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11. 发明授权

US6007586A Pigment dyeing and pigment printing process 失效
标题翻译：颜料染色和颜料印花工艺
公开(公告)号：US6007586A
公开(公告)日：1999-12-28
申请号：US100001
申请日：1998-06-17
申请人： Peter Aeschlimann , Paul Herzig
发明人： Peter Aeschlimann , Paul Herzig
IPC分类号： C09B56/12 , C09B29/01 , C09B29/42 , C09B29/46 , D06P1/44 , D06P1/02 , D06P1/14
CPC分类号： D06P1/44 , C09B29/0022 , C09B29/363 , C09B29/3652
摘要： The present invention describes a process for dyeing or printing fiber material by the pigment dyeing or pigment printing process, which comprises applying to the fiber material, and subsequently fixing, a dyeing liquor or a print paste comprising at least one dye of the formulaD--(X).sub.n (1)in whichD is a radical of an insoluble organic dye of the phthalocyanine, perinone, indigoid, thioindigoid, dioxazine, diketopyrrolopyrrole, isoindolinone, perylene, quinacridone, metal complex, monoazo, disazo, trisazo or anthraquinone series, X is a hydrophilic polar radical, and n is 1, 2 or 3, and at least one pigment dye binder, and also, if desired, further auxiliaries.
摘要翻译：本发明描述了通过颜料染色或颜料印刷方法对纤维材料进行染色或印花的方法，该方法包括向纤维材料施加染色液或印刷浆料，染色液或印刷浆料包含至少一种式D-（ X）n（1）其中D是酞菁，百里香酮，靛类，硫靛，二恶嗪，二酮吡咯并吡咯，异吲哚啉酮，苝，喹吖啶酮，金属络合物，单偶氮，二偶氮，三偶氮或蒽醌系列的不溶性有机染料的基团，X 是亲水性极性基团，n为1,2或3，以及至少一种颜料染料粘合剂，以及如果需要，还有其它助剂。

12. 发明授权

US6008332A Phthalimidylazo dyes, process for their preparation and the use thereof 失效
标题翻译：邻苯二甲酰亚氨基偶氮染料，其制备方法及其用途
公开(公告)号：US6008332A
公开(公告)日：1999-12-28
申请号：US682201
申请日：1996-07-17
申请人： Paul Herzig , Romeo Dreier
发明人： Paul Herzig , Romeo Dreier
IPC分类号： C09B29/00 , C09B29/08 , C09B29/036 , C09B29/09 , D06P1/18 , D06P3/42
CPC分类号： C09B29/0809 , C09B29/0033
摘要： Disperse azo dyes of formula ##STR1## wherein R.sub.1 is hydrogen, C.sub.1 -C.sub.2 alkyl, halogen, NH--CO--R.sub.5 or O--SO.sub.2 --R.sub.6 ; R.sub.2 is hydrogen, halogen, C.sub.1 -C.sub.4 alkyl, unsubstituted C.sub.1 -C.sub.8 alkoxy or C.sub.1 -C.sub.8 alkoxy which is substituted by halogen, cyano, phenyl, --Y--C.sub.1 -C.sub.8 alkyl or --Y-phenyl; R.sub.3 is unsubstituted C.sub.1 -C.sub.8 alkyl or C.sub.1 -C.sub.8 alkyl which is substituted by hydroxy, cyano, vinyl, phenyl, halogen, --X-phenyl or --X--C.sub.1 -C.sub.8 alkyl, and --X--C.sub.1 -C.sub.8 alkyl may be substituted by halogen or cyano and --X-phenyl may be substituted by C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.4 alkoxy or halogen; R.sub.4 is hydrogen or, independently of R.sub.3, has the meaning of R.sub.3, and R.sub.3 and R.sub.4, together with the linking nitrogen atom, can also be a heterocyclic radical; R.sub.5 is unsubstituted C.sub.1 -C.sub.3 alkyl or C.sub.1 -C.sub.3 alkyl which is substituted by halogen, phenyl, cyano or C.sub.1 -C.sub.3 alkoxy; R.sub.6 is unsubstituted C.sub.1 -C.sub.4 alkyl or C.sub.1 -C.sub.4 alkyl which is substituted by halogen, cyano or phenyl, and phenyl in turn may be substituted by C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.4 alkoxy or halogen; Y is a linking group of formula --O--, --S-- or --SO.sub.2 --; and X is a linking group of formula --O--, ##STR2## The novel disperse azo dyes of formula (1) are suitable in particular for dyeing polyester textile material.
摘要翻译：分散式的偶氮染料其中R1是氢，C1-C2烷基，卤素，NH-CO-R5或O-SO2-R6; R 2是氢，卤素，C 1 -C 4烷基，未取代的C 1 -C 8烷氧基或被卤素，氰基，苯基，-Y-C 1 -C 8烷基或-Y-苯基取代的C 1 -C 8烷氧基; R3是未取代的C1-C8烷基或被羟基，氰基，乙烯基，苯基，卤素，-X-苯基或-X-C1-C8烷基取代的C1-C8烷基，-X-C1-C8烷基可以被卤素或氰基和-X-苯基可以被C1-C4烷基，C1-C4烷氧基或卤素取代; R4是氢或独立地是R3，具有R3的含义，R3和R4与连接氮原子一起也可以是杂环基; R 5是被卤素，苯基，氰基或C 1 -C 3烷氧基取代的未取代的C 1 -C 3烷基或C 1 -C 3烷基; R6是未取代的C1-C4烷基或被卤素，氰基或苯基取代的C1-C4烷基，苯基又可被C1-C4烷基，C1-C4烷氧基或卤素取代; Y是式-O - ， - S-或-SO 2 - 的连接基团; 并且X是式-O-的连接基团。式（1）的新型分散偶氮染料特别适用于染色聚酯纺织材料。

