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11. 发明授权

US07691256B2 Process for the conversion of heavy charges such as heavy crude oils and distillation residues 有权
标题翻译：用于重质原油和蒸馏残渣转化的方法
公开(公告)号：US07691256B2
公开(公告)日：2010-04-06
申请号：US11311147
申请日：2005-12-20
申请人： Romolo Montanari , Mario Marchionna , Sergio Rosi , Nicoletta Panariti , Alberto Delbianco
发明人： Romolo Montanari , Mario Marchionna , Sergio Rosi , Nicoletta Panariti , Alberto Delbianco
IPC分类号： C10G65/14 , C10G49/22 , C10G45/00 , C10C3/08
CPC分类号： C10G65/18 , C10G67/049 , C10G2300/1033 , C10G2300/107 , C10G2300/1077 , C10G2300/206 , C10G2300/207 , C10G2300/4081 , C10G2300/44 , C10G2300/706
摘要： Heavy hydrocarbon charges are converted in a deasphalting section in the presence of solvents and obtaining two streams, one consisting of deasphalted oil and the other one containing asphaltenes, mixing the deasphalted oil stream with a hydrogenation catalyst and passing the thus obtained mixture to a hydroprocessing section containing hydrogen or hydrogen/H2S, mixing the stream consisting of asphaltenes discharged from the deasphalting section with an appropriate hydrogenation catalyst and passing the obtained mixture to a second hydroprocessing section where it is reacted with hydrogen or a mixture of hydrogen and H2S, passing both the stream containing the reaction product with dispersed catalyst from the hydroprocessing section and the stream containing the reaction product with dispersed catalyst from the second hydroprocessing section, to one or more distillation or flash stages, whereby the more volatile fractions are separated from the distillation residue (tar) or from the liquid discharged from the flash unit, sending the distillation residue (tar) or the liquid discharged from the flash unit, containing the catalyst in the dispersed phase, with a high content of metal sulphides, produced by demetallization of the charge, to a second deasphalting section thereby obtaining deasphalted oil and asphaltenes.
摘要翻译：在溶剂存在下，在脱沥青部分中转化重质烃装料，得到两股流，一种由脱沥青油组成，另一种含有沥青质，将脱沥青油料流与氢化催化剂混合，将得到的混合物通入加氢处理段含有氢或氢/硫化氢，将由脱沥青部分排出的沥青质组成的料流与合适的氢化催化剂混合，并将得到的混合物送入第二加氢处理部分，在其中与氢气或氢气和硫酸氢气的混合物反应，将含有来自加氢处理部分的分散催化剂的反应产物和含有来自第二加氢处理部分的分散催化剂的反应产物的物流转移到一个或多个蒸馏或闪蒸阶段，由此将更多的挥发性馏分与蒸馏残余物（焦油）或从李从闪光单元排出，将含有分散相中的催化剂的闪蒸单元排出的蒸馏残余物（焦油）或通过电荷脱金属产生的高含量金属硫化物送入第二脱沥青从而获得脱沥青油和沥青质。

