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11. 发明申请

US20050282011A1 Microcapsule emulsion and method for producing the same 审中-公开
标题翻译：微胶囊乳剂及其制备方法
公开(公告)号：US20050282011A1
公开(公告)日：2005-12-22
申请号：US11153789
申请日：2005-06-15
申请人： Hiroshi Yokoyama , Kouji Kinoshita , Takehiko Fukumoto , Ryuichi Saguchi , Tatsuya HoJo , Toshimi Kobayashi , Kinya Ogawa
发明人： Hiroshi Yokoyama , Kouji Kinoshita , Takehiko Fukumoto , Ryuichi Saguchi , Tatsuya HoJo , Toshimi Kobayashi , Kinya Ogawa
IPC分类号： A01N25/28 , B01J13/14 , B05D7/00
CPC分类号： B01J13/14 , Y10T428/2984
摘要： Provided are a microcapsule emulsion which can release almost all the amount of a biological active substance comprised therein at a constant release rate over a prolonged period, and a method for producing the same. More specifically, provided is the microcapsule emulsion comprising an emulsion particle formed by emulsion polymerization of a total amount of 15 to 90 parts by weight of a first monofunctional alkyl (meth)acrylate ester and a first multifunctional (meth)acrylate ester in the presence of 100 parts by weight of a biological active substance; and a coated layer on the emulsion particle, the layer being formed by emulsion polymerization of a total amount of 20 to 200 parts by weight of a second monofunctional alkyl (meth)acrylate ester and a second multifunctional (meth)acrylate ester in the presence of the emulsion particle; wherein difference in carbon numbers between an alkyl group of the first monofunctional alkyl (meth)acrylate ester and an alkyl group of the second monofunctional alkyl (meth)acrylate ester is from 3 to 17.
摘要翻译：本发明提供一种微胶囊乳剂，其能够以长时间恒定的释放速度释放其中包含的几乎全部量的生物活性物质及其制造方法。更具体地，提供了包含通过乳液聚合形成的乳液颗粒的微胶囊乳液，其总量为15至90重量份的第一单官能（甲基）丙烯酸烷基酯和第一多官能（甲基）丙烯酸烷基酯在存在 100重量份的生物活性物质; 和乳液颗粒上的涂层，该层通过乳液聚合形成，总量为20〜200重量份的第二单官能烷基（甲基）丙烯酸酯和第二多官能（甲基）丙烯酸酯），在乳液颗粒; 其中第一单官能（甲基）丙烯酸烷基酯的烷基与第二单官能（甲基）丙烯酸烷基酯的烷基之间的碳数之差为3〜17。

12. 发明授权

US5880318A Process for the preparation of .alpha.-bromo, .omega.-chloroalkanes 失效
标题翻译：制备α-溴，ω-氯代烷烃的方法
公开(公告)号：US5880318A
公开(公告)日：1999-03-09
申请号：US906816
申请日：1997-08-06
申请人： Takehiko Fukumoto , Hiroshi Suzuki , Kinya Ogawa , Kazushi Hirokawa
发明人： Takehiko Fukumoto , Hiroshi Suzuki , Kinya Ogawa , Kazushi Hirokawa
IPC分类号： C07C17/20 , C07C19/075 , C07C19/00
CPC分类号： C07C17/202
摘要： Described is a process for easily preparing an .alpha.-bromo,.omega.-chloroalkane which is high in purity represented by the formula: Br(CH.sub.2).sub.n Cl in which n stands for an integer of 4 to 12. The process comprises reacting in an organic solvent an .alpha.,.omega.-dichloroalkane with an .alpha..omega.-dibromoalkane. As the organic solvent, an aprotic nitrogen-containing or sulfur-containing organic solvent having a dielectric constant at 20.degree. C. of 20 or larger, for example, N,N-dimethylformamide, N,N-dimethylacetamide or N,N-dimethylimidazolidinone is preferred.
摘要翻译：描述了一种易于制备由式Br（CH 2）n Cl表示的纯度高的α-溴，ω-氯烷烃的方法，其中n表示4至12的整数。该方法包括在有机溶剂具有αω-二溴烷烃的α，ω-二氯烷烃。作为有机溶剂，在20℃下介电常数为20以上的非质子性含氮或含硫有机溶剂，例如N，N-二甲基甲酰胺，N，N-二甲基乙酰胺或N，N-二甲基咪唑烷酮是优选的。

