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11. 发明授权

US08188153B2 Fischer-Tropsch synthesis using microchannel technology and novel catalyst and microchannel reactor 有权
标题翻译：使用微通道技术的费 - 托合成和新型催化剂和微通道反应器
公开(公告)号：US08188153B2
公开(公告)日：2012-05-29
申请号：US12718356
申请日：2010-03-05
申请人： Yong Wang , Anna Lee Tonkovich , Terry Mazanec , Francis P. Daly , Dave VanderWiel , Jianli Hu , Chunshe Cao , Charles Kibby , Xiaohong Shari Li , Michael D. Briscoe , Nathan Gano , Ya-Huei Chin
发明人： Yong Wang , Anna Lee Tonkovich , Terry Mazanec , Francis P. Daly , Dave VanderWiel , Jianli Hu , Chunshe Cao , Charles Kibby , Xiaohong Shari Li , Michael D. Briscoe , Nathan Gano , Ya-Huei Chin
IPC分类号： C07C27/00 , B01J8/00
CPC分类号： C10G2/332 , B01J19/0093 , B01J21/04 , B01J23/75 , B01J23/8896 , B01J23/8913 , B01J35/0066 , B01J35/1019 , B01J35/1038 , B01J35/1042 , B01J37/0205 , B01J2219/00783 , B01J2219/00822 , B01J2219/00824 , B01J2219/00826 , B01J2219/00831 , B01J2219/00835 , B01J2219/00844 , B01J2219/0086 , B01J2219/00873 , C10G2/341 , C10G2300/301 , C10G2300/4018 , C10G2300/4025 , C10G2300/70 , C10G2400/04 , C10G2400/10 , Y02P20/582
摘要： The disclosed invention relates to a process for converting a reactant composition comprising H2 and CO to a product comprising at least one aliphatic hydrocarbon having at least about 5 carbon atoms, the process comprising: flowing the reactant composition through a microchannel reactor in contact with a Fischer-Tropsch catalyst to convert the reactant composition to the product, the microchannel reactor comprising a plurality of process microchannels containing the catalyst; transferring heat from the process microchannels to a heat exchanger; and removing the product from the microchannel reactor; the process producing at least about 0.5 gram of aliphatic hydrocarbon having at least about 5 carbon atoms per gram of catalyst per hour; the selectivity to methane in the product being less than about 25%. The disclosed invention also relates to a supported catalyst comprising Co, and a microchannel reactor comprising at least one process microchannel and at least one adjacent heat exchange zone.
摘要翻译：所公开的发明涉及将包含H 2和CO的反应物组合物转化为包含至少一种具有至少约5个碳原子的脂族烃的产物的方法，该方法包括：使反应物组合物流过与Fischer接触的微通道反应器 - 催化剂将反应物组合物转化成产物，微通道反应器包含多个含有催化剂的工艺微通道; 将热量从工艺微通道传递到热交换器; 并从微通道反应器中除去产物; 该方法每小时产生至少约0.5克具有至少约5个碳原子的每克催化剂的脂族烃; 产品中甲烷的选择性小于约25％。所公开的发明还涉及包含Co的载体催化剂和包含至少一个工艺微通道和至少一个相邻的热交换区的微通道反应器。

