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11. 发明申请

US20100113851A1 System and Method of Deactivating and Quenching an Oligomerization Catalyst 有权
标题翻译：灭活和淬灭低聚催化剂的系统和方法
公开(公告)号：US20100113851A1
公开(公告)日：2010-05-06
申请号：US12609631
申请日：2009-10-30
申请人： Bruce E. Kreischer , Orson L. Sydora , Ronald D. Knudsen
发明人： Bruce E. Kreischer , Orson L. Sydora , Ronald D. Knudsen
IPC分类号： C07C2/34 , C07C2/08 , C07C7/00
CPC分类号： B01J31/122 , B01J31/0237 , B01J31/0239 , B01J31/0244 , B01J31/143 , B01J2231/20 , B01J2531/62 , Y02P20/582 , Y10S585/903
摘要： A method of deactivate a catalyst system is described. The method may include contacting a reactor effluent comprising a catalyst system, an oligomerized olefin, and diluent with a kill agent to at least partially deactivate the catalyst system, separating the reactor effluent into one or more first streams comprising oligomerized olefin and diluent, the one or more first streams being substantially devoid of the at least partially deactivated catalyst, and a second stream comprising the deactivated catalyst; and contacting the second stream with a quench agent.
摘要翻译：描述了使催化剂体系失活的方法。该方法可以包括将包含催化剂体系，低聚烯烃和稀释剂的反应器流出物与杀灭剂接触以使催化剂体系至少部分失活，将反应器流出物分离成一个或多个包含低聚烯烃和稀释剂的第一流，或更多的第一物流基本上不含至少部分失活的催化剂，以及包含失活的催化剂的第二物流; 并使第二流与骤冷剂接触。

12. 发明授权

US08344198B2 Process to decrease or eliminate corrosion from the decomposition of halide containing olefin catalysts 有权
标题翻译：减少或消除含卤化烯烃催化剂分解腐蚀的方法
公开(公告)号：US08344198B2
公开(公告)日：2013-01-01
申请号：US10800471
申请日：2004-03-15
申请人： Warren M. Ewert , Bruce E. Kreischer , Ronald D. Knudsen
发明人： Warren M. Ewert , Bruce E. Kreischer , Ronald D. Knudsen
IPC分类号： C07C2/08 , B08B9/00
CPC分类号： C07C7/005 , B01J31/0244 , B01J31/143 , B01J31/181 , B01J31/4015 , B01J2231/20 , B01J2531/62 , C08F110/14 , C10G50/00 , C10G2300/1092 , C10G2300/44 , C10G2300/802 , C10G2400/22 , Y02P20/582 , Y02P20/584 , C08F2500/02
摘要： A processes is provided to inhibit or limit the decomposition of a halide-containing olefin oligomerization catalyst system during recovery of an oligomerization product. The process includes deactivation of an olefin oligomerization catalyst system present in an olefin oligomerization reactor effluent stream by contact with an alcohol under conditions that minimize potential for deactivated catalyst system decomposition. Such conditions include minimization of the water content of the deactivation agent and concentration of the deactivation agent.
摘要翻译：提供了在回收低聚产物期间抑制或限制含卤烯烃低聚催化剂体系的分解的方法。该方法包括使烯烃低聚反应器流出物流中存在的烯烃低聚催化剂体系通过与醇的接触来使在失活的催化剂体系分解的潜力最小化的条件下失活。这些条件包括减活化剂的水含量的最小化和失活剂的浓度。

13. 发明授权

US07718838B2 Olefin production process 有权
标题翻译：烯烃生产过程
公开(公告)号：US07718838B2
公开(公告)日：2010-05-18
申请号：US11637407
申请日：2006-12-12
申请人： William M. Woodard , Warren M. Ewert , Harvey D. Hensley , Mark E. Lashier , Glyndal D. Cowan , Jeffrey W. Freeman , Ralph V. Franklin , Ronald D. Knudsen , Richard L. Anderson , Lyle R. Kallenbach , Bruce E. Kreischer
发明人： William M. Woodard , Warren M. Ewert , Harvey D. Hensley , Mark E. Lashier , Glyndal D. Cowan , Jeffrey W. Freeman , Ralph V. Franklin , Ronald D. Knudsen , Richard L. Anderson , Lyle R. Kallenbach , Bruce E. Kreischer
IPC分类号： C07C2/26
CPC分类号： B01J31/122 , B01J31/0231 , B01J31/04 , B01J31/143 , B01J31/181 , B01J2231/20 , B01J2531/62 , C07C2/30 , C07C2527/08 , C07C2527/10 , C07C2527/126 , C07C2527/135 , C07C2531/02 , C07C2531/14 , C07C2531/22 , Y02P20/584 , C07C11/107
摘要： A process is provided to stabilize and/or reactivate an olefin production catalyst system which comprises contacting an olefin production catalyst system, either before or after use, with an aromatic compound.
摘要翻译：提供了一种稳定和/或重新活化烯烃生产催化剂体系的方法，其包括将烯烃生产催化剂体系在使用前或使用后与芳族化合物接触。