12. 发明申请

US20090101540A1 PROCESS FOR THE CONVERSION OF HEAVY CHARGES SUCH AS HEAVY CRUDE OILS AND DISTILLATION RESIDUES 审中-公开
标题翻译：重金属转换的过程如重油原油和蒸馏残留物
公开(公告)号：US20090101540A1
公开(公告)日：2009-04-23
申请号：US12248163
申请日：2008-10-09
申请人： Mario MARCHIONNA , Alberto Delbianco , Nicoletta Panariti , Romolo Montanari , Sergio Rosi , Sebastiano Correra
发明人： Mario MARCHIONNA , Alberto Delbianco , Nicoletta Panariti , Romolo Montanari , Sergio Rosi , Sebastiano Correra
IPC分类号： C10G49/18
CPC分类号： C10G67/0454 , C10G67/00 , C10G2300/1033 , C10G2300/107 , C10G2300/1077 , C10G2300/205 , C10G2300/206 , C10G2300/207 , C10G2300/4081 , C10G2300/44 , Y02P30/20
摘要： Process for the conversion of heavy charges such as heavy crude oils, tars from oil sands and distillation residues, by the combined use of the following three process units: hydroconversion with catalysts in slurry phase (HT), distillation or flash (D), deasphalting (SDA), characterized in that the three units operate on mixed streams consisting of fresh charge and recycled streams, by the use of the following steps: sending at least one fraction of the heavy charge to a deasphalting section (SDA) in the presence of hydrocarbon solvents obtaining two streams, one consisting of deasphalted oil (DAO), the other of asphalts; mixing the asphalt with a suitable hydrogenation catalyst and optionally with the remaining fraction of heavy charge not sent to the deasphalting section and sending the mixture obtained to a hydro-treatment reactor (HT) into which hydrogen or a mixture of hydrogen and H2S is charged; sending the stream containing the hydro-treatment reaction product and the catalyst in dispersed phase to one or more distillation or flash steps (D) whereby the most volatile fractions are separated, among which the gases produced in the hydro-treatment reaction; recycling at least 60% by weight, preferably at least 80%, more preferably at least 95%, of the distillation residue (tar) or liquid leaving the flash unit, containing the catalyst in dispersed phase, rich in metallic sulfides produced by demetallation of the charge and possibly coke, to the deasphalting zone.
摘要翻译：通过组合使用以下三个工艺单元，将重质原油，来自油砂和蒸馏残余物的焦油转化为重质装料的方法：用浆液相（HT），蒸馏或闪蒸（D）中的催化剂进行加氢转化，脱沥青（SDA），其特征在于，三个单元通过使用以下步骤在由新鲜电荷和再循环流组成的混合流中操作：将至少一部分重电荷发送到脱沥青部分（SDA），存在烃溶剂获得两股，一种由脱沥青油（DAO），另一种沥青组成; 将沥青与合适的氢化催化剂混合，并且任选地将剩余部分的重质进料混合物送入脱沥青部分，并将得到的混合物送入氢气或氢气与H 2 S的混合物的氢化反应器（HT）中; 将含有分散相中的加氢处理反应产物和催化剂的物流送至一个或多个蒸馏或快速步骤（D），由此分离出最挥发性馏分，其中在加氢处理反应中产生的气体; 回收至少60重量％，优选至少80％，更优选至少95％的蒸馏残余物（焦油）或离开闪蒸单元的液体，其含有分散相中的催化剂，富含金属硫化物，其通过脱金属该充电并可能焦化到脱沥青区。