13. 发明授权

US5942604A Azo dye mixtures 失效
标题翻译：偶氮染料混合物
公开(公告)号：US5942604A
公开(公告)日：1999-08-24
申请号：US27479
申请日：1998-02-20
申请人： Paul Herzig , Antoine Clement , Romeo Dreier , Alfons Arquint
发明人： Paul Herzig , Antoine Clement , Romeo Dreier , Alfons Arquint
IPC分类号： C09B29/08 , C07C229/16 , C07C233/43 , C09B29/085 , C09B67/22 , C09B67/36 , D06P1/02 , C07C219/06 , C09B41/00
CPC分类号： C09B67/0051 , C07C229/16 , C07C233/43 , Y10S534/01 , Y10S8/922
摘要： A dye mixture, which comprises as component (A) a dye of formula as component (B) a dye of formula ##STR1## and/or as component (C) a dye of formula ##STR2## wherein D, X and Y are as defined in the specification. These dyes are particularly suitable for dyeing polyester fiber textile material.
摘要翻译：作为组分（A）的染料混合物，其包含式（B）的染料，式（B）的染料和/或作为组分（C）的染料，其中D，X和Y如说明书中所定义。这些染料特别适用于染色聚酯纤维纺织材料。

14. 发明授权

US5939579A Disperse dyes 失效
公开(公告)号：US5939579A
公开(公告)日：1999-08-17
申请号：US110595
申请日：1998-07-06
申请人： Paul Herzig , Antoine Clement , Alfons Arquint
发明人： Paul Herzig , Antoine Clement , Alfons Arquint
IPC分类号： C09B29/085 , C07C233/43 , C09B29/08 , C09B29/26
CPC分类号： C07C233/43 , C09B29/0817 , Y10S8/922
摘要： Disperse dyes of formula wherein R is nitro or cyano, R.sub.1 is halogen, R.sub.2 is C.sub.1 -C.sub.4 alkyl which is unsubstituted or substituted by C.sub.1 -C.sub.3 alkoxy, halogen, cyano or phenyl, R.sub.3 is C.sub.1 -C.sub.4 alkyl, R.sub.4 is methyl or ethyl, R.sub.5 is hydrogen, methyl or ethyl, and R.sub.6 is methyl or ethyl, with the proviso that R.sub.5 is not hydrogen if R is nitro, R.sub.1 is halogen and R.sub.2 is C.sub.1 -C.sub.4 alkyl.These dyes are particularly suitable for dyeing and printing textile materials consisting of polyester fibres.