13. 发明授权

US5481040A Process for the preparation of phosphonium salts 失效
标题翻译：鏻盐的制备方法
公开(公告)号：US5481040A
公开(公告)日：1996-01-02
申请号：US412912
申请日：1995-03-29
申请人： Takehiko Fukumoto , Kazushi Hirokawa , Kurao Okada
发明人： Takehiko Fukumoto , Kazushi Hirokawa , Kurao Okada
IPC分类号： C07C1/34 , C07C69/007 , C07F9/54 , C07F9/655 , C07F9/02
CPC分类号： C07F9/6552 , C07C1/34 , C07C69/007 , C07F9/5407 , C07F9/5428 , C07F9/5442
摘要： A process for the preparation of phosphonium salts by the use of chlorides, which is useful in the course of synthesis of olefin compounds by the Wittig reaction, and which comprises reacting a phosphine compound of the general formulaR.sup.1.sub.3 Pwherein R.sup.1 is a phenyl group or a straight-chain alkyl group having 2 to 8 carbon atoms, with a primary or secondary chloride of the general formula ##STR1## wherein R.sup.2 and R.sup.3 are hydrocarbon radicals, in a solvent selected from the group consisting of N,N-dimethylformamide, N,N-dimethylacetamide and N,N-1,3-dimethyl-2-imidazolidinone, and in the presence of an alkali metal salt of the general formula MBr or MI.
摘要翻译：一种通过使用氯化物制备鏻盐的方法，该方法在通过维t希反应合成烯烃化合物的过程中是有用的，并且包括使通式R 13 P的膦化合物，其中R1是苯基或具有2-8个碳原子的直链烷基，具有通式“IMAGE”的一级或二级氯化物，其中R 2和R 3是烃基，在选自N，N-二甲基甲酰胺，N，N-二甲基甲酰胺， N-二甲基乙酰胺和N，N-1,3-二甲基-2-咪唑烷酮，并在通式为MBr或MI的碱金属盐的存在下进行。

14. 发明授权

US08828374B2 Sustained pheromone releaser 有权
标题翻译：持续的信息素释放者
公开(公告)号：US08828374B2
公开(公告)日：2014-09-09
申请号：US11257957
申请日：2005-10-25
申请人： Tatsuya Hojo , Ryuichi Saguchi , Takehiko Fukumoto , Noboru Aiba
发明人： Tatsuya Hojo , Ryuichi Saguchi , Takehiko Fukumoto , Noboru Aiba
IPC分类号： A01N25/00 , A01N25/08 , A01N25/34 , A01N25/18
CPC分类号： A01N25/18
摘要： Provided is a sustained releaser of a sex pheromone having a high release rate, especially preferably of a sex pheromone of an aliphatic acetate compound having 10 to 16 carbon atoms, wherein the release of the sex pheromone is controlled so that it can be released at a constant rate over a control period of a pest insect. More specifically, provided is a sustained pheromone releaser comprising a polymer container and having, enclosed therein, a mixture having a melting point of 15 to 35° C. and being obtained by mixing a sex pheromone substance and a compound having a melting point of 10 to 40° C.
摘要翻译：提供具有高释放速度的性信息素的持续释放剂，特别优选具有10至16个碳原子的脂族乙酸酯化合物的性信息素，其中性信息素的释放被控制，使得其可以在在虫害控制期间的恒定速率。更具体地说，提供了一种持续的信息素释放剂，其包含聚合物容器，并且在其中包含熔点为15至35℃的混合物，并且通过混合性信息素物质和熔点为10的化合物至40℃

