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11. 发明授权

US07686940B2 Acoustic agglomeration to reduce fouling in thermal conversion processes 失效
标题翻译：声学聚集，以减少热转换过程中的结垢
公开(公告)号：US07686940B2
公开(公告)日：2010-03-30
申请号：US11330867
申请日：2006-01-12
申请人： Glen E. Phillips , Leo D. Brown , Michael Siskin
发明人： Glen E. Phillips , Leo D. Brown , Michael Siskin
IPC分类号： C10G9/16 , C10G75/00 , B01D51/08
CPC分类号： C10G9/00 , B01D51/08 , C10G9/005 , C10G9/007 , C10G9/16 , C10G9/32 , C10G2300/1033 , C10G2300/107 , C10G2300/1077 , C10G2300/4075
摘要： This invention relates to a process for reducing fouling of equipment used in fluidized bed thermal conversion processes such as fluid coking and FLEXICOKING™. Acoustic energy is used to acoustically agglomerate fine mists created during the coking process. The agglomerated mists are then carried along with the circulating coke instead of depositing on coking equipment.
摘要翻译：本发明涉及一种减少流化床热转化过程如流体焦化和FLEXICOKING™中使用的设备结垢的方法。声能被用于声音聚集在焦化过程中产生的细雾。然后将聚集的薄雾与循环焦炭一起携带，而不是沉积在焦化设备上。

12. 发明申请

US20090184029A1 Method to alter coke morphology using metal salts of aromatic sulfonic acids and/or polysulfonic acids 有权
标题翻译：使用芳族磺酸和/或多磺酸的金属盐改变焦炭形态的方法
公开(公告)号：US20090184029A1
公开(公告)日：2009-07-23
申请号：US12010145
申请日：2008-01-22
申请人： Ramesh Varadaraj , Michael Siskin , Leo D. Brown , Cornelius H. Brons
发明人： Ramesh Varadaraj , Michael Siskin , Leo D. Brown , Cornelius H. Brons
IPC分类号： C10G9/14
CPC分类号： C10B55/00 , C10B57/06
摘要： A method for altering coke morphology in a delayed coking process of heavy oil is provided. An effective amount of oil dispersible or oil soluble metal salts of aromatic sulfonic acids and/or polysulfonic acids is added or contacted with the resid or heavy oil at a point before or after the step of heating the heavy oil to coking temperatures. The addition of additives facilitates the formation of shot coke and inhibits the formation of sponge coke.
摘要翻译：提供了一种在重油延迟焦化过程中改变焦炭形态的方法。在将重油加热至焦化温度的步骤之前或之后的一点加入芳族磺酸和/或多磺酸的有效量的油分散性或油溶性金属盐与残油或重油接触。添加添加剂促进了焦炭的形成并抑制海绵焦炭的形成。

13. 发明授权

US07538251B2 Synthesis of severely sterically hindered secondary aminoether alcohols from a ketene and/or carboxylic acid halide and/or carboxylic acid anhydride 有权
标题翻译：从烯酮和/或羧酸卤化物和/或羧酸酐合成严重位阻的仲氨基醚醇
公开(公告)号：US07538251B2
公开(公告)日：2009-05-26
申请号：US10587204
申请日：2005-02-01
申请人： Michael Siskin , Alan Roy Katritzky , Kostyantyn Mykolayevich Kirichenko , Adeana Richelle Bishop , Christine Nicole Elia
发明人： Michael Siskin , Alan Roy Katritzky , Kostyantyn Mykolayevich Kirichenko , Adeana Richelle Bishop , Christine Nicole Elia
IPC分类号： C07C209/22
CPC分类号： C07C213/02 , C07C215/08
摘要： Severely sterically hindered secondary aminoether alcohols are prepared by a process comprising reacting a ketene with sulfuric acid to produce an anhydride which is then reacted with, to cleave the ring of, a dioxane to yield a cleavage product which is then aminated using an amine, followed by hydrolysis with a base to yield the desired severely sterically hindered secondary aminoether alcohol.
摘要翻译：通过包括使乙烯酮与硫酸反应以产生酸酐的方法来制备严格位阻的仲氨基醚醇，所述酸酐然后与二恶烷的环进行反应以切割二环环，得到裂解产物，然后使用胺将其胺化，随后通过用碱水解产生所需的严格空间位阻的仲氨基醚醇。