13. 发明申请

US20060186021A1 Process for the conversion of heavy charges such as heavy crude oils and distillation residues 审中-公开
标题翻译：用于重质原油和蒸馏残渣转化的方法
公开(公告)号：US20060186021A1
公开(公告)日：2006-08-24
申请号：US11404746
申请日：2006-04-17
申请人： Mario Marchionna , Alberto Delbianco , Nicoletta Panariti , Romolo Montanari , Sergio Rosi , Sebastiano Correra
发明人： Mario Marchionna , Alberto Delbianco , Nicoletta Panariti , Romolo Montanari , Sergio Rosi , Sebastiano Correra
IPC分类号： C10G67/04 , C10G55/00 , C10G1/04
CPC分类号： C10G67/0454 , C10G67/00 , C10G2300/1033 , C10G2300/107 , C10G2300/1077 , C10G2300/205 , C10G2300/206 , C10G2300/207 , C10G2300/4081 , C10G2300/44 , Y02P30/20
摘要： Process for the conversion of heavy charges such as heavy crude oils, tars from oil sands and distillation residues, by the combined use of the following three process units: hydroconversion with catalysts in slurry phase (HT), distillation or flash (D), deasphalting (SDA), characterized in that the three units operate on mixed streams consisting of fresh charge and recycled streams, by the use of the following steps: sending at least one fraction of the heavy charge to a deasphalting section (SDA) in the presence of hydrocarbon solvents obtaining two streams, one consisting of deasphalted oil (DAO), the other of asphalts; mixing the asphalt with a suitable hydrogenation catalyst and optionally with the remaining fraction of heavy charge not sent to the deasphalting section and sending the mixture obtained to a hydro-treatment reactor (HT) into which hydrogen or a mixture of hydrogen and H2S is charged; sending the stream containing the hydro-treatment reaction product and the catalyst in dispersed phase to one or more distillation or flash steps (D) whereby the most volatile fractions are separated, among which the gases produced in the hydro-treatment reaction; recycling at least 60% by weight, preferably at least 80%, more preferably at least 95%, of the distillation residue (tar) or liquid leaving the flash unit, containing the catalyst in dispersed phase, rich in metallic sulfides produced by demetallation of the charge and possibly coke, to the deasphalting zone.
摘要翻译：通过组合使用以下三个工艺单元，将重质原油，来自油砂和蒸馏残余物的焦油转化为重质装料的方法：用浆液相（HT），蒸馏或闪蒸（D）中的催化剂进行加氢转化，脱沥青（SDA），其特征在于，三个单元通过使用以下步骤在由新鲜电荷和再循环流组成的混合流中操作：将至少一部分重电荷发送到脱沥青部分（SDA），存在烃溶剂获得两股，一种由脱沥青油（DAO），另一种沥青组成; 将沥青与合适的氢化催化剂混合，并且任选地将剩余部分的重质进料混入未脱沥青部分，并将得到的混合物送入加氢处理反应器（HT），氢气或氢气与H 2的混合物 2 S被充电; 将含有分散相中的加氢处理反应产物和催化剂的物流送至一个或多个蒸馏或快速步骤（D），由此分离出最挥发性馏分，其中在加氢处理反应中产生的气体; 回收至少60重量％，优选至少80％，更优选至少95％的蒸馏残余物（焦油）或离开闪蒸单元的液体，其含有分散相中的催化剂，富含金属硫化物，其通过脱金属该充电并可能焦化到脱沥青区。

14. 发明授权

US08057660B2 Process for the total conversion of heavy feedstocks to distillates 有权
标题翻译：将重质原料总量转化为馏出物的方法
公开(公告)号：US08057660B2
公开(公告)日：2011-11-15
申请号：US12375615
申请日：2007-07-27
申请人： Mario Marchionna , Salvatore Meli , Luigi Patron , Alberto Delbianco , Nicoletta Panariti
发明人： Mario Marchionna , Salvatore Meli , Luigi Patron , Alberto Delbianco , Nicoletta Panariti
IPC分类号： C10G45/00
CPC分类号： C10G67/049 , C10G2300/1033 , C10G2300/107 , C10G2300/1077 , C10G2300/205 , C10G2300/206 , C10G2300/207 , C10G2300/4081 , C10G2300/44 , C10G2400/02 , C10G2400/06
摘要： Process for the conversion of heavy feedstocks selected from heavy crude oils, distillation residues from crude oil or catalytic treatment, “visbreaker tars”, “thermal tars”, bitumens from “oil sands” liquids from coals of different origins and other high boiling feedstocks of a hydrocarbon origin.
摘要翻译：将重质原油，原油蒸馏残渣或催化处理的重质原料转化为不同来源的煤的“油砂”液体和其他高沸点原料的“脱蜡剂焦油”，“热焦油” 烃类来源。