15. 发明申请

US20100021417A1 ACETATE-CONTAINING MATING DISRUPTANT AND MATING DISRUPTION METHOD USING THE SAME 审中-公开
标题翻译：含乙酸的主要污染物和使用该物质的破坏方法
公开(公告)号：US20100021417A1
公开(公告)日：2010-01-28
申请号：US12507498
申请日：2009-07-22
申请人： Kinya Ogawa , Tatsuya Hojo , Takehiko Fukumoto
发明人： Kinya Ogawa , Tatsuya Hojo , Takehiko Fukumoto
IPC分类号： A01N25/00
CPC分类号： A01N31/02 , A01N37/02 , A01N37/06 , A01N2300/00
摘要： Provided are a mating disruptant having an improved mating disruption effect against pest insects. Specifically, provided is a mating disruptant for the control of pest insects whose natural sex pheromone composition is substantially free of an alcohol and comprises one or more acetates, the disruptant comprising the one or more acetates and an alcohol or alcohols which can be derived from the one or more acetate, wherein an amount of each of the alcohol or alcohols is from 0.5 to 10% by weight relative to an amount of each deriving acetate; and a mating disruption method using the mating disruptant. The alcohol which can be derived from the acetate is an alcohol obtainable by hydrolysis of the acetate and means an alcohol component of the ester derived from an acid and the alcohol.
摘要翻译：提供了具有改善的对害虫的交配破坏作用的交配破坏剂。具体来说，提供了用于控制害虫的交配扰乱物，其自然性信息素组合物基本上不含醇，并且包含一种或多种乙酸盐，所述破坏剂包含一种或多种乙酸盐，以及可衍生自一种或多种乙酸酯，其中每种醇或醇的量相对于每种衍生的乙酸酯的量为0.5至10重量％以及使用交配中断器的交配中断方法。可以从乙酸酯衍生的醇是通过乙酸酯水解得到的醇，并且是指由酸和醇衍生的酯的醇组分。

16. 发明授权

US07638647B2 Method for preparing (E3,Z5)-3,5-alkadienyl acetate 有权
标题翻译：（E3，Z5）-3,5-链二烯酸乙酯的制备方法
公开(公告)号：US07638647B2
公开(公告)日：2009-12-29
申请号：US12323823
申请日：2008-11-26
申请人： Miyoshi Yamashita , Takehiko Fukumoto
发明人： Miyoshi Yamashita , Takehiko Fukumoto
IPC分类号： C07C67/02
CPC分类号： C07C41/48 , C07C29/10 , C07C41/50 , C07C67/08 , C07C69/007 , C07C69/145 , C07C33/02 , C07C43/30
摘要： Provided is a method for preparing (E3,Z5)-3,5-alkadienyl acetate and (E3,Z5)-3,5-dodecadienyl acetate which is a sex pheromone of Brazilian apple leafminer. Specifically, provided is a method for preparing (E3,Z5)-3,5-alkadienyl acetate, comprising steps of hydrolyzing 5,5-diethoxy-(Z3)-3-pentenyl methoxymethyl ether in the presence of an acid to obtain 4-formyl-(E3)-butenyl methoxymethyl ether; reacting the 4-formyl-(E3)-butenyl methoxymethyl ether with alkylidene triphenylphosphorane in accordance with the Wittig reaction to obtain (E3,Z5)-3,5-alkadienyl methoxymethyl ether; and obtaining (E3,Z5)-3,5-alkadienyl acetate using the (E3,Z5)-3,5-alkadienyl methoxymethyl ether as a starting substance.
摘要翻译：提供一种制备（E3，Z5）-3,5-链二烯酸乙酸酯和（E3，Z5）-3,5-十二烷基乙酸酯的方法，其是巴西苹果叶片的性信息素。具体地说，提供了制备（E3，Z5）-3,5-链二烯基乙酸酯的方法，包括在酸存在下水解5,5-二乙氧基 - （Z 3）-3-戊烯基甲基甲基醚的步骤，得到4- 甲酰基 - （E3） - 丁烯基甲氧基甲基醚; 根据Wittig反应使4-甲酰基 - （E3） - 丁烯基甲氧基甲基醚与亚烷基三苯基正膦反应，得到（E3，Z5）-3,5-二甲氧基甲基醚; 并使用（E3，Z5）-3,5-链二烯基甲氧基甲基醚作为起始物质获得（E3，Z5）-3,5-链二烯酸乙酯。