14. 发明授权

US07157612B2 Olefin production process 有权
标题翻译：烯烃生产过程
公开(公告)号：US07157612B2
公开(公告)日：2007-01-02
申请号：US10872250
申请日：2004-06-18
申请人： Warren M. Ewert , William M. Woodard , Harvey D. Hensley , Mark E. Lashier , Glyndal D. Cowan , Jeffrey W. Freeman , Ralph V. Franklin , Ronald D. Knudsen , Richard L. Anderson , Lyle R. Kallenbach , Bruce E. Kreischer
发明人： Warren M. Ewert , William M. Woodard , Harvey D. Hensley , Mark E. Lashier , Glyndal D. Cowan , Jeffrey W. Freeman , Ralph V. Franklin , Ronald D. Knudsen , Richard L. Anderson , Lyle R. Kallenbach , Bruce E. Kreischer
IPC分类号： C07C2/26 , C07C2/30
CPC分类号： B01J31/122 , B01J31/0231 , B01J31/04 , B01J31/143 , B01J31/181 , B01J2231/20 , B01J2531/62 , C07C2/30 , C07C2527/08 , C07C2527/10 , C07C2527/126 , C07C2527/135 , C07C2531/02 , C07C2531/14 , C07C2531/22 , Y02P20/584 , C07C11/107
摘要： A process is provided to stabilize and/or reactivate an olefin production catalyst system which comprises contacting an olefin production catalyst system, either before or after use, with an aromatic compound.
摘要翻译：提供了一种稳定和/或重新活化烯烃生产催化剂体系的方法，其包括将烯烃生产催化剂体系在使用前或使用后与芳族化合物接触。

15. 发明授权

US06455648B1 Olefin production 有权
标题翻译：烯烃生产
公开(公告)号：US06455648B1
公开(公告)日：2002-09-24
申请号：US09474067
申请日：1999-12-29
申请人： Jeffrey W. Freeman , Warren M. Ewert , Bruce E. Kreischer , Ronald D. Knudsen , Glyndal D. Cowan
发明人： Jeffrey W. Freeman , Warren M. Ewert , Bruce E. Kreischer , Ronald D. Knudsen , Glyndal D. Cowan
IPC分类号： C08F478
CPC分类号： B01J31/04 , B01J31/0244 , B01J31/122 , B01J31/143 , B01J2231/20 , B01J2531/62 , C07C2/30 , C07C2/32 , C07C2527/132 , C07C2531/02 , C07C2531/04 , C07C2531/12 , C07C2531/22
摘要： A process is provided which comprises preparing an olefin oligomerization or trimerization catalyst system and producing olefins in the presence of the olefin oligomerization or trimerization catalyst system and a solvent, wherein said catalyst system preparation comprises the steps of first contacting a chromium source and a pyrrole-containing compound to form a chromium/pyrrole mixture; second, contacting said chromium/pyrrole mixture with a metal alkyl to form a catalyst system; and then contacting said catalyst system with an alpha-olefin, preferably ethylene.
摘要翻译：提供了一种方法，其包括在烯烃低聚或三聚催化剂体系和溶剂的存在下制备烯烃低聚或三聚催化剂体系和生产烯烃，其中所述催化剂体系制备包括以下步骤：首先使铬源和吡咯 - 以形成铬/吡咯混合物; 第二，使所述铬/吡咯混合物与烷基金属接触以形成催化剂体系; 然后使所述催化剂体系与α-烯烃（优选乙烯）接触。

