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11. 发明申请

US20060063952A1 Method for producing aromatic diamine derivative 失效
标题翻译：芳族二胺衍生物的制备方法
公开(公告)号：US20060063952A1
公开(公告)日：2006-03-23
申请号：US10544764
申请日：2004-01-28
申请人： Hisayuki Kawamura , Hiroyuki Matsui , Koji Hirota
发明人： Hisayuki Kawamura , Hiroyuki Matsui , Koji Hirota
IPC分类号： C07C209/08
CPC分类号： C07C209/62 , C07C211/54
摘要： The invention provides a method for efficiently producing an aromatic diamine derivative represented by formula (3) at high yield, the method including reacting an aromatic amide represented by formula (1) with an aromatic halide represented by formula (2): (wherein each of Ar, Ar1 and Ar2 represents a substituted or unsubstituted aryl group or heteroaryl group; Ar3 represents a substituted or unsubstituted arylene group or heteroarylene group; and X represents a halogen atom).
摘要翻译：本发明提供一种以高收率高效制备式（3）表示的芳族二胺衍生物的方法，该方法包括使式（1）表示的芳族酰胺与式（2）表示的芳族卤化物反应：

12. 发明授权

US5894963A Pump mechanism for ejecting liquid 失效
标题翻译：用于喷射液体的泵机构
公开(公告)号：US5894963A
公开(公告)日：1999-04-20
申请号：US969023
申请日：1997-11-12
申请人： Koji Hirota
发明人： Koji Hirota
IPC分类号： B65D83/76 , A61M11/00 , B05B11/00 , G01F11/30
CPC分类号： B05B11/3019
摘要： In a pump mechanism for ejecting liquid, an upper inside wall of a bell-shaped portion which is formed around a lower end of a first piston constitutes a guide surface inclined upward toward an axial hole of the first piston. The guide surface serves to prevent entrapping of air underneath the upper inside wall of the bell-shaped portion, or in an upper part of a metering chamber and stabilize the amount of liquid measured in each successive spraying action.
摘要翻译：在用于喷射液体的泵机构中，围绕第一活塞的下端形成的钟形部分的上内壁构成朝向第一活塞的轴向孔向上倾斜的引导表面。引导表面用于防止在钟形部分的上部内壁或计量室的上部中夹带空气，并稳定在每个连续的喷射动作中测量的液体量。

13. 发明授权

US08778408B2 Antimicrobial substance, method for producing same, and antimicrobial material 有权
标题翻译：抗微生物物质，其制造方法和抗菌材料
公开(公告)号：US08778408B2
公开(公告)日：2014-07-15
申请号：US13985816
申请日：2012-02-13
申请人： Koji Hirota , Hiroshi Mase
发明人： Koji Hirota , Hiroshi Mase
IPC分类号： B32B15/08 , B32B15/12 , C23C14/06 , C23C14/24 , B32B27/06 , B32B29/06
CPC分类号： A01N59/20 , A01N59/16 , A61F13/00059 , A61F2013/00936 , B32B5/022 , B32B2255/02 , B32B2255/205 , B32B2307/7145 , B32B2437/00 , C22C9/02 , C22F1/00 , C22F1/08 , C23C14/06 , C23C14/14 , C23C14/20 , C23C30/00 , Y10T428/2958 , Y10T442/2525
摘要： Provided an antimicrobial substance that includes a base material layer, and a copper-tin alloy layer 5-200 nm in thickness disposed on the base material layer, the copper-tin alloy layer containing copper in an amount of more than 60 atomic percent but not more than 90 atomic percent, and containing tin in an amount of not less than 10 atomic percent but less than 40 atomic percent. The copper-tin alloy layer includes a Cu41Sn11 crystalline phase, and a Cu3Sn crystalline phase. The Q value (Ω/(nm·Cu atomic percent)), which is derived by dividing the sheet resistance (Ω) of the copper-tin alloy layer by the thickness of the copper-tin alloy layer and the copper content (Cu atomic percent), is 1.5×10−4-6.0×10−4.
摘要翻译：提供一种抗菌物质，其包括基材层和设置在基材层上的厚度为5-200nm的铜锡合金层，含有铜原子百分比以上但不含铜的铜 - 锡合金层大于90原子％，含有不小于10原子％但小于40原子％的锡。铜 - 锡合金层包括Cu41Sn11结晶相和Cu 3 Sn结晶相。通过将铜锡合金层的薄层电阻（＆OHgr）除以铜 - 锡合金层的厚度和铜含量得到的Q值（＆OHgr; /（nm·Cu原子％）） Cu原子百分比）为1.5×10-4-6.0×10-4。

