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11. 发明申请

US20060247446A1 Multi-metal oxide containing silver, vanadium and a promoter metal and use thereof 失效
标题翻译：含有银，钒和助催化剂金属的多金属氧化物及其用途
公开(公告)号：US20060247446A1
公开(公告)日：2006-11-02
申请号：US10566019
申请日：2004-07-23
申请人： Samuel Neto , Hartmut Hibst , Frank Rosowski , Sebastian Storck
发明人： Samuel Neto , Hartmut Hibst , Frank Rosowski , Sebastian Storck
IPC分类号： C07D307/89 , C07C51/255 , C07C51/16
CPC分类号： C07C51/313 , B01J23/002 , B01J23/682 , B01J23/688 , B01J35/002 , B01J35/1014 , B01J35/1019 , B01J37/0045 , B01J37/0223 , B01J2523/00 , C01G31/006 , C07C51/265 , C07C63/16 , B01J2523/18 , B01J2523/3712 , B01J2523/55 , B01J2523/72 , B01J2523/47
摘要： A multimetal oxide of the formula I, Aga-cQbMcV2Od*eH2O, I where a is from 0.3 to 1.9, Q is an element selected from among P, As, Sb and/or Bi, is from 0 to 0.3, M is a metal selected from among Nb, Ce, W, Mn, Ta, Pd, Pt, Ru and/or Rh, c is from 0.001 to 0.5, with the proviso that (a-c)≧0.1, d is a number which is determined by the valence and abundance of the elements other than oxygen in the formula I and e is from 0 to 20, and also precatalysts and catalysts produced therefrom for the partial oxidation of aromatic hydrocarbons are described.
摘要翻译：式I的多金属氧化物，<？in-line-formula description =“In-line Formulas”end =“lead”？> Ag ？V V V V V * O O O O O，，------------------------------------- 其中a为0.3〜1.9，Q为选自P，As，Sb和/或Bi的元素，为0〜0.3，M为选自Nb， Ce，W，Mn，Ta，Pd，Pt，Ru和/或Rh，c为0.001至0.5，条件是（ac）> = 0.1，d为由化合价描述了式I中的氧以外的元素和e为0至20，并且还描述了由其制备的用于芳族烃的部分氧化的预催化剂和催化剂。

12. 发明申请

US20060276661A1 Three-layered or four-layered catalyst systems for producing phthalic anhydride 有权
标题翻译：用于生产邻苯二甲酸酐的三层或四层催化剂体系
公开(公告)号：US20060276661A1
公开(公告)日：2006-12-07
申请号：US10557993
申请日：2004-05-15
申请人： Sebastian Storck , Jurgen Zuhike , Samuel Neto , Frank Rosowski
发明人： Sebastian Storck , Jurgen Zuhike , Samuel Neto , Frank Rosowski
IPC分类号： C07D307/89 , B01J21/00
CPC分类号： C07C51/313 , B01J23/002 , B01J23/22 , B01J27/198 , B01J35/0006 , B01J35/10 , B01J35/1009 , B01J35/1014 , B01J2523/00 , C07C51/265 , C07C63/16 , B01J2523/15 , B01J2523/47 , B01J2523/53 , B01J2523/55 , B01J2523/51
摘要： Catalyst systems for preparing phthalic anhydride by means of gas-phase oxidation of o-xylene and/or naphthalene, and a process for preparing phthalic anhydride using the catalyst systems.
摘要翻译：通过邻二甲苯和/或萘的气相氧化制备邻苯二甲酸酐的催化剂体系，以及使用催化剂体系制备邻苯二甲酸酐的方法。