16. 发明申请

US20100113257A1 Compositions and Catalyst Systems of Metal Precursors and Olefinic Diluents 有权
标题翻译：金属前体和烯烃稀释剂的组成和催化剂体系
公开(公告)号：US20100113257A1
公开(公告)日：2010-05-06
申请号：US12609189
申请日：2009-10-30
申请人： Bruce E. Kreischer , Ronald D. Knudsen , Orson L. Sydora
发明人： Bruce E. Kreischer , Ronald D. Knudsen , Orson L. Sydora
IPC分类号： B01J31/00
CPC分类号： B01J31/122 , B01J31/0237 , B01J31/0239 , B01J31/0244 , B01J31/143 , B01J2231/20 , B01J2531/62 , Y02P20/582 , Y10S585/903
摘要： A system and method for preparing and using a metal precursor diluent composition are described. The composition includes a metal precursor, and about 18% to about 80% by weight of an olefinic diluent having between 6 and 18 carbon atoms. Such compositions may be used in oligomerization catalyst systems.
摘要翻译：描述了制备和使用金属前体稀释剂组合物的系统和方法。该组合物包含金属前体，约18％至约80％重量的具有6至18个碳原子的烯烃稀释剂。这种组合物可用于低聚催化剂体系。

17. 发明授权

US06380451B1 Methods for restoring the heat transfer coefficient of an oligomerization reactor 有权
标题翻译：恢复低聚反应器传热系数的方法
公开(公告)号：US06380451B1
公开(公告)日：2002-04-30
申请号：US09474306
申请日：1999-12-29
申请人： Bruce E. Kreischer , Warren M. Ewert , Ronald D. Knudsen
发明人： Bruce E. Kreischer , Warren M. Ewert , Ronald D. Knudsen
IPC分类号： C07C208
CPC分类号： B08B9/08 , B01J19/002 , B01J2219/00252 , C07C2/08 , Y02P20/52 , Y02P20/582 , Y10S585/95
摘要： The specification discloses a method for cleaning an oligomerization reactor after making a higher olefin in the reactor. An olefin is reacted in the presence of a catalyst comprising an aluminum alkyl to form an olefin reaction product. For example, ethylene can be trimerized in the reaction to produce 1-hexene. The reaction also causes a co-product residue of the catalyst to form on the interior surface of the reactor. The interior surface of the reactor is then contacted with an alcohol under conditions effective to remove at least a substantial amount of the catalyst residue from the interior surface of the reactor. The catalyst-removing step can be carried out by combining an alcohol with the process medium used in the reactor. The combined medium can be used to remove both the accumulated polymer co-product and the accumulated catalyst residue from the reactor.
摘要翻译：该说明书公开了在反应器中制备高级烯烃之后清洗低聚反应器的方法。烯烃在包含烷基铝的催化剂的存在下反应以形成烯烃反应产物。例如，乙烯可以在反应中进行三聚，以产生1-己烯。该反应还导致催化剂的副产物残余物在反应器的内表面上形成。然后在有效地从反应器的内表面除去至少大量催化剂残余物的条件下，将反应器的内表面与醇接触。催化剂除去步骤可以通过将醇与反应器中使用的加工介质结合来进行。组合的介质可用于从反应器中除去累积的聚合物共同产物和累积的催化剂残余物。

18. 发明授权

US6045661A Process and apparatus for recovering diluent, monomer, and comonomer from a polymerization reactor effluent 失效
标题翻译：用于从聚合反应器流出物回收稀释剂，单体和共聚单体的方法和设备
公开(公告)号：US6045661A
公开(公告)日：2000-04-04
申请号：US82398
申请日：1998-05-20
申请人： Bruce E. Kreischer , Donald W. Verser , James E. Hein
发明人： Bruce E. Kreischer , Donald W. Verser , James E. Hein
IPC分类号： B01D3/06 , B01D3/14 , C08F6/00
CPC分类号： C08F6/003 , B01D3/06 , B01D3/146
摘要： A process and apparatus are provided for recovering diluent, unreacted monomer, and unreacted comonomer from a polymerization reactor effluent. The comonomer has a boiling point higher than the boiling point of the monomer and the diluent has a boiling point between the boiling points of the monomer and comonomer. The process and apparatus employ at least one flash tank, a first fractionation stage including a first column and operating at a first fractionation pressure, and a second fraction stage including a second column and operating at a higher second fractionation pressure. Comonomer is withdrawn from the first column as a fractionation product, and overhead vapor containing diluent and monomer is substantially condensed to yield a substantially condensed overhead stream. Liquid and vapor from the stream are separated in an accumulator. Vapor and liquid from the accumulator are compressed and pumped, respectively, for delivery to the second fractionation stage at approximately the second fractionation pressure. The pumped liquid is a major portion by weight of the total flow of pumped liquid and compressed vapor to the second fractionation stage. Diluent and monomer are withdrawn from the second column as fractionation products.
摘要翻译：提供了从聚合反应器流出物中回收稀释剂，未反应单体和未反应的共聚单体的方法和装置。共聚单体的沸点高于单体的沸点，稀释剂的沸点在单体和共聚单体的沸点之间。该方法和装置使用至少一个闪蒸罐，包括第一塔并在第一分馏压力下操作的第一分馏阶段和包含第二塔并在较高的第二分馏压力下运行的第二馏分级。共聚单体作为分馏产物从第一塔排出，并且含有稀释剂和单体的塔顶蒸气基本上冷凝以产生基本上冷凝的塔顶馏出物流。来自流的液体和蒸汽在蓄液器中分离。来自蓄能器的蒸汽和液体分别被压缩和泵送，以在大约第二分馏压力下输送到第二分馏级。泵送的液体是泵送液体和压缩蒸气到第二分馏级的总流量的主要部分。稀释剂和单体作为分馏产物从第二塔排出。