15. 发明申请

US20090261016A1 PROCESS FOR THE TOTAL CONVERSION OF HEAVY FEEDSTOCKS TO DISTILLATES 有权
公开(公告)号：US20090261016A1
公开(公告)日：2009-10-22
申请号：US12375610
申请日：2007-07-27
申请人： Mario Marchionna , Salvatore Meli , Luigi Patron , Alberto Delbianco , Nicoletta Panariti
发明人： Mario Marchionna , Salvatore Meli , Luigi Patron , Alberto Delbianco , Nicoletta Panariti
IPC分类号： C10G45/00
CPC分类号： C10G67/049 , C10G2300/1033 , C10G2300/107 , C10G2300/1077 , C10G2300/205 , C10G2300/206 , C10G2300/207 , C10G2300/4081 , C10G2300/44 , C10G2300/802 , C10G2400/02 , C10G2400/06
摘要： Process for the conversion of heavy feedstocks comprising the following steps: mixing the heavy feedstock with a suitable hydrogenation catalyst and sending the mixture obtained to a first hydrotreatment area (HT1) to which hydrogen or a mixture of hydrogen and H2S are introduced; sending the effluent stream from the first hydrotreatment area (HT1), containing the hydrotreatment reaction product and the catalyst in dispersed phase, to a first distillation area (D1) having one or more flash steps and/or atmospheric distillation and/or vacuum distillation whereby the various fractions coming from the hydrotreatment reaction are separated; sending at least part of the distillation residue (tar) or liquid leaving the flash unit of the first distillation area (D1), containing the catalyst in dispersed phase, rich in metallic sulfides produced by demetallation of the feedstock and optionally minimum quantities of coke, to a deasphalting area (SDA) in the presence of solvents or to a physical separation area, obtaining, in the case of the deasphalting area, two streams, one consisting of deasphalted oil (DAO), the other containing asphaltenes at least partially recycled to the first hydrotreatment area, in the case of the physical separation area, the solids separated and a liquid stream; sending the stream consisting of deasphalted oil (DAO) or the liquid stream separated in the physical separation area to a second hydrotreatment area (HT2), to which hydrogen or a mixture of hydrogen and H2S and a suitable hydrogenation catalyst are introduced; sending the effluent stream from the second hydrotreatment area (HT2), containing the hydrotreatment reaction product and the catalyst in dispersed phase, to a second distillation area (D2) having one or more flash and/or distillation steps whereby the various fractions coming from the second hydrotreatment area are separated; recycling at least part of the distillation residue or liquid leaving the flash unit of the second distillation area (D2), containing the catalyst in dispersed phase to the second hydrotreatment area (HT2).

16. 发明授权

US08147675B2 Process for the total conversion of heavy feedstocks to distillates 有权
标题翻译：将重质原料总量转化为馏出物的方法
公开(公告)号：US08147675B2
公开(公告)日：2012-04-03
申请号：US12375610
申请日：2007-07-27
申请人： Mario Marchionna , Salvatore Meli , Luigi Patron , Alberto Delbianco , Nicoletta Panariti
发明人： Mario Marchionna , Salvatore Meli , Luigi Patron , Alberto Delbianco , Nicoletta Panariti
IPC分类号： C10G45/00
CPC分类号： C10G67/049 , C10G2300/1033 , C10G2300/107 , C10G2300/1077 , C10G2300/205 , C10G2300/206 , C10G2300/207 , C10G2300/4081 , C10G2300/44 , C10G2300/802 , C10G2400/02 , C10G2400/06
摘要： A process for the conversion of heavy feedstocks selected from heavy crude oils, distillation residues from crude oil or coming from catalytic treatment, visbreaker tars, thermal tars, bitumens from oil sands, liquids from coats of different origins and other high-boiling feedstocks of a hydrocarbon nature known as “black oils.”
摘要翻译：用于将重质原油，原油蒸馏残渣或来自催化处理的重质原料转化成重质原料的方法，来自油砂的热粘焦油，来自油砂的沥青，来自不同来源的涂料的液体和其它高沸点原料烃性质被称为“黑油”。

17. 发明授权

US5017282A Single-step coal liquefaction process 失效
标题翻译：单步煤液化过程
公开(公告)号：US5017282A
公开(公告)日：1991-05-21
申请号：US247855
申请日：1988-09-22
申请人： Alberto Delbianco , Ermanno Girardi
发明人： Alberto Delbianco , Ermanno Girardi
IPC分类号： C10G1/00
CPC分类号： C10G1/00
摘要： A process for the single-step coal liquefaction is disclosed, which comprises reacting coal in an aqueous suspension with carbon monoxide in the presence of a CO-conversion catalyst selected from the group consisting of an alkaline hydroxide and a carbonate, and in the presence of a hydrogenation catalyst selected from the group consisting of transition metals and compounds thereof, by operating at temperatures within the range of from 300.degree. to 450.degree. C. for a reaction time within the range of from 30 to 80 minutes.