12. 发明授权

US08062623B2 Stable, catalyzed, high temperature combustion in microchannel, integrated combustion reactors 有权
标题翻译：在微通道，综合燃烧反应堆中稳定，催化，高温燃烧
公开(公告)号：US08062623B2
公开(公告)日：2011-11-22
申请号：US10966162
申请日：2004-10-15
申请人： Francis P. Daly , Junko M. Watson , Yong Wang , Jianli Hu , Chunshe Cao , Richard Long
发明人： Francis P. Daly , Junko M. Watson , Yong Wang , Jianli Hu , Chunshe Cao , Richard Long
IPC分类号： C01B3/26
CPC分类号： B01J19/0093 , B01J23/42 , B01J23/6567 , B01J35/0006 , B01J35/04 , B01J35/06 , B01J37/0225 , B01J37/0226 , B01J37/0238 , B01J2219/00783 , B01J2219/00822 , B01J2219/00835 , B01J2219/0086 , B01J2219/00873 , B01J2219/00889 , B01J2219/00891 , C01B3/384 , C01B3/386 , C01B2203/0233 , C01B2203/0261 , C01B2203/0811 , C01B2203/0822 , C01B2203/0827 , C01B2203/0844 , C01B2203/1041 , C01B2203/107 , C01B2203/1241 , C01B2203/141 , C01B2203/82 , F23C13/00 , F23C2900/03001 , Y02P20/128 , Y02P20/52
摘要： Catalysts containing 30 weight percent or more platinum have surprisingly been discovered to possess superior stability and activity for catalyzing combustion reactions. The addition of rhenium improves catalyst performance in fuel lean conditions but has undesirable effects in fuel rich conditions. The invention provides integrated combustion microreactors, chemical systems utilizing these integrated combustion microreactors, methods of combustion, and methods of providing heat to endothermic reactions in integrated combustion microreactors.
摘要翻译：令人惊奇地发现含有30重量％或更多的铂的催化剂具有优异的催化燃烧反应的稳定性和活性。添加铼提高了燃料贫乏条件下的催化剂性能，但在富燃料条件下具有不良影响。本发明提供了综合燃烧微反应器，利用这些综合燃烧微反应器的化学系统，燃烧方法和向集成燃烧微反应器中的吸热反应提供热量的方法。

13. 发明申请

US20100160463A1 FISCHER-TROPSCH SYNTHESIS USING MICROCHANNEL TECHNOLOGY AND NOVEL CATALYST AND MICROCHANNEL REACOTR 有权
标题翻译：使用微通道技术和新型催化剂和微通道反应器进行FISCHER-TROPSCH合成
公开(公告)号：US20100160463A1
公开(公告)日：2010-06-24
申请号：US12718356
申请日：2010-03-05
申请人： Yong Wang , Anna Lee Tonkovich , Terry Mazanec , Francis P. Daly , Dave VanderWiel , Jianli Hu , Chunshe Cao , Charles Kibby , Xiaohong Shari Li , Michael D. Briscoe , Nathan Gano , Ya-Huei Chin
发明人： Yong Wang , Anna Lee Tonkovich , Terry Mazanec , Francis P. Daly , Dave VanderWiel , Jianli Hu , Chunshe Cao , Charles Kibby , Xiaohong Shari Li , Michael D. Briscoe , Nathan Gano , Ya-Huei Chin
IPC分类号： C07C1/04 , B01J8/02
CPC分类号： C10G2/332 , B01J19/0093 , B01J21/04 , B01J23/75 , B01J23/8896 , B01J23/8913 , B01J35/0066 , B01J35/1019 , B01J35/1038 , B01J35/1042 , B01J37/0205 , B01J2219/00783 , B01J2219/00822 , B01J2219/00824 , B01J2219/00826 , B01J2219/00831 , B01J2219/00835 , B01J2219/00844 , B01J2219/0086 , B01J2219/00873 , C10G2/341 , C10G2300/301 , C10G2300/4018 , C10G2300/4025 , C10G2300/70 , C10G2400/04 , C10G2400/10 , Y02P20/582
摘要： The disclosed invention relates to a process for converting a reactant composition comprising H2 and CO to a product comprising at least one aliphatic hydrocarbon having at least about 5 carbon atoms, the process comprising: flowing the reactant composition through a microchannel reactor in contact with a Fischer-Tropsch catalyst to convert the reactant composition to the product, the microchannel reactor comprising a plurality of process microchannels containing the catalyst; transferring heat from the process microchannels to a heat exchanger; and removing the product from the microchannel reactor; the process producing at least about 0.5 gram of aliphatic hydrocarbon having at least about 5 carbon atoms per gram of catalyst per hour; the selectivity to methane in the product being less than about 25%. The disclosed invention also relates to a supported catalyst comprising Co, and a microchannel reactor comprising at least one process microchannel and at least one adjacent heat exchange zone.
摘要翻译：所公开的发明涉及将包含H 2和CO的反应物组合物转化为包含至少一种具有至少约5个碳原子的脂族烃的产物的方法，该方法包括：使反应物组合物流过与Fischer接触的微通道反应器 - 催化剂将反应物组合物转化成产物，微通道反应器包含多个含有催化剂的工艺微通道; 将热量从工艺微通道传递到热交换器; 并从微通道反应器中除去产物; 该方法每小时产生至少约0.5克具有至少约5个碳原子的每克催化剂的脂族烃; 产品中甲烷的选择性小于约25％。所公开的发明还涉及包含Co的载体催化剂和包含至少一个工艺微通道和至少一个相邻的热交换区的微通道反应器。