15. 发明授权

US5665125A Mixtures of fibre-reactive ring-opened phthalimidylazo dyes 失效
标题翻译：纤维反应开环的邻苯二甲酰亚氨基偶氮染料的混合物
公开(公告)号：US5665125A
公开(公告)日：1997-09-09
申请号：US579189
申请日：1995-12-27
申请人： Paul Herzig , Anton Andreoli
发明人： Paul Herzig , Anton Andreoli
IPC分类号： C09B62/51 , C09B62/44 , C09B62/507 , C09B62/513 , C09B67/22 , C09B62/00 , D06P1/382 , D06P1/384 , D06P3/66
CPC分类号： C09B62/4411 , C09B62/507 , C09B67/0047 , Y10S8/918
摘要： Mixtures comprising a compound of the formula ##STR1## and a compound of the formula ##STR2## in which K is the radical of a coupling component, s is the same in the compounds of formulae (16a) and (16b) and is the number 1 or 2, R and R' are each hydrogen, sulfo, hydroxyl, C.sub.1 -C.sub.4 alkoxy, halogen or cyano, A is C.sub.1 -C.sub.6 alkylene which is optionally substituted by halogen, hydroxyl, sulfato, carboxyl, cyano, C.sub.2 -C.sub.4 alkanoyloxy, C.sub.1 -C.sub.4 alkoxycarbonyl or carbamoyl or interrupted by a group --O-- or --NR"--, or is C.sub.1 -C.sub.6 alkylenephenylene which is unsubstituted or substituted in the phenyl part by C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.4 alkoxy, halogen or sulfo, and R" is hydrogen or C.sub.1 -C.sub.4 alkyl, and the ratio of the compounds of formulae (16a) and (16b) is about 1:1, are suitable as fibre-reactive dyes for dyeing or printing widely varying fibre materials.
摘要翻译：包含下式化合物（16a）和式（16b）化合物的混合物，其中K是偶联组分的基团，s在式（16a）和（ 16b，并且是数1或2，R和R'各自为氢，磺基，羟基，C 1 -C 4烷氧基，卤素或氰基，A为任选被卤素，羟基，硫酸根，羧基，氰基， C 1 -C 4烷酰氧基，C 1 -C 4烷氧基羰基或氨基甲酰基或被-O-或-NR“基团中断，或者是未被取代或被苯基部分被C1-C4烷基，C1-C4烷氧基，卤素或磺基取代的C1-C6亚烷基亚苯基，并且R“是氢或C 1 -C 4烷基，式（16a）和（16b）化合物的比例为约1:1可适用于用于染色或印刷广泛变化的纤维材料的纤维活性染料。

16. 发明授权

US5532345A Fiber reactive phthalimidylazo dyes and use thereof 失效
标题翻译：纤维反应性苯二酰亚氨基偶氮染料及其用途
公开(公告)号：US5532345A
公开(公告)日：1996-07-02
申请号：US451354
申请日：1995-05-26
申请人： Paul Herzig , Anton Andreoli
发明人： Paul Herzig , Anton Andreoli
IPC分类号： C09B62/51 , C09B62/44 , C09B62/507 , C09B62/513 , C09B67/22 , C09B62/006 , C09B62/08 , D06P1/38
CPC分类号： C09B62/4411 , C09B62/507 , C09B67/0047 , Y10S8/918
摘要： Compounds of the formula ##STR1## in which the variables are as defined in the claims, which are suitable as fibre-reactive dyes for dyeing or printing widely varying fibre materials, are described.
摘要翻译：描述了其中变量如权利要求中所定义的式（IMA）（1）的化合物，其适用于用于染色或印刷广泛变化的纤维材料的纤维活性染料。