14. 发明授权

US07901498B2 Trisazo compound, ink composition, printing method and colored product 有权
标题翻译：三唑烷化合物，油墨组合物，印刷方法和有色产品
公开(公告)号：US07901498B2
公开(公告)日：2011-03-08
申请号：US12734655
申请日：2008-11-25
申请人： Koji Hirota , Takahiko Matsui , Takashi Yoshimoto , Shinsuke Shimizu
发明人： Koji Hirota , Takahiko Matsui , Takashi Yoshimoto , Shinsuke Shimizu
IPC分类号： C09D11/02 , C09B31/16
CPC分类号： C07D471/04 , B41M5/0023 , C09B31/28 , C09D11/328
摘要： The present invention relates to a trisazo compound represented by the following formula (1): wherein, n represents 0 or 1, the group A represents a substituted heterocyclic group, R1 represents a C1-C4 alkyl group which may be substituted or the like, R2 represents a cyano group or the like, R3 and R4 each independently represent a hydrogen atom, a sulfo group or the like, R5 to R7 each independently represent a hydrogen atom, a C1-C4 alkyl group which may be substituted, a C1-C4 alkoxy group which may be substituted or the like, respectively or salt thereof. Said trisazo compound or salt thereof provides a coloring matter compound for black ink and an ink composition thereof where they have high solubility in medium where water is a principal component, their aqueous solution and ink having high concentration is stable even when stored for a long period of time, printed images therewith have very high density, no bronzing is caused on the images printed even with their high concentration solution, and they give black recorded images excellent in fastness, particularly in both light fastness and ozone gas fastness.
摘要翻译：本发明涉及由下式（1）表示的三偶氮化合物：其中，n表示0或1，A组代表取代的杂环基，R 1表示可被取代的C 1 -C 4烷基等， R2表示氰基等，R3和R4各自独立地表示氢原子，磺基等，R5〜R7各自独立地表示氢原子，可以被取代的C1-C4烷基，C1- 分别为可被取代的C 4烷氧基或类似物或其盐。所述三偶氮化合物或其盐提供黑色墨水的着色剂化合物及其油墨组合物，其中以水为主要成分的介质中具有高溶解性，即使长期储存，其浓度高的水溶液和油墨也是稳定的的时间，印刷图像具有非常高的密度，即使在高浓度溶液下印刷的图像也不会导致烫伤，并且它们给出耐光性优异的黑色记录图像，特别是耐光牢度和耐臭氧气体牢度。