14. 发明申请

US20060083675A1 Stable, catalyzed, high temperature combustion in microchannel, integrated combustion reactors 有权
标题翻译：在微通道，综合燃烧反应堆中稳定，催化，高温燃烧
公开(公告)号：US20060083675A1
公开(公告)日：2006-04-20
申请号：US10966162
申请日：2004-10-15
申请人： Francis Daly , Junko Watson , Yong Wang , Jianli Hu , Chunshe Cao , Richard Long
发明人： Francis Daly , Junko Watson , Yong Wang , Jianli Hu , Chunshe Cao , Richard Long
IPC分类号： C01B3/26 , B01J8/02
CPC分类号： B01J19/0093 , B01J23/42 , B01J23/6567 , B01J35/0006 , B01J35/04 , B01J35/06 , B01J37/0225 , B01J37/0226 , B01J37/0238 , B01J2219/00783 , B01J2219/00822 , B01J2219/00835 , B01J2219/0086 , B01J2219/00873 , B01J2219/00889 , B01J2219/00891 , C01B3/384 , C01B3/386 , C01B2203/0233 , C01B2203/0261 , C01B2203/0811 , C01B2203/0822 , C01B2203/0827 , C01B2203/0844 , C01B2203/1041 , C01B2203/107 , C01B2203/1241 , C01B2203/141 , C01B2203/82 , F23C13/00 , F23C2900/03001 , Y02P20/128 , Y02P20/52
摘要： Catalysts containing 30 weight percent or more platinum have surprisingly been discovered to possess superior stability and activity for catalyzing combustion reactions. The addition of rhenium improves catalyst performance in fuel lean conditions but has undesirable effects in fuel rich conditions. The invention provides integrated combustion microreactors, chemical systems utilizing these integrated combustion microreactors, methods of combustion, and methods of providing heat to endothermic reactions in integrated combustion microreactors.
摘要翻译：令人惊奇地发现含有30重量％或更多的铂的催化剂具有优异的催化燃烧反应的稳定性和活性。添加铼提高了燃料贫乏条件下的催化剂性能，但在富燃料条件下具有不良影响。本发明提供了综合燃烧微反应器，利用这些综合燃烧微反应器的化学系统，燃烧方法和向集成燃烧微反应器中的吸热反应提供热量的方法。

