and a residual fraction, wherein the residual fraction has a T10wt.% boiling point of between 200 and 450°C; (e) dewaxing the low boiling fraction of step (b) to obtain a second middle distillates fraction; and f) dewaxing the residual fraction of step (d) to obtain one or more base oils.
摘要翻译：本发明提供了制备第一中间馏分馏分，第二中间馏分和一种或多种基础油的方法，该方法至少包括以下步骤：（a）提供费 - 托产物流; （b）分离步骤（a）的费 - 托产物流，从而得到至少沸点低于300-450℃的沸点，沸点高于沸点在300〜450℃的范围内; （c）使步骤（b）的高沸点馏分进行加氢裂化/加氢异构化步骤以获得至少部分异构化的产物流; （d）分离步骤（c）的产物流，从而获得第一中间馏分和残余馏分，其中残余馏分的T10重量％沸点在200-450℃之间; （e）将步骤（b）的低沸点馏分脱蜡得到第二中间馏分; 和f）使步骤（d）的残余馏分脱蜡得到一种或多种基础油。

17. 发明申请

WO2009065878A3 METHOD FOR THE START-UP OF A CATALYTIC PROCESS 审中-公开
公开(公告)号：WO2009065878A3
公开(公告)日：2009-05-28
申请号：PCT/EP2008/065877
申请日：2008-11-19
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , DOMOKOS, Lászlo , JONGKIND, Hermanus , VAN DER LAAN, Pieter , RIGUTTO, Marcello Stefano
发明人： DOMOKOS, Lászlo , JONGKIND, Hermanus , VAN DER LAAN, Pieter , RIGUTTO, Marcello Stefano
IPC分类号： C10G49/24 , C10G45/08 , B01J37/03
摘要： The present invention relates to a process for starting up a hydrotreating process using a bulk metal catalyst, said process comprising the steps of: i) providing a hydrocarbon feed stream containing less than 100 ppmw nitrogen-containing species; ii) adding a nitrogen-containing compound to said hydrocarbon feed stream; and iii) contacting the resultant feed stream with the bulk metal catalyst in the presence of hydrogen and a sulfur-containing species. The present invention also relates to a process for hydrotreating a hydrocarbon feedstock, said process comprising the steps of : i) providing a hydrocarbon feed stream containing less than 100 ppmw nitrogen-containing species; ii) adding a nitrogen-containing compound to said hydrocarbon feed stream; iii) contacting the resultant feed stream with a bulk metal catalyst in the presence of hydrogen and a sulfur-containing species; and iv) subsequently contacting the resultant bulk metal catalyst with the hydrocarbon feedstock in the presence of hydrogen.

18. 发明申请

WO2014173878A1 PROCESS FOR PREPARING A SULPHIDED CATALYST 审中-公开
标题翻译：制备硫化催化剂的方法
公开(公告)号：WO2014173878A1
公开(公告)日：2014-10-30
申请号：PCT/EP2014/058103
申请日：2014-04-22
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , SHELL OIL COMPANY
发明人： AZGHAY, Ali , RIGUTTO, Marcello Stefano
IPC分类号： B01J37/20 , B01J23/85 , B01J27/049 , B01J27/051 , C10G45/08
CPC分类号： B01J27/19 , B01J37/0213 , B01J37/0236 , B01J37/20 , C10G45/08
摘要： The invention provides a process for preparing a sulphided catalyst comprising the steps of (a) treating a catalyst carrier with one or more Group VIB metal components, one or more Group VIII metal components and a glycolic acid ethoxylate ether compound according to the formula (I) R-(CH 2 ) x –CH 2 –O-[-(CH 2 ) 2 -O-] m -CH 2 –COOH (I) wherein R is a hydrocarbyl group containing of from 5 to 20 carbon atoms,x is in the range of from 1 to 15, and m is in the range of from 1 to 10, and wherein the molar ratio of compound (I) to the Group VIB and Group VIII metal content is at least 0.01:1to 1:0.01;(b)drying the treated catalyst carrier at a temperature of at most 200 °C to form a dried impregnated carrier; and (c) sulphiding the dried impregnated carrier to obtain a sulphided catalyst.
摘要翻译：本发明提供了一种制备硫化催化剂的方法，包括以下步骤：（a）用一种或多种VIB族金属组分，一种或多种VIII族金属组分和根据式（I）的乙醇酸乙氧基化醚化合物处理催化剂载体）R-（CH 2）x -CH 2 -O - [ - （CH 2）2 -O-] m -CH 2 -COOH（I）其中R是含有5至20个碳原子的烃基，x在为1〜10，m为1〜10，化合物（I）与VIB族和VIII族金属含量的摩尔比为0.01：1〜1：0.01;（b）在最多200℃的温度下干燥经处理的催化剂载体以形成干燥的浸渍载体; 和（c）硫化干燥的浸渍载体以获得硫化催化剂。