14. 发明授权

US07344889B2 Chemical structural and compositional yields model for predicting hydrocarbon thermolysis products 有权
标题翻译：用于预测碳氢化合物热解产物的化学结构和组成产量模型
公开(公告)号：US07344889B2
公开(公告)日：2008-03-18
申请号：US10426356
申请日：2003-04-30
申请人： Simon R. Kelemen , Howard Freund , Michael Siskin , David J. Curry , Yitian Xiao , William N. Olmstead , Martin L. Gorbaty , A. E. Bence
发明人： Simon R. Kelemen , Howard Freund , Michael Siskin , David J. Curry , Yitian Xiao , William N. Olmstead , Martin L. Gorbaty , A. E. Bence
IPC分类号： G01N33/24
CPC分类号： G01N33/241 , G01N33/2823 , G06F19/702 , G06F19/703
摘要： A method of predicting the composition of hydrocarbon products of a complex carbonaceous material when exposed to specific time and temperature conditions is disclosed. In one embodiment, the material is characterized to obtain elemental, chemical and structural parameters. A representative chemical structure of the material is constructed based on the characterization information. The representative chemical structure is then stochastically expanded to a molecular ensemble chemical structural model that includes heteroatoms. The chemical structural model is coupled to a compositional yield model and the composition of the material products is determined using kinetic modeling. Methods are provided of constructing a chemical structural model of complex carbonaceous material, of coupling a molecular ensemble of chemical structures to a thermal chemical mechanism, of updating an ensemble of chemical structures during the kinetic modeling to reflect chemical reaction products and of eliminating molecules from the system.
摘要翻译：公开了当暴露于特定的时间和温度条件时预测复合碳质材料的烃产物的组成的方法。在一个实施方案中，该材料的特征在于获得元素，化学和结构参数。基于特征信息构建材料的代表性化学结构。然后将代表性的化学结构随机扩展到包括杂原子的分子整体化学结构模型。化学结构模型与组合产量模型耦合，并且使用动力学模型确定材料产物的组成。提供了构建复杂碳质材料的化学结构模型的方法，将化学结构的分子组合耦合到热化学机制，在动力学建模期间更新化学结构的集合以反映化学反应产物并从中消除分子系统。

15. 发明申请

US20070287866A1 Synthesis of Severely Sterically Hindered Secondary Aminoether Alcohols from a Ketene and/or Carboxylic Acid Halide and/or Carboxylic Acid Anhydride 有权
标题翻译：从乙烯和/或羧酸卤化物和/或羧酸酐合成严重受阻的仲氨基醚醇
公开(公告)号：US20070287866A1
公开(公告)日：2007-12-13
申请号：US10587204
申请日：2005-02-01
申请人： Michael Siskin , Alan Katritzky , Kostyantyn Kirichenko , Adeana Bishop , Christine Elia
发明人： Michael Siskin , Alan Katritzky , Kostyantyn Kirichenko , Adeana Bishop , Christine Elia
IPC分类号： C07C213/00
CPC分类号： C07C213/02 , C07C215/08
摘要： Severely sterically hindered secondary aminoether alcohols are prepared by a process comprising reacting a ketene with sulfuric acid to produce an anhydride which is then reacted with, to cleave the ring of, a dioxane to yield a cleavage product which is then aminated using an amine, followed by hydrolysis with a base to yield the desired severely sterically hindered secondary aminoether alcohol.
摘要翻译：通过包括使乙烯酮与硫酸反应以产生酸酐的方法来制备严格位阻的仲氨基醚醇，所述酸酐然后与二恶烷的环进行反应以切割二环环，得到裂解产物，然后使用胺将其胺化，随后通过用碱水解产生所需的严格空间位阻的仲氨基醚醇。

16. 发明申请

US20070108036A1 Continuous coking process 失效
标题翻译：连续焦化工艺
公开(公告)号：US20070108036A1
公开(公告)日：2007-05-17
申请号：US11272656
申请日：2005-11-14
申请人： Michael Siskin , Christopher Eppig , Glen Phillips , Te-Hung Chen , Charles Mart
发明人： Michael Siskin , Christopher Eppig , Glen Phillips , Te-Hung Chen , Charles Mart
IPC分类号： B09B3/00 , C10B47/28
CPC分类号： C10B55/00 , C10B1/04 , C10B31/12 , C10B33/12 , C10G9/005 , C10G2300/80
摘要： The invention relates to a thermal conversion process for continuously producing hydrocarbon vapor and continuously removing a free-flowing coke. The coke, such as a shot coke, can be withdrawn continuously via, e.g., a staged lock hopper system.
摘要翻译：本发明涉及一种用于连续生产烃蒸气并连续除去自由流动焦炭的热转化方法。可以通过例如分段锁料斗系统连续地取出焦炭，例如喷射焦炭。

17. 发明授权

US07033486B2 Residuum conversion process 失效
标题翻译：残留转化过程
公开(公告)号：US07033486B2
公开(公告)日：2006-04-25
申请号：US10368186
申请日：2003-02-18
申请人： Martin L. Gorbaty , Michael Siskin , Mitchell Jacobson
发明人： Martin L. Gorbaty , Michael Siskin , Mitchell Jacobson
IPC分类号： C10G11/14
CPC分类号： C10G9/32 , C10G2300/107
摘要： The present invention relates to a process for increasing the capacity for processing residua and obtaining higher yields of liquids having an average boiling point equal to or less than about 510° C. A residual feedstock is introduced with recycled product asphaltenes into a short vapor contact time thermal process unit wherein the vaporized product is sent to a fractionator zone to produce a 510° C.− fraction and a 510° C.+ fraction. The 510° C.+ fraction is sent to a solvent extraction zone to produce an asphaltene-rich fraction that is recycled to the short vapor contact time thermal process unit.
摘要翻译：本发明涉及一种增加处理残留物的能力并获得更高产量的平均沸点等于或小于约510℃的液体的方法。将残余原料与再循环产物沥青质引入短时间的蒸气接触时间热处理单元，其中蒸发的产物被送到分馏器区域以产生510℃的馏分和510℃的+馏分。将510℃的馏分送入溶剂萃取区，以产生富含沥青质的馏分，再循环到短蒸汽接触时间热处理装置。