15. 发明申请

US20090062545A1 Trisazo Compound, Ink Composition, Recording Method, and Colored Article 有权
标题翻译：三唑类化合物，油墨组合物，记录方法和彩色制品
公开(公告)号：US20090062545A1
公开(公告)日：2009-03-05
申请号：US12087426
申请日：2006-12-28
申请人： Takahiko Matsui , Yoshiyuki Dejima , Takashi Yoshimoto , Ryoutarou Morita , Koji Hirota
发明人： Takahiko Matsui , Yoshiyuki Dejima , Takashi Yoshimoto , Ryoutarou Morita , Koji Hirota
IPC分类号： C07D471/04 , B05D5/00 , C09D11/02
CPC分类号： C07D471/04 , C09B31/28 , C09D11/17 , C09D11/328
摘要： The present invention relates to a trisazo compound represented by the following formula (1) or a salt thereof,The formula (1) (wherein, the group A is a substituted phenyl group, the group B and the group C are substituted para-phenylene groups, R1 represents a C1 to C4 alkyl group (which may be substituted by a carboxy group), a phenyl group (which may be substituted by a sulfo group), or a carboxy group, R2 represents a cyano group, a carbamoyl group or a carboxy group, each of R3 and R4 independently represents a hydrogen atom, a methyl group, a chlorine atom or a sulfo group, respectively) and a water-based black ink composition containing said compound; said compound has high solubility in a medium where the main component is water, its aqueous solution having a high concentration and ink are stable when stored for a long period of time, black-recorded images with it can be provided where both light fastness and ozone gas fastness of the printed images are excellent.
摘要翻译：本发明涉及由下式（1）表示的三偶氮化合物或其盐。式（1）（其中A为取代苯基，B为基团，C为取代对亚苯基基团，R 1表示C 1〜C 4烷基（可以被羧基取代），苯基（可以被磺基取代）或羧基，R 2表示氰基，氨基甲酰基或羧基，R 3和R 4分别独立地表示氢原子，甲基，氯原子或磺基）和含有所述化合物的水性黑色油墨组合物; 所述化合物在主要成分为水的介质中具有高溶解度，其浓度高的水溶液和长时间储存时的油墨稳定，可以提供具有耐光性和臭氧性的黑色记录图像印刷图像的耐气牢度优异。

16. 发明授权

US07223480B2 Metal laminate and etching method therefor 失效
标题翻译：金属层压板及其蚀刻方法
公开(公告)号：US07223480B2
公开(公告)日：2007-05-29
申请号：US10500846
申请日：2003-07-28
申请人： Koji Hirota , Masanao Kobayashi , Minehiro Mori , Naoki Nakazawa
发明人： Koji Hirota , Masanao Kobayashi , Minehiro Mori , Naoki Nakazawa
IPC分类号： B32B15/08 , B32B15/18 , G11B5/00 , G11B21/00 , H01B13/00
CPC分类号： H05K3/002 , G11B5/4833 , H05K1/0346 , H05K1/056 , H05K3/0041 , H05K3/385 , H05K2201/0154 , H05K2203/0315 , H05K2203/163 , Y10T428/12951 , Y10T428/265 , Y10T428/31681
摘要： The present invention relates to a metal laminate which is broadly used for a flexible wiring board or the like and an etching method therefor. In particular, the present invention relates to a metal laminate which includes a layer obtained by laminating a metal layer and an insulating layer, where the insulating layer is subjected to an etching process, wherein, in a surface of the metal layer which is positioned so as to come in contact with the insulating layer, respective concentrations of main metal element and oxygen element constituting the metal layer are measured from the surface of the metal layer towards inside of the metal layer in a time-elapsing manner according to AES (Auger electron spectroscopy) and a value of the thickness of a metal oxide film of the surface of the metal layer measured at a time when atomic concentrations of the main metal element and the oxygen element constituting the metal layer become equal to each other is in a range of at least 0 Å to less than 50 Å.According to the present invention, an etching time of polyimide in the polyimide metal laminate can be calculated and a flexure used for a suspension for a hard disc drive having a high productivity can be provided.
摘要翻译：本发明涉及广泛用于柔性布线板等的金属层压体及其蚀刻方法。特别地，本发明涉及一种金属层压体，其包括通过层压金属层和绝缘层而获得的层，其中绝缘层进行蚀刻处理，其中在该金属层的表面上为了与绝缘层接触，根据AES（俄歇电子学（俄歇电子学），从金属层的表面到金属层的内部）以时间流逝的方式测量构成金属层的主要金属元素和氧元素的各自浓度光谱），并且在构成金属层的主金属元素和氧元素的原子浓度变得相等的时刻测量的金属层的表面的金属氧化物膜的厚度的值在至少从0到小于50。根据本发明，可以计算聚酰亚胺金属层叠体中的聚酰亚胺的蚀刻时间，并且可以提供用于具有高生产率的硬盘驱动器的悬架的挠曲。