15. 发明申请

US20050165121A1 Fischer-Tropsch synthesis using microchannel technology and novel catalyst and microchannel reactor 有权
标题翻译：使用微通道技术的费 - 托合成和新型催化剂和微通道反应器
公开(公告)号：US20050165121A1
公开(公告)日：2005-07-28
申请号：US10766297
申请日：2004-01-28
申请人： Yong Wang , Anna Tonkovich , Terry Mazanec , Francis Daly , Dave VanderWiel , Jianli Hu , Chunshe Cao , Charles Kibby , Xiaohong Li , Michael Briscoe , Nathan Gano , Ya-Huei Chin
发明人： Yong Wang , Anna Tonkovich , Terry Mazanec , Francis Daly , Dave VanderWiel , Jianli Hu , Chunshe Cao , Charles Kibby , Xiaohong Li , Michael Briscoe , Nathan Gano , Ya-Huei Chin
IPC分类号： B01J19/00 , B01J19/24 , B01J21/04 , B01J23/75 , B01J23/889 , B01J23/89 , B01J35/10 , B01J37/02 , C10G2/00 , C07C27/26
CPC分类号： C10G2/332 , B01J19/0093 , B01J21/04 , B01J23/75 , B01J23/8896 , B01J23/8913 , B01J35/0066 , B01J35/1019 , B01J35/1038 , B01J35/1042 , B01J37/0205 , B01J2219/00783 , B01J2219/00822 , B01J2219/00824 , B01J2219/00826 , B01J2219/00831 , B01J2219/00835 , B01J2219/00844 , B01J2219/0086 , B01J2219/00873 , C10G2/341 , C10G2300/301 , C10G2300/4018 , C10G2300/4025 , C10G2300/70 , C10G2400/04 , C10G2400/10 , Y02P20/582
摘要： The disclosed invention relates to a process for converting a reactant composition comprising H2 and CO to a product comprising at least one aliphatic hydrocarbon having at least about 5 carbon atoms, the process comprising: flowing the reactant composition through a microchannel reactor in contact with a Fischer-Tropsch catalyst to convert the reactant composition to the product, the microchannel reactor comprising a plurality of process microchannels containing the catalyst; transferring heat from the process microchannels to a heat exchanger; and removing the product from the microchannel reactor; the process producing at least about 0.5 gram of aliphatic hydrocarbon having at least about 5 carbon atoms per gram of catalyst per hour; the selectivity to methane in the product being less than about 25%. The disclosed invention also relates to a supported catalyst comprising Co, and a microchannel reactor comprising at least one process microchannel and at least one adjacent heat exchange zone.
摘要翻译：所公开的发明涉及将包含H 2 CO和CO的反应物组合物转化成包含至少一种具有至少约5个碳原子的脂族烃的产物的方法，该方法包括：使反应物组合物通过与费 - 托催化剂接触以将反应物组合物转化成产物的微通道反应器，该微通道反应器包含多个含有该催化剂的工艺微通道; 将热量从工艺微通道传递到热交换器; 并从微通道反应器中除去产物; 该方法每小时产生至少约0.5克具有至少约5个碳原子的每克催化剂的脂族烃; 产品中甲烷的选择性小于约25％。所公开的发明还涉及包含Co的载体催化剂和包含至少一个工艺微通道和至少一个相邻的热交换区的微通道反应器。

16. 发明授权

US07566441B2 Methods of conducting catalytic combustion in a multizone reactor, and a method of making a thermally stable catalyst support 有权
标题翻译：在多区域反应器中进行催化燃烧的方法以及制备热稳定催化剂载体的方法
公开(公告)号：US07566441B2
公开(公告)日：2009-07-28
申请号：US10966158
申请日：2004-10-15
申请人： Francis P. Daly , Junko M. Watson , Yong Wang , Jianli Hu , Chunshe Cao , Richard Long , Rachid Taha
发明人： Francis P. Daly , Junko M. Watson , Yong Wang , Jianli Hu , Chunshe Cao , Richard Long , Rachid Taha
IPC分类号： C07C1/02 , C01B3/26 , F23C13/00
CPC分类号： B01J23/42 , B01J19/0093 , B01J23/688 , B01J35/04 , B01J35/10 , B01J35/1014 , B01J37/0215 , B01J2219/00783 , B01J2219/00788 , B01J2219/00822 , B01J2219/00824 , B01J2219/00835 , B01J2219/00873 , B01J2219/00957 , B01J2219/00984 , C01B3/382 , C01B3/386 , C01B3/40 , C01B32/40 , C01B2203/0244 , C01B2203/0261 , C01B2203/107 , C01B2203/1082 , C01B2203/1217 , C01B2203/1235 , C01B2203/143 , C01B2203/1614 , C01B2203/82 , F23C13/00 , F23C2900/03001 , Y02P20/52
摘要： The invention provides methods of combusting a fuel in a reactor that includes at least 3 zones each of which contains a solid catalyst. A method of making a thermally-stable alumina support from fumed alumina is also described.
摘要翻译：本发明提供在反应器中燃烧燃料的方法，其包括至少3个区，每个区含有固体催化剂。还描述了由热解氧化铝制备热稳定氧化铝载体的方法。