18. 发明申请

US20050279673A1 Delayed coking process for producing free-flowing coke using an overbased metal detergent additive 审中-公开
标题翻译：使用高碱性金属洗涤剂添加剂生产自由流动焦炭的延迟焦化工艺
公开(公告)号：US20050279673A1
公开(公告)日：2005-12-22
申请号：US11127823
申请日：2005-05-12
申请人： Christopher Eppig , Michael Siskin , Daniel Leta
发明人： Christopher Eppig , Michael Siskin , Daniel Leta
IPC分类号： C10B55/00 , C10B57/06 , C10G9/14
CPC分类号： C10B55/00 , C10B57/06 , C10G2300/107 , C10G2300/1077
摘要： A delayed coking process for making substantially free-flowing coke, preferably shot coke. A coker feedstock, such as a vacuum residuum, is heated in a heating zone to coking temperatures then conducted to a coking zone wherein volatiles are collected overhead and coke is formed. An overbased alkaline earth metal detergent additive is added to the feedstock prior to it being heated in the heating zone, prior to its being conducted to the coking zone, or both.
摘要翻译：一种延迟焦化工艺，用于制造基本上自由流动的焦炭，优选喷射焦炭。焦化原料如真空残渣在加热区被加热至焦化温度，然后进入焦化区，其中挥发物在塔顶馏出并形成焦炭。将高碱性碱土金属洗涤剂添加剂在其被加热到加热区之前，在其被引导到焦化区之前或两者的同时，被加入到原料中。

19. 发明申请

US20050043532A1 Direct synthesis of di-heteroatom containing cyclic organic compounds 审中-公开
标题翻译：直接合成含二杂原子的环状有机化合物
公开(公告)号：US20050043532A1
公开(公告)日：2005-02-24
申请号：US10894804
申请日：2004-07-20
申请人： Michael Siskin , Edmund Mozeleski
发明人： Michael Siskin , Edmund Mozeleski
IPC分类号： C07D295/02 , C07D295/027 , C07D319/12 , C07D279/12 , C07D265/30 , C07D339/02
CPC分类号： C07D295/027 , C07D319/12
摘要： The present invention provides for the simplified, direct synthesis of di-heteroatom containing cyclic organic compounds by forming an aqueous mixture of material of the formula 1 wherein X and Y are heteroatoms which may be the same or different and X is selected from the group consisting of O, S and N, and both Y's are the same and are selected from the group consisting of O, S and N, and R1 through R8 are the same or different and are selected from the group consisting of H, C1 to C10 alkyl radicals, C1 to C10 aryl radicals, C1 to C10 alkyl aryl radicals, and z is zero when X and Y are O or S, and z is 1 when X and Y are N, and water at a mole ratio of water to material of formula I in the range of about 10:1 to about 0.001:1 and heating the mixture to a temperature in the range of about 250° C. to about 350° C. under autogeneous pressure for a time of from about 0.5 to 10 hours. Trace amounts of liquid, solid or gaseous acid can be present to further accelerate dehydration, dehydrosulfurization or deamination and cyclization.
摘要翻译：本发明通过形成式1的材料的水性混合物来简化，直接合成含二杂原子的环状有机化合物，其中X和Y是可以相同或不同的杂原子，X选自的O，S和N，并且两个Y都相同并且选自O，S和N，并且R 1至R 8相同或不同，并且选自由以下组成的组： H，C1至C10烷基，C1至C10芳基，C1至C10烷基芳基，当X和Y为O或S时z为零，当X和Y为N时z为1，水与式I物质的比例在约10:1至约0.001:1的范围内，并将混合物在自压下加热至约250℃至约350℃的温度，持续一段时间约0.5至10小时。可以存在微量的液体，固态或气态酸，以进一步加速脱水，脱硫脱硫或脱氨和环化。

20. 发明授权

US5611915A Process for removal of heteroatoms under reducing conditions in supercritical water 失效
标题翻译：在超临界水中还原条件下去除杂原子的方法
公开(公告)号：US5611915A
公开(公告)日：1997-03-18
申请号：US583692
申请日：1996-01-05
申请人： Michael Siskin , David T. Ferrughelli , Alan R. Katritzky , William N. Olmstead
发明人： Michael Siskin , David T. Ferrughelli , Alan R. Katritzky , William N. Olmstead
IPC分类号： C07B37/00 , C07C1/00 , C07C1/32 , C07C15/02 , C10G1/00 , C10G1/04 , C10G1/06
CPC分类号： C07C1/322 , C07C1/323 , C10G1/00 , Y02P20/544 , Y10S208/952
摘要： A process for heteroatom removal-enhancing hydrogenation