13. 发明申请

US20070135302A1 Mehtod for the production of a catalyst for gas-phase oxidations by the coating of support materials in a fluid bed apparatus 审中-公开
标题翻译： Mehtod用于通过在流化床装置中涂覆支撑材料来生产用于气相氧化的催化剂
公开(公告)号：US20070135302A1
公开(公告)日：2007-06-14
申请号：US10573480
申请日：2004-09-24
申请人： Samuel Neto , Wolfgang Rummel , Sebastien Storck , Jurgen Zuhlke , Frank Rosowski
发明人： Samuel Neto , Wolfgang Rummel , Sebastien Storck , Jurgen Zuhlke , Frank Rosowski
IPC分类号： B01J23/00
CPC分类号： B01J2/16 , B01J2/006 , B01J23/22 , B01J35/0006 , B01J35/002 , B01J35/1014 , B01J37/0009 , B01J37/0221 , B01J37/0232 , B01J37/0244
摘要： The invention relates to a process for producing a catalyst for gas-phase oxidations, which comprises weighing a particulate inert support having a total mass of Msupport into a fluidized-bed apparatus, providing an aqueous suspension of a catalytically active material or sources therefor and a binder having a binder content of Bsusp, fluidizing the inert support by introduction of a gas stream heated to a temperature of Tgas at a flow rate of Qgas, and spraying the suspension at a rate of Qsusp onto the fluidized inert support. When Qgas, Qsusp, Bsusp, Msupport and Tgas are selected within the ranges 3000≦Qgas [m3/h]≦9000, 1000≦Qsusp [g/min]≦3500, 2≦Bsusp [% by weight]≦18, 60≦Msupport [kg]≦240. 75≦Tgas [° C.]≦120 so that a parameter K defined as K=0.020 Qgas−0.055 Qsusp+7.500 Bsusp−0.667 Msupport+2.069 Tgas−7satisfies the relationship 127.5≦K≦202, high-quality coatings can be produced and the formation of twins made up of support particles adhering to one another can be avoided.
摘要翻译：本发明涉及一种用于生产气相氧化催化剂的方法，该方法包括将具有总质量的载体的颗粒惰性载体称重到流化床装置中，提供水悬浮液催化活性材料或其来源以及具有粘合剂含量为B susp susp susp susp susp a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a a Q气体的流速，并以悬浮液的速度将悬浮液喷雾到流化的惰性载体上。当气体气体时，Q 1，B 2，B 3，M 3，N 2，在3000以下范围内选择气体[m 3 / h] <= 9000,1000 <= Q [g / min ] <= 3500，2 <= B [重量％] <= 18,60 <= M [kg] = 240。 75 <= T [°C] <= 120，使得定义为<？in-line-formula description =“In-Line Formulas”end =“lead”？> K = 0.020 Q气体-0.055 Q + +7.500 B＆lt;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp;＆nbsp; 气体-7 <？在线公式描述=“在线公式”end =“tail”？>满足关系127.5 <= K <= 202，可以生产高品质涂层并形成可以避免由彼此粘附的支撑颗粒构成的双胞胎。

14. 发明授权

US07851398B2 Catalytic titanium dioxide mixtures, catalysts and catalyst systems containing the same, processes for making the same, and uses therefor 有权
标题翻译：催化二氧化钛混合物，催化剂和含有其的催化剂体系，其制备方法及其用途
公开(公告)号：US07851398B2
公开(公告)日：2010-12-14
申请号：US11719422
申请日：2005-11-16
申请人： Samuel Neto , Sebastian Storck , Jürgen Zühlke , Frank Rosowski
发明人： Samuel Neto , Sebastian Storck , Jürgen Zühlke , Frank Rosowski
IPC分类号： B01J27/198 , B01J21/06
CPC分类号： B01J21/063 , B01J23/002 , B01J23/22 , B01J35/0006 , B01J35/1014 , B01J37/0232 , B01J2523/00 , C07C51/265 , C07C51/313 , C07C63/16 , B01J2523/53 , B01J2523/55 , B01J2523/15 , B01J2523/47 , B01J2523/51
摘要： Catalytic titanium dioxide mixtures comprising: a first anatase titanium dioxide having a BET surface area greater than 15 m2/g and a hydrogen uptake for the reduction of Ti4+ to Ti3+ of from 5 to 20 μmol/m2; and a second anatase titanium dioxide having a BET surface area less than or equal to 15 m2/g and a hydrogen uptake for the reduction of Ti4+ to Ti3+ of from 0.6 to 7 μmol/m2, processes for preparing catalysts containing the same, catalysts containing active compositions including such titanium dioxide mixtures on support materials, and catalyst systems using the same.
摘要翻译：催化二氧化钛混合物，其包含：BET表面积大于15m 2 / g的第一锐钛型二氧化钛和用于还原Ti 4+至Ti 3+的氢吸收为5至20μmol/ m 2; 和BET表面积小于或等于15m 2 / g的第二锐钛矿型二氧化钛和用于还原Ti 4+至Ti 3+的氢吸收为0.6〜7μmol/ m 2，制备含有该催化剂的催化剂，含有包含载体材料上的这种二氧化钛混合物的活性组合物和使用其的催化剂体系。

15. 发明授权

US07687425B2 Three-layered or four-layered catalyst systems for producing phthalic anhydride 有权
标题翻译：用于生产邻苯二甲酸酐的三层或四层催化剂体系
公开(公告)号：US07687425B2
公开(公告)日：2010-03-30
申请号：US10557993
申请日：2004-05-15
申请人： Sebastian Storck , Jürgen Zühlke , Samuel Neto , Frank Rosowski
发明人： Sebastian Storck , Jürgen Zühlke , Samuel Neto , Frank Rosowski
IPC分类号： B01J31/36
CPC分类号： C07C51/313 , B01J23/002 , B01J23/22 , B01J27/198 , B01J35/0006 , B01J35/10 , B01J35/1009 , B01J35/1014 , B01J2523/00 , C07C51/265 , C07C63/16 , B01J2523/15 , B01J2523/47 , B01J2523/53 , B01J2523/55 , B01J2523/51
摘要： Catalyst systems for preparing phthalic anhydride by means of gas-phase oxidation of o-xylene and/or naphthalene, and a process for preparing phthalic anhydride using the catalyst systems.
摘要翻译：通过邻二甲苯和/或萘的气相氧化制备邻苯二甲酸酐的催化剂体系，以及使用催化剂体系制备邻苯二甲酸酐的方法。