17. 发明申请

US20070173653A1 Method of performing sugar dehydration and catalyst treatment 失效
标题翻译：糖脱水和催化剂处理方法
公开(公告)号：US20070173653A1
公开(公告)日：2007-07-26
申请号：US11342146
申请日：2006-01-26
申请人： Jianli Hu , Johnathan Holladay , Xinjie Zhang , Yong Wang
发明人： Jianli Hu , Johnathan Holladay , Xinjie Zhang , Yong Wang
IPC分类号： C07D311/22
CPC分类号： C07H1/00
摘要： The invention includes a method of treating a solid acid catalyst. After exposing the catalyst to a mixture containing a sugar alcohol, the catalyst is washed with an organic solvent and is then exposed to a second reaction mixture. The invention includes a process for production of anhydrosugar alcohol. A solid acid catalyst is provided to convert sugar alcohol in a first sample to an anhydrosugar alcohol. The catalyst is then washed with an organic solvent and is subsequently utilized to expose a second sample. The invention includes a method for selective production of an anhydrosugar. A solid acid catalyst is provided within a reactor and anhydrosugar alcohol is formed by flowing a starting sugar alcohol into the reactor. The acid catalyst is then exposed to an organic solvent which allows a greater amount of additional anhydrosugar to be produced than would occur without exposing the acid catalyst to the organic solvent.
摘要翻译：本发明包括一种处理固体酸催化剂的方法。在将催化剂暴露于含有糖醇的混合物之后，用有机溶剂洗涤催化剂，然后暴露于第二反应混合物。本发明包括生产脱水葡萄糖醇的方法。提供固体酸催化剂以将第一样品中的糖醇转化为脱水葡萄糖醇。然后将催化剂用有机溶剂洗涤，随后用于暴露第二个样品。本发明包括选择性生产脱水糖的方法。在反应器内提供固体酸催化剂，通过将起始糖醇流入反应器而形成脱水葡萄糖醇。然后将酸催化剂暴露于有机溶剂，其允许比不会将酸催化剂暴露于有机溶剂而产生更多量的额外的脱水糖。

18. 发明申请

US20070173652A1 Method of forming a dianhydrosugar alcohol 失效
标题翻译：形成二脱水糖醇的方法
公开(公告)号：US20070173652A1
公开(公告)日：2007-07-26
申请号：US11341961
申请日：2006-01-26
申请人： Johnathan Holladay , Jianli Hu , Yong Wang , Todd Werpy , Xinjie Zhang
发明人： Johnathan Holladay , Jianli Hu , Yong Wang , Todd Werpy , Xinjie Zhang
IPC分类号： C07D311/22
CPC分类号： C07D307/20 , C07D493/04 , Y02P20/127
摘要： The invention includes methods of producing dianhydrosugars. A polyol is reacted in the presence of a first catalyst to form a monocyclic sugar. The monocyclic sugar is transferred to a second reactor where it is converted to a dianhydrosugar alcohol in the presence of a second catalyst. The invention includes a process of forming isosorbide. An initial reaction is conducted at a first temperature in the presence of a solid acid catalyst. The initial reaction involves reacting sorbitol to produce 1,4-sorbitan, 3,6-sorbitan, 2,5-mannitan and 2,5-iditan. Utilizing a second temperature, the 1,4-sorbitan and 3,6-sorbitan are converted to isosorbide. The invention includes a method of purifying isosorbide from a mixture containing isosorbide and at least one additional component. A first distillation removes a first portion of the isosorbide from the mixture. A second distillation is then conducted at a higher temperature to remove a second portion of isosorbide from the mixture.
摘要翻译：本发明包括生产二脱水甘油糖的方法。多元醇在第一催化剂存在下反应形成单环糖。将单环糖转移到第二反应器中，在第二反应器中，在第二催化剂的存在下将其转化为二脱水甘油醇。本发明包括形成异山梨醇的方法。在固体酸催化剂存在下，在第一温度下进行初始反应。初始反应包括使山梨醇反应生成1,4-脱水山梨糖醇，3,6-脱水山梨糖醇，2,5-甘露聚糖和2,5-己烷。利用第二温度，将1,4-脱水山梨醇和3,6-脱水山梨醇转化为异山梨醇。本发明包括从含有异山梨醇和至少一种另外的组分的混合物中纯化异山梨醇的方法。第一蒸馏从混合物中除去第一部分的异山梨醇。然后在较高温度下进行第二次蒸馏以从混合物中除去第二部分的异山梨醇。