19. 发明申请

WO2014154862A1 PROCESS FOR REJUVENATION OF A USED HYDROTREATING CATALYST 审中-公开
标题翻译：重新使用氢化催化剂的方法
公开(公告)号：WO2014154862A1
公开(公告)日：2014-10-02
申请号：PCT/EP2014/056274
申请日：2014-03-28
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , SHELL OIL COMPANY
发明人： AZGHAY, Ali , GILTAY, Patricia Johanna Anne Maria , RIGUTTO, Marcello Stefano , VAN WELSENES, Arend Jan , WINTER, Ferry
IPC分类号： B01J37/20 , B01J38/00 , B01J38/12 , B01J23/85 , B01J23/88 , B01J23/882 , B01J23/883 , B01J23/888 , B01J27/049 , B01J27/051 , C10G45/08
CPC分类号： B01J38/62 , B01J23/882 , B01J23/94 , B01J27/0515 , B01J37/20 , B01J38/12 , B01J38/48 , C10G45/08 , C10G65/00 , C10G2300/70
摘要： The invention provides a process for rejuvenation of a used hydrotreating catalyst comprising at least 8 %wt of coke and one or more non-noble Group VIII and/or Group VIb metals, which process comprises the steps of: (i) removing coke from the used hydrotreating catalyst; and (ii) treating the catalyst obtained in step (i) with of from 2 to 60 %wt of gluconic acid, based on weight of dry catalyst.
摘要翻译：本发明提供了一种使用的加氢处理催化剂的再生方法，其包含至少8重量％的焦炭和一种或多种非贵金属VIII族和/或VIb族金属，该方法包括以下步骤：（i）使用加氢处理催化剂; 和（ii）以干燥催化剂的重量，用2-60重量％的葡萄糖酸处理步骤（ⅰ）中获得的催化剂。

20. 发明申请

WO2014001552A1 PROCESS TO PREPARE MIDDLE DISTILLATES AND BASE OILS 审中-公开
标题翻译：制备中间馏分和基础油的方法
公开(公告)号：WO2014001552A1
公开(公告)日：2014-01-03
申请号：PCT/EP2013/063738
申请日：2013-06-28
申请人： SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ B.V. , SHELL OIL COMPANY
发明人： KIEFFER, Eduard Philip , RIGUTTO, Marcello Stefano , SIETSMA, Jelle Rudolf Anne
IPC分类号： C10G65/12 , C10G65/04 , C10G73/02 , C10G73/44 , C10G45/62 , C10G45/64 , C10L1/08
CPC分类号： C10G69/00 , C10G2/32 , C10G45/62 , C10G45/64 , C10G65/00 , C10G65/043 , C10G65/12 , C10G73/44 , C10G2300/1022
摘要： The present invention provides a process to prepare a first middle distillates fraction, a second middle distillates fraction, a distillate base oil and a residual base oil, which process at least comprises the following steps: (a) providing a Fischer-Tropsch product stream; (b) separating the Fischer-Tropsch product stream of step (a), thereby obtaining at least a low boiling fraction, boiling below a temperature in the range of from 300 to 450°C, and a high boiling fraction, boiling above a temperature in the range of from 300 to 450°C; (c) subjecting the high boiling fraction of step (b) to a hydrocracking/hydroisomerization step to obtain an at least partially isomerised product stream; (d) separating the product stream of step (c), thereby obtaining a first middle distillates fraction, a heavy distillates fraction and a residual fraction, wherein the residual fraction has a T5 wt. % boiling point of between 400 and 650°C; (e) dewaxing the low boiling fraction of step (b) to obtain a second middle distillates fraction; f) dewaxing the heavy distillates fraction of step (d) to obtain a distillate base oil; and g) dewaxing the residual fraction of step (d) to obtain a residual base oil.
摘要翻译：本发明提供一种制备第一中间馏分馏分，第二中间馏分，馏出物基础油和残余基础油的方法，该方法至少包括以下步骤：（a）提供费 - 托产物流; （b）分离步骤（a）的费 - 托产物流，从而得到至少沸点低于300-450℃的沸点，沸点高于沸点在300〜450℃的范围内; （c）使步骤（b）的高沸点馏分进行加氢裂化/加氢异构化步骤以获得至少部分异构化的产物流; （d）分离步骤（c）的产物流，从而获得第一中间馏分馏分，重馏分馏分和残余馏分，其中残余馏分具有T5wt。沸点在400-650℃之间; （e）将步骤（b）的低沸点馏分脱蜡得到第二中间馏分; f）将步骤（d）的重馏分馏分脱蜡得到馏出物基油; 和g）将步骤（d）的残余馏分脱蜡得到残留的基础油。

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