17. 发明申请

US20090143617A1 METHOD FOR PREPARING (E3, Z5) -3,5-ALKADIENYL ACETATE 有权
标题翻译：制备（E3，Z5）-3,5-亚氨基乙酸酯的方法
公开(公告)号：US20090143617A1
公开(公告)日：2009-06-04
申请号：US12323823
申请日：2008-11-26
申请人： MIYOSHI YAMASHITA , Takehiko Fukumoto
发明人： MIYOSHI YAMASHITA , Takehiko Fukumoto
IPC分类号： C07C57/18
CPC分类号： C07C41/48 , C07C29/10 , C07C41/50 , C07C67/08 , C07C69/007 , C07C69/145 , C07C33/02 , C07C43/30
摘要： Provided is a method for preparing (E3,Z5)-3,5-alkadienyl acetate and (E3,Z5)-3,5-dodecadienyl acetate which is a sex pheromone of Brazilian apple leafminer. Specifically, provided is a method for preparing (E3,Z5)-3,5-alkadienyl acetate, comprising steps of hydrolyzing 5,5-diethoxy-(Z3)-3-pentenyl methoxymethyl ether in the presence of an acid to obtain 4-formyl-(E3)-butenyl methoxymethyl ether; reacting the 4-formyl-(E3)-butenyl methoxymethyl ether with alkylidene triphenylphosphorane in accordance with the Wittig reaction to obtain (E3,Z5)-3,5-alkadienyl methoxymethyl ether; and obtaining (E3,Z5)-3,5-alkadienyl acetate using the (E3,Z5)-3,5-alkadienyl methoxymethyl ether as a starting substance.
摘要翻译：提供一种制备（E3，Z5）-3,5-链二烯酸乙酸酯和（E3，Z5）-3,5-十二烷基乙酸酯的方法，其是巴西苹果叶片的性信息素。具体地说，提供了制备（E3，Z5）-3,5-链二烯基乙酸酯的方法，包括在酸存在下水解5,5-二乙氧基 - （Z 3）-3-戊烯基甲基甲基醚的步骤，得到4- 甲酰基 - （E3） - 丁烯基甲氧基甲基醚; 根据Wittig反应使4-甲酰基 - （E3） - 丁烯基甲氧基甲基醚与亚烷基三苯基正膦反应，得到（E3，Z5）-3,5-二甲氧基甲基醚; 并使用（E3，Z5）-3,5-链二烯基甲氧基甲基醚作为起始物质获得（E3，Z5）-3,5-链二烯酸乙酯。

18. 发明授权

US06599500B1 Communication disruptant and communication disruption method 有权
标题翻译：沟通破坏和沟通破坏的方法
公开(公告)号：US06599500B1
公开(公告)日：2003-07-29
申请号：US09297638
申请日：1999-05-05
申请人： Kinya Ogawa , Masaomi Azuma , Fumiaki Mochizuki , Takehiko Fukumoto
发明人： Kinya Ogawa , Masaomi Azuma , Fumiaki Mochizuki , Takehiko Fukumoto
IPC分类号： A01N3702
CPC分类号： A01N37/02 , A01N2300/00
摘要： When a communication disruptant containing (Z)-11-tetradecen-1-yl acetate as the only active ingredient is continually used for a period of 5 to 10 years, a phenomenon has been observed in which its communication-disrupting effect on insect pests, particularly of the family Tortricidae, living in the field or the like through successive generations is reduced. Accordingly, it is eagerly desired to develop a new communication disruptant which is also effective for such fields where the communication-disrupting effect (on insect pests, particularly of the family Tortricidae, living there through successive generations) has been reduced. The present invention provides, for use in the control of insect pests having (Z)-11-tetradecen-1-yl acetate contained in their sex pheromone, a communication disruptant containing (Z)-11-tetradecen-1-yl acetate and the maximum component in the composition of the sex pheromone excepting (Z)-11-tetradecen-1-yl acetate, wherein the weight percentage of the maximum component in the communication disruptant is equal to a value obtained by multiplying the weight percentage of the maximum component in the sex pheromone by a number in the range of 2/100 to 50/100.
摘要翻译：当含有（Z）-11-十四碳烯-1-基乙酸酯作为唯一活性成分的通信中断剂连续使用5至10年时，已经观察到其对昆虫害虫的通信中断作用的现象，特别是通过连续几代生活在田野里的Tortricidae家族减少了。因此，迫切需要开发一种新的通信破坏者，对于通信中断效应（特别是通过连续世代生活在这里的Tortricidae的昆虫害虫）已经减少的领域也是有效的。本发明提供了用于控制其性信息素中含有（Z）-11-十四碳烯-1-基乙酸酯的昆虫害虫，其含有（Z）-11-十四碳烯-1-基乙酸酯和除了（Z）-11-十四碳烯-1-基乙酸酯之外的性信息素的组成中的最大成分，其中通信中断剂中最大成分的重量百分比等于通过将最大成分的重量百分比乘以在性信息素数量在2/100到50/100之间。