19. 发明申请

US20120083609A1 METHODS FOR THE CONVERSION OF A SUBSTITUTED FURAN TO A SUBSTITUTED PYRROLE 有权
标题翻译：将替代糠醛转化为取代的吡咯的方法
公开(公告)号：US20120083609A1
公开(公告)日：2012-04-05
申请号：US12895945
申请日：2010-10-01
申请人： Bruce E. Kreischer , Orson L. Sydora , Steven Hutchinson , Eduardo J. Baralt , Ron D. Knudsen
发明人： Bruce E. Kreischer , Orson L. Sydora , Steven Hutchinson , Eduardo J. Baralt , Ron D. Knudsen
IPC分类号： C07D207/323
CPC分类号： C07D207/323
摘要： The present invention discloses processes for producing substituted pyrrole compounds, such as 2,5-disubstituted pyrroles. Synthetic processes which directly convert substituted furan compounds to substituted pyrrole compounds, via a reaction of the substituted furan compound with ammonia and/or an ammonium salt in the presence of a catalyst, also are described.
摘要翻译：本发明公开了制备取代吡咯化合物如2,5-二取代吡咯的方法。还描述了在催化剂存在下通过取代的呋喃化合物与氨和/或铵盐的反应直接将取代的呋喃化合物转化为取代的吡咯化合物的合成方法。

20. 发明授权

US5641842A Ethylene copolymerization process 失效
标题翻译：乙烯共聚方法
公开(公告)号：US5641842A
公开(公告)日：1997-06-24
申请号：US471894
申请日：1995-06-07
申请人： Max P. McDaniel , Rickey D. Badley , Bruce E. Kreischer , Joseph S. Shveima
发明人： Max P. McDaniel , Rickey D. Badley , Bruce E. Kreischer , Joseph S. Shveima
IPC分类号： C08F4/22 , C08F10/02 , C08F110/02 , C08F210/16 , C08F4/24
CPC分类号： C08F10/02 , C08F110/02 , C08F210/16 , Y10S526/908
摘要： A process is provided comprising copolymerizing, under copolymerizing conditions, ethylene with one or more alpha-olefins, using a catalyst system, where said catalyst system has been sized, to produce a lower-density-copolymer, where said lower-density-copolymer has a density lower than a similar copolymer produced by copolymerizing, under said copolymerizing conditions, ethylene with said one or more alpha-olefins, using said catalyst system, where said catalyst system has not been sized, where said catalyst system that has been sized has had substantially all particles removed that produce, under said copolymerizing conditions, a higher-density-copolymer, where said higher-density-copolymer has a density higher than said similar copolymer.
摘要翻译：提供了一种方法，包括在共聚合条件下使乙烯与一种或多种α-烯烃共聚，使用催化剂体系，其中所述催化剂体系的尺寸被制成低密度共聚物，其中所述低密度共聚物具有通过使用所述催化剂体系在所述共聚条件下共聚乙烯和所述一种或多种α-烯烃，其中所述催化剂体系未被大小化，其中所述催化剂体系的尺寸已经达到规定尺寸基本上所有去除的颗粒在所述共聚条件下产生高密度共聚物，其中所述高密度共聚物的密度高于所述类似的共聚物。

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