16. 发明授权

US07592294B2 Gas phase oxidation catalyst with defined vanadium oxide particle size distribution 有权
标题翻译：气相氧化催化剂具有规定的氧化钒粒度分布
公开(公告)号：US07592294B2
公开(公告)日：2009-09-22
申请号：US10573481
申请日：2004-09-24
申请人： Sebastian Storck , Jürgen Zühlke , Samuel Neto , Frank Rosowski , Wolfgang Rummel
发明人： Sebastian Storck , Jürgen Zühlke , Samuel Neto , Frank Rosowski , Wolfgang Rummel
IPC分类号： B01J23/22 , B01J21/06
CPC分类号： C07C51/313 , B01J23/002 , B01J23/22 , B01J27/198 , B01J35/023 , B01J37/0219 , B01J37/0221 , B01J2523/00 , C07C51/265 , C07C63/16 , B01J2523/15 , B01J2523/47 , B01J2523/53 , B01J2523/55
摘要： A process is described for producing a catalyst for gas-phase oxidations, in which a suspension of TiO2 and V2O5 particles is applied to a fluidized inert support, wherein at least 90% by volume of the V2O5 particles have a diameter of 20 μm or less and at least 95% by volume of the V2O5 particles have a diameter of 30 μm or less. The defined particle size distribution of the V2O5 allows a high coating efficiency.
摘要翻译：描述了一种制备用于气相氧化的催化剂的方法，其中将TiO 2和V 2 O 5颗粒的悬浮液施加到流化惰性载体上，其中至少90体积％的V 2 O 5颗粒的直径为20μm或更小并且至少95体积％的V 2 O 5颗粒的直径为30μm或更小。 V2O5的定义的粒度分布允许高涂层效率。

17. 发明授权

US07371893B2 Production of aldehydes, carboxylic acids and/or carboxylic acid anhydrides by means of catalysts containing vanadium oxide, titanium dioxide, and antimony oxide 有权
标题翻译：通过含有氧化钒，二氧化钛和氧化锑的催化剂生产醛，羧酸和/或羧酸酐
公开(公告)号：US07371893B2
公开(公告)日：2008-05-13
申请号：US10557791
申请日：2004-05-21
申请人： Sebastian Storck , Jürgen Zühlke , Samuel Neto , Frank Rosowski
发明人： Sebastian Storck , Jürgen Zühlke , Samuel Neto , Frank Rosowski
IPC分类号： C07C51/16 , C07D307/89
CPC分类号： C07C51/265 , C07C51/313 , C07C63/16
摘要： A description is given of a process for preparing aldehydes, carboxylic acids and/or carboxylic anhydrides, in particular phthalic anhydride, in which a gaseous stream comprising an aromatic hydrocarbon and molecular oxygen is passed at elevated temperature over a bed of a first catalyst and a bed which is made up of a second catalyst having a higher activity than the first catalyst and is located downstream of the first catalyst in the flow direction of the gaseous stream, wherein the catalytically active composition of the first catalyst comprises at least vanadium oxide, titanium dioxide and antimony oxide and the ratio of vanadium, calculated as V2O5, to antimony, calculated as Sb2O3, in the first catalyst is from 3.5:1 to 5:1. The source of antimony oxide used for the first catalyst is preferably particulate antimony trioxide having a mean particle size of from 0.5 to 5 μm. The process allows the desired oxidation products to be obtained in high yield over longer periods of time.
摘要翻译：给出了制备醛，羧酸和/或羧酸酐，特别是邻苯二甲酸酐的方法的描述，其中包含芳族烃和分子氧的气流在升高的温度下通过第一催化剂的床和床，其由比第一催化剂高的活性的第二催化剂组成，并且位于气流的流动方向上位于第一催化剂的下游，其中第一催化剂的催化活性组合物至少包含氧化钒，钛二氧化锑和氧化锑，以V 2 O 5 5计算的钒与锑的比例计算为Sb 2 O 3 在第一催化剂中为3.5:1至5:1。用于第一催化剂的氧化锑的来源优选是平均粒径为0.5-5微米的颗粒状三氧化锑。该方法允许在较长时间内以高产率获得所需的氧化产物。