18. 发明授权

US5690176A Composition effective in removing asphaltenes 失效
标题翻译：组合物有效去除沥青质
公开(公告)号：US5690176A
公开(公告)日：1997-11-25
申请号：US615535
申请日：1996-03-12
申请人： Alberto Delbianco , Fabrizio Stroppa
发明人： Alberto Delbianco , Fabrizio Stroppa
IPC分类号： E21B37/06 , C09K8/524 , F28G9/00 , E21B37/00 , E21B43/12
CPC分类号： F28G9/00 , C09K8/524 , Y10S507/93
摘要： Process for the dissolution of asphaltene sediments in oil wells which consists in introducing a solubilizing composition for the above asphaltenes into the oil wells, characterized in that the solubilizing composition comprises: (a) a basically hydrocarbon fraction consisting of at least 70%, preferably at least 80% by weight, of aromatic and alkyl aromatic hydrocarbons, the alkyl group being from C.sub.1 to C.sub.4 ; (b) a fraction basically consisting of quinoline and isoquinoline as such or alkyl substituted, preferably as such, the alkyl group being from C.sub.1 to C.sub.4 ; the weight ratio between fraction (a) and (b) being from 97.5/2.5 to 75/25, preferably from 97/3 to 90/10.
摘要翻译：沥青质沉淀物在油井中溶解的方法，其包括将用于上述沥青质的增溶组合物引入油井中，其特征在于，所述增溶组合物包含：（a）基本上由以下组成的烃馏分：至少70％至少80重量％的芳族和烷基芳族烃，该烷基为C1至C4; （b）基本上由喹啉和异喹啉组成的馏分或烷基取代，优选为烷基取代为C1至C4; 级分（a）和（b）之间的重量比为97.5 / 2.5〜75/25，优选为97/3〜90/10。

19. 发明授权

US4968414A Process for single-step coal liquefaction 失效
标题翻译：单步煤液化过程
公开(公告)号：US4968414A
公开(公告)日：1990-11-06
申请号：US251136
申请日：1988-09-29
申请人： Alberto Delbianco , Ermanno Girardi
发明人： Alberto Delbianco , Ermanno Girardi
IPC分类号： C10G1/00 , C10G1/04 , C10G1/06
CPC分类号： C10G1/047 , C10G1/00
摘要： A process for the single-step coal liquefaction is disclosed, which comprises reacting the coal in an aqueous suspension with carbon monoxide in the presence of a CO-conversion catalyst selected from an alkaline hydroxide or carbonate, wherein the reaction takes place at a temperature maintained for a time of up to about 20 minutes equal to a value selected within the range of from about 300.degree. to 370.degree. C., and then is increased over a time within the range of from about 20 to 40 minutes, until a temperature value is reached, within the range of from about 420.degree. to 450.degree. C. and is kept constant for a time of up to about 20 minutes.

20. 发明授权

US5128017A Single-step coal liquefaction process 失效
标题翻译：单步煤液化过程
公开(公告)号：US5128017A
公开(公告)日：1992-07-07
申请号：US653513
申请日：1991-02-11
申请人： Alberto Delbianco , Ermanno Girardi
发明人： Alberto Delbianco , Ermanno Girardi
IPC分类号： C10G1/00
CPC分类号： C10G1/00
摘要： A process for the single-step coal liquefaction is disclosed, which comprises reacting coal in an aqueous suspension with carbon monoxide in the presence of a CO-conversion catalyst selected from the group consisting of an alkaline hydroxide and a carbonate, and in the presence of a hydrogenation catalyst selected from the group consisting of transition metals and compounds thereof, by operating at temperatures within the range of from 300.degree. to 450.degree. C. for a reaction time within the range of from 30 to 80 minutes.
摘要翻译：公开了单步煤液化的方法，其包括在水悬浮液中的煤与一氧化碳在选自碱金属氢氧化物和碳酸盐的CO转化催化剂存在下反应，并在选自过渡金属和其化合物的加氢催化剂，通过在300-450℃的温度范围内操作，反应时间在30-80分钟的范围内。

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