17. 发明申请

US20060127685A1 Layered polyimide/metal product 审中-公开
标题翻译：分层聚酰亚胺/金属制品
公开(公告)号：US20060127685A1
公开(公告)日：2006-06-15
申请号：US10544185
申请日：2004-02-09
申请人： Koji Hirota , Naoki Nakazawa , Youichi Kodama
发明人： Koji Hirota , Naoki Nakazawa , Youichi Kodama
IPC分类号： B32B15/08
CPC分类号： B32B27/281 , B32B15/08 , B32B15/18 , B32B15/20 , B32B2250/03 , B32B2274/00 , B32B2307/306 , B32B2307/584 , B32B2307/734 , B32B2457/00 , G11B5/4833 , H05K1/056 , H05K3/002 , Y10T428/31681 , Y10T428/31721
摘要： A polyimide metal laminate comprising a polyimide resin formed on a metal foil, wherein the polyimide resin does not cause the peeling of not less than 100 μm in the polyimide resin and/or at an interface between the polyimide resin and the metal foil when the polyimide resin is heated in an oven at an atmospheric temperature of from 340 to 360° C. for 5 to 10 minutes, the coefficient of humidity expansion at 320 is from 1 to 20 ppm/% RH, and an average value of the etching rate by a 50 wt % aqueous solution of potassium hydroxide at 80° C. is not less than 1.0 μm/min. The polyimide metal laminate can provide good heat resistance, superior dimensional stability and can be etching processed by an aqueous alkaline solution.
摘要翻译：一种聚酰亚胺金属层压体，其包含在金属箔上形成的聚酰亚胺树脂，其中，当聚酰亚胺树脂和/或聚酰亚胺树脂与金属箔之间的界面处，聚酰亚胺树脂不会在聚酰亚胺树脂中和/ 树脂在340〜360℃的大气温度的烘箱中加热5〜10分钟，320℃的湿度膨胀系数为1〜20ppm /％RH，蚀刻速度的平均值为在80℃下氢氧化钾的50重量％水溶液不小于1.0毫姆/分钟。聚酰亚胺金属层压体可以提供良好的耐热性，优异的尺寸稳定性，并且可以通过碱性水溶液进行蚀刻加工。

18. 发明申请

US20050267366A1 Ultrasonic diagnostic apparatus and image processing method 审中-公开
标题翻译：超声波诊断仪及图像处理方法
公开(公告)号：US20050267366A1
公开(公告)日：2005-12-01
申请号：US11117242
申请日：2005-04-27
申请人： Masaru Murashita , Koji Hirota
发明人： Masaru Murashita , Koji Hirota
IPC分类号： A61B8/00 , A61B8/08 , A61B8/14 , G06T1/00 , G06T5/00 , G06T7/00
CPC分类号： G01S15/8993 , A61B6/469 , A61B8/08 , A61B8/14 , A61B8/466 , A61B8/467 , A61B8/469 , A61B8/483 , G01S7/52063
摘要： A three-dimensional image data memory stores three-dimensional image data including that of a imaging target. A digitization processor unit applies a digitizing process to the three-dimensional image data using a first threshold value to extract data corresponding to the target. A user sets a two-dimensional region of interest surrounding a portion in which the extraction of data using the first threshold value is inaccurate and a 3D region-of-interest generator unit generates a three-dimensional region of interest from the two-dimensional region of interest which is set. The digitization processor unit applies a digitizing process using a second threshold value to the three-dimensional image data within the three-dimensional region of interest.
摘要翻译：三维图像数据存储器存储包括成像目标的三维图像数据。数字化处理器单元使用第一阈值将数字化处理应用于三维图像数据，以提取与目标对应的数据。用户设置利用第一阈值的数据提取不准确的部分周围的感兴趣的二维区域，并且3D感兴趣区域生成单元从二维区域生成三维感兴趣区域感兴趣的。数字化处理器单元使用第二阈值对三维感兴趣区域内的三维图像数据进行数字化处理。