19. 发明申请

US20070173651A1 Two-stage dehydration of sugars 有权
标题翻译：糖两步脱水
公开(公告)号：US20070173651A1
公开(公告)日：2007-07-26
申请号：US11341930
申请日：2006-01-26
申请人： Johnathan Holladay , Jianli Hu , Yong Wang , Todd Werpy
发明人： Johnathan Holladay , Jianli Hu , Yong Wang , Todd Werpy
IPC分类号： C07D311/22
CPC分类号： C07D493/04
摘要： The invention includes methods for producing dianhydrosugar alcohol by providing an acid catalyst within a reactor and passing a starting material through the reactor at a first temperature. At least a portion of the staring material is converted to a monoanhydrosugar isomer during the passing through the column. The monoanhydrosugar is subjected to a second temperature which is greater than the first to produce a dianhydrosugar. The invention includes a method of producing isosorbide. An initial feed stream containing sorbitol is fed into a continuous reactor containing an acid catalyst at a temperature of less than 120° C. The residence time for the reactor is less than or equal to about 30 minutes. Sorbitol converted to 1,4-sorbitan in the continuous reactor is subsequently provided to a second reactor and is dehydrated at a temperature of at least 120° C. to produce isosorbide.
摘要翻译：本发明包括通过在反应器内提供酸催化剂并使原料在第一温度下通过反应器来生产二脱水甘油的方法。在通过色谱柱期间，至少一部分起始物质被转化为单一脱氢葡萄糖异构体。单糖酐经受大于第一温度的第二温度以产生二脱水糖。本发明包括一种生产异山梨醇的方法。含有山梨醇的初始进料流在小于120℃的温度下进料到含有酸催化剂的连续反应器中。反应器的停留时间小于或等于约30分钟。随后将连续反应器中转化为1,4-脱水山梨醇的山梨糖醇提供给第二反应器，并在至少120℃的温度下脱水以制备异山梨醇。

20. 发明授权

US07722833B2 Microchannel reactor 有权
标题翻译：微通道反应器
公开(公告)号：US07722833B2
公开(公告)日：2010-05-25
申请号：US11484069
申请日：2006-07-11
申请人： Yong Wang , Anna Lee Tonkovich , Terry Mazanec , Francis P. Daly , Dave VanderWiel , Jianli Hu , Chunshe Cao , Charles Kibby , Xiaohong Shari Li , Michael D. Briscoe , Nathan Gano , Ya-Huei Chin
发明人： Yong Wang , Anna Lee Tonkovich , Terry Mazanec , Francis P. Daly , Dave VanderWiel , Jianli Hu , Chunshe Cao , Charles Kibby , Xiaohong Shari Li , Michael D. Briscoe , Nathan Gano , Ya-Huei Chin
IPC分类号： B01J19/00
CPC分类号： C10G2/332 , B01J19/0093 , B01J21/04 , B01J23/75 , B01J23/8896 , B01J23/8913 , B01J35/0066 , B01J35/1019 , B01J35/1038 , B01J35/1042 , B01J37/0205 , B01J2219/00783 , B01J2219/00822 , B01J2219/00824 , B01J2219/00826 , B01J2219/00831 , B01J2219/00835 , B01J2219/00844 , B01J2219/0086 , B01J2219/00873 , C10G2/341 , C10G2300/301 , C10G2300/4018 , C10G2300/4025 , C10G2300/70 , C10G2400/04 , C10G2400/10 , Y02P20/582
摘要： A microchannel reactor is described which has at least one process microchannel and at least one heat exchange zone. The microchannel reactor may be used for conducting a Fischer-Tropsch synthesis reaction.
摘要翻译：描述了具有至少一个工艺微通道和至少一个热交换区的微通道反应器。微通道反应器可用于进行费 - 托合成反应。

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