18. 发明授权

US07390911B2 Method for producing phthalic anhydride 有权
标题翻译：邻苯二甲酸酐的制造方法
公开(公告)号：US07390911B2
公开(公告)日：2008-06-24
申请号：US10557705
申请日：2004-05-15
申请人： Samuel Neto , Jürgen Zühlke , Sebastian Storck , Frank Rosowski
发明人： Samuel Neto , Jürgen Zühlke , Sebastian Storck , Frank Rosowski
IPC分类号： C07D307/89
CPC分类号： C07C51/265 , C07C51/313 , C07D307/89 , C07C63/16
摘要： The invention relates to a process for preparing phthalic anhydride, in which the catalytic gas-phase oxidation of o-xylene and/or naphthalene is carried out over at least three zones of catalysts of increasing activity, with only the last zone of the catalyst system containing phosphorus and the last zone also comprising at least 10% by weight of vanadium (calculated as V2O5) based on the active composition of the catalyst and having a ratio of vanadium (calculated as V2O5) to phosphorus of greater than 35.
摘要翻译：本发明涉及一种制备邻苯二甲酸酐的方法，其中邻二甲苯和/或萘的催化气相氧化在活性增加的催化剂的至少三个区域上进行，只有催化剂体系的最后一个区域并且最后一个区域还包含至少10重量％的钒（以V 2 O 5 N计算），基于催化剂的活性组成，并且其比例的钒（以V 2 O 5计算）至大于35的磷。

19. 发明申请

US20070213555A1 Catalyst Having a Silver-Vanaduim Oxide Phase and a Promoter Phase 失效
标题翻译：具有银 - 钒酸钠相和促进剂相的催化剂
公开(公告)号：US20070213555A1
公开(公告)日：2007-09-13
申请号：US10594128
申请日：2005-03-24
申请人： Samuel Neto , Frank Rosowski , Sebastian Storck , Stefan Bauer
发明人： Samuel Neto , Frank Rosowski , Sebastian Storck , Stefan Bauer
IPC分类号： B01J23/50 , C07C47/00 , C07C61/08 , C07C65/00
CPC分类号： B01J23/682 , B01J23/002 , B01J35/0006 , B01J37/0045 , B01J37/0215 , B01J37/0219 , B01J37/0223 , B01J2523/00 , C07C51/265 , C07C63/16 , B01J2523/15 , B01J2523/47 , B01J2523/55 , B01J2523/18
摘要： A catalyst is described which has a catalytically active composition which contains a phase A and a phase B in the form of three-dimensional delimited regions, wherein phase A is a silver-vanadium oxide bronze and phase B a mixed oxide phase based on titanium dioxide and vanadium pentoxide. The catalyst serves to prepare aldehydes, carboxylic acids and/or carboxylic anhydrides from aromatic or heteroaromatic hydrocarbons by gas phase oxidation.
摘要翻译：描述了一种具有催化活性组合物的催化剂，其包含三维定界区域的A相和B相，其中A相是银 - 钒氧化物青铜，B相是基于二氧化钛的混合氧化物相和五氧化二钒。催化剂用于通过气相氧化从芳族或杂芳族烃制备醛，羧酸和/或羧酸酐。

20. 发明授权

US07338918B2 Catalyst having a silver-vanadium oxide phase and a promoter phase 失效
标题翻译：具有银 - 钒氧化物相和助催化剂相的催化剂
公开(公告)号：US07338918B2
公开(公告)日：2008-03-04
申请号：US10594128
申请日：2005-03-24
申请人： Samuel Neto , Frank Rosowski , Sebastian Storck , Stefan Bauer
发明人： Samuel Neto , Frank Rosowski , Sebastian Storck , Stefan Bauer
IPC分类号： B01J23/50 , C07C51/255 , C07C65/00 , C07C45/00
CPC分类号： B01J23/682 , B01J23/002 , B01J35/0006 , B01J37/0045 , B01J37/0215 , B01J37/0219 , B01J37/0223 , B01J2523/00 , C07C51/265 , C07C63/16 , B01J2523/15 , B01J2523/47 , B01J2523/55 , B01J2523/18
摘要： A catalyst is described which has a catalytically active composition which contains a phase A and a phase B in the form of three-dimensional delimited regions, wherein phase A is a silver-vanadium oxide bronze and phase B a mixed oxide phase based on titanium dioxide and vanadium pentoxide. The catalyst serves to prepare aldehydes, carboxylic acids and/or carboxylic anhydrides from aromatic or heteroaromatic hydrocarbons by gas phase oxidation.
摘要翻译：描述了一种具有催化活性组合物的催化剂，其包含三维定界区域的A相和B相，其中A相是银 - 钒氧化物青铜，B相是基于二氧化钛的混合氧化物相和五氧化二钒。催化剂用于通过气相氧化从芳族或杂芳族烃制备醛，羧酸和/或羧酸酐。

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