19. 发明授权

US5961489A Spray adaptors for spraying collunarium and sprayers employing the spray adaptors 失效
标题翻译：喷雾适配器，用于喷涂使用喷雾适配器的货架和喷雾器
公开(公告)号：US5961489A
公开(公告)日：1999-10-05
申请号：US37387
申请日：1998-03-10
申请人： Koji Hirota
发明人： Koji Hirota
IPC分类号： A61M11/06 , A61M15/08 , A61M5/00
CPC分类号： A61M15/08 , A61M11/007
摘要： A spray adaptor includes a main adaptor element having a pair of spray nozzles and a connector attached to the main adaptor element. A sprayer for spraying collunarium is prepared by fitting the connector of the spray adaptor to an outlet of a syringe. The collunarium discharged from the syringe is guided to the spray nozzles and sprayed into both nostrils at one time.
摘要翻译：喷雾适配器包括具有一对喷嘴和连接到主适配器元件的连接器的主适配器元件。通过将喷雾适配器的连接器装配到注射器的出口来制备用于喷雾霰弹的喷雾器。从注射器排出的is鱼被引导到喷嘴并一次喷射到两个鼻孔中。

20. 发明授权

US09050386B2 Antimicrobial raw material and method for manufacturing the same, and antimicrobial material 有权
标题翻译：抗菌原料及其制造方法及抗菌材料
公开(公告)号：US09050386B2
公开(公告)日：2015-06-09
申请号：US13394907
申请日：2010-09-07
申请人： Hiroshi Mase , Koji Hirota
发明人： Hiroshi Mase , Koji Hirota
IPC分类号： C23C14/06 , B32B15/08 , B32B15/12 , B32B27/06 , B32B29/06 , B32B3/02 , C23C14/24 , A61L15/46 , A61L15/18 , C22C9/02 , C23C14/20 , A01N59/20
CPC分类号： A61L15/46 , A01N59/20 , A61L15/18 , A61L2300/102 , A61L2300/404 , C22C9/02 , C23C14/20 , Y10T428/239 , Y10T428/265 , Y10T428/2958 , Y10T442/2525 , A01N25/10 , A01N25/34 , A01N59/16 , A01N2300/00
摘要： Provided is an antimicrobial raw material having excellent antibacterial and corrosion-resistance properties, which can be directly formed as a film even on a plastic substrate with low heat-resistance or a substrate whereof the color or properties are likely to change due to heat, and this can be achieved at relatively low cost. The antimicrobial raw material is a laminated structure which comprises a substrate layer and a copper-tin alloy layer disposed on the substrate layer, and which has a thickness ranging from 5 nm to 200 nm. The substrate layer is made of resin, natural fiber, or paper, the resin having the deflection temperature under load being 115° C. or lower when measured in accordance with ASTM-D648-56 under a load of 1820 kPa. The copper-tin alloy layer contains over 60 at % but no more than 90 at % of copper and 10 at % or more but less than 40 at % of tin.
摘要翻译：本发明提供抗菌，耐腐蚀性优异的抗微生物原料，即使在耐热性低的塑料基材上也可以直接形成膜或由于热而导致颜色或性质变化的基材，这可以以相对低的成本实现。抗微生物原料是层叠结构，其包含基材层和设置在基材层上的铜锡合金层，其厚度范围为5nm〜200nm。基材层由树脂，天然纤维或纸制成，当根据ASTM-D648-56在1820kPa的负荷下测量时，负载挠曲温度为115℃或更低的树脂。铜 - 锡合金层含有超过60原子％但不超过90原子％的铜和10原子％以上但小于40原子％的锡。

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