19. 发明授权

US06521224B1 Method for controlling injurious insect 失效
标题翻译：防治害虫的方法
公开(公告)号：US06521224B1
公开(公告)日：2003-02-18
申请号：US08665046
申请日：1996-06-07
申请人： Koichi Ogura , Kinya Ogawa , Takehiko Fukumoto
发明人： Koichi Ogura , Kinya Ogawa , Takehiko Fukumoto
IPC分类号： A01N2518
CPC分类号： A01N25/00
摘要： A method for controlling an injurious insect is herein disclosed, which comprises disturbing the copulative communication of an injurious insect to prevent proliferation of the insect by distributing a source of the sex pheromone thereof over a field to be controlled to make the sex pheromone release from the source distributed in the field, wherein a source of the sex pheromone having a high effective component-release rate per unit time is distributed over the central region of the field at a low density while a source of the sex pheromone having a low effective component-release rate per unit time is distributed over the peripheral region of the field at a high density. A sex pheromone-release agent having an effective component-release rate ranging from 0.01 to 2 g/day may be distributed over the central region of the field at a density ranging from 1 to 50 locations/ha, while a sex pheromone-release rope having an effective component-release rate ranging from 5 to 250 mg/m/day may be substantially uniformly stretched around the peripheral region of the field at a density ranging from 10 to 150 m/ha.
摘要翻译：本文公开了一种用于控制有害昆虫的方法，其包括通过在要控制的场中分布其信息素来源来扰乱有害昆虫的相互通信以防止昆虫的扩散，以使性信息素从分布在现场的源，其中每单位时间具有高有效成分释放速率的性信息素的来源以低密度分布在场的中心区域上，而具有低有效成分释放速率的性信息素的来源，单位时间的释放速率以高密度分布在场的周边区域上。具有0.01至2g /天的有效成分释放速率的性信息素释放剂可以以1至50个位置/ ha的密度分布在场的中心区域上，而性信息素释放绳具有5至250mg / m 2 /天的有效组分释放速率可以以10至150m / ha的密度基本上均匀地拉伸在场周边区域周围。

20. 发明授权

US5714649A 1-Halo-cis-3-tetradecenes and processes for the preparation of cis-Olefin compounds by using same 失效
标题翻译： 1-顺 - 顺-3-十四碳烯和通过使用它们制备顺式烯烃化合物的方法
公开(公告)号：US5714649A
公开(公告)日：1998-02-03
申请号：US575333
申请日：1995-12-20
申请人： Takehiko Fukumoto , Daisuke Iwai , Shigeo Okano , Hiroshi Suzuki , Mitsuyoshi Oshima
发明人： Takehiko Fukumoto , Daisuke Iwai , Shigeo Okano , Hiroshi Suzuki , Mitsuyoshi Oshima
IPC分类号： A01N27/00 , C07C1/32 , C07C11/02 , C07C17/16 , C07C21/04 , C07C21/14 , C07C21/17 , C07F1/02 , C07F3/02 , C07C19/08
CPC分类号： C07C11/02 , C07C17/16 , C07C21/04 , C07C21/14 , C07C21/17
摘要： Disclosed are compounds suitable for use as raw materials which enable cis-olefin compounds useful as physiologically active substances such as the sex pheromones of various insects, or as intermediates for the synthesis thereof to be prepared on an industrial scale at a reasonable cost, and processes for the preparation of cis-olefin compounds by using the same. For this purpose, novel compounds (i.e., 1-halo-cis-3-tetradecenes) of the general formula (I) CH.sub.3 (CH.sub.2).sub.9 CH.dbd.CH(CH.sub.2).sub.2 X (I) wherein X is a halogen atom, are used as raw materials for the preparation of cis-olefin compounds.
摘要翻译：公开了适合用作原料的化合物，其使得可用作诸如各种昆虫的性信息素的生理活性物质的顺式烯烃化合物或其合成成本的工业规模的合成中间体，以及方法用于通过使用它们制备顺式烯烃化合物。为此，将通式（I）CH（CH 2）9 CH = CH（CH 2）2 X（I）的新化合物（即1-卤代 - 顺式-3-十四碳烯）其中X为卤素原子用作用于制备顺式烯烃化合物的原料。

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