17. 发明授权

US6034226A Disperse dyes 有权
标题翻译：分散染料
公开(公告)号：US6034226A
公开(公告)日：2000-03-07
申请号：US311093
申请日：1999-05-13
申请人： Paul Herzig , Antoine Clement , Alfons Arquint
发明人： Paul Herzig , Antoine Clement , Alfons Arquint
IPC分类号： C09B29/085 , C07C233/43 , C09B29/08 , C09B29/26 , C09B67/38 , D06P3/54
CPC分类号： C07C233/43 , C09B29/0817 , Y10S8/922
摘要： Disperse dyes of formula ##STR1## wherein R is nitro or cyano, R.sub.1 is halogen, R.sub.2 is C.sub.1 -C.sub.4 alkyl which is unsubstituted or substituted by C.sub.1 -C.sub.3 alkoxy, halogen, cyano or phenyl, R.sub.3 is C.sub.1 -C.sub.4 alkyl, R.sub.4 is methyl or ethyl, R.sub.5 is hydrogen, methyl or ethyl, and R6 is methyl or ethyl, with the proviso that R.sub.5 is not hydrogen if R is nitro, R.sub.1 is halogen and R.sub.2 is C.sub.1 -C.sub.4 alkyl.These dyes are particularly suitable for dyeing and printing textile materials consisting of polyester fibres.
摘要翻译：卤素，氰基或苯基取代的未取代或取代的C1-C4烷基，R3是C1-C4烷基，R4是甲基或乙基，R5是氢，甲基或乙基，R6是甲基或乙基，条件是如果R是硝基，则R 5不是氢，R 1是卤素，R 2是C 1 -C 4烷基。这些染料特别适用于染色和印花由聚酯纤维组成的纺织品。

18. 发明授权

US5869628A Disperse dyes 失效
标题翻译：分散染料
公开(公告)号：US5869628A
公开(公告)日：1999-02-09
申请号：US918883
申请日：1997-08-26
申请人： Paul Herzig , Antoine Clement
发明人： Paul Herzig , Antoine Clement
IPC分类号： C09B29/08 , C09B67/38 , D06P3/54 , C09B29/085 , D06P1/18
CPC分类号： C09B29/0817 , Y10S8/922
摘要： Disperse dyes of formula ##STR1## wherein R.sub.1 is chloro or bromo,R.sub.2 is methyl or ethyl, andR.sub.3 is methyl or ethyl.The dyes are particularly suitable for dyeing or printing polyester fiber textile material.
摘要翻译：式（1）的分散染料其中R1是氯或溴，R2是甲基或乙基，R3是甲基或乙基。该染料特别适用于染色或印花聚酯纤维纺织材料。

19. 发明授权

US5189206A Process for the preparation of aminobenzenesulfonic acids 失效
标题翻译：制备氨基苯磺酸的方法
公开(公告)号：US5189206A
公开(公告)日：1993-02-23
申请号：US746131
申请日：1991-08-12
申请人： Paul Herzig
发明人： Paul Herzig
IPC分类号： C07C303/06 , C07C309/46 , C07C309/48 , C07C309/49 , C09B62/44
CPC分类号： C09B62/4413 , C07C303/06
摘要： There is disclosed a process for the preparation of compounds of formula ##STR1## wherein the symbols are as defined in claim 1, which process comprises dissolving a compound of formula ##STR2## in sulfuric acid, adding this solution to oleum and reacting the mixture in the temperature range from 10.degree. to 80.degree. C. until a sulfo group has been completely introduced, and, in an optional further step, subjecting the reaction mixture to further reaction in the temperature range from 100.degree. to 200.degree. C. to introduce a second sulfo group.The compounds of formula (1) obtainable by this process are useful intermediates for the synthesis of dyes and are particularly suitable diazo components for the synthesis of azo dyes.
摘要翻译：公开了制备式（1）化合物的方法，其中符号如权利要求1所定义，该方法包括将式（2）化合物溶解在硫酸中，将该溶液加入到将该混合物在10℃至80℃的温度范围内反应直到磺基完全引入，并且在任选的另外步骤中，将反应混合物在100至200℃的温度范围内进一步反应以引入第二个磺基。通过该方法可获得的式（1）化合物是用于合成染料的有用的中间体，并且是用于合成偶氮染料的特别合适的重氮组分。

20. 发明授权

US5576445A Intermediates for reactive dyes 失效
标题翻译：活性染料中间体
公开(公告)号：US5576445A
公开(公告)日：1996-11-19
申请号：US451355
申请日：1995-05-26
申请人： Paul Herzig , Anton Andreoli
发明人： Paul Herzig , Anton Andreoli
IPC分类号： C07C317/28 , C07C317/32 , C07D209/48 , C09B62/008 , C09B62/343 , C09B62/51
CPC分类号： C07D209/48 , C09B62/51
摘要： Compounds of the formula ##STR1## in which the variables are as defined in the claims and which are suitable diazo components for the synthesis of fibre-reactive dyes are described.
摘要翻译：描述了其中变量如权利要求中所定义并且是用于合成纤维活性染料的合适的重氮组分的式（IMA）（1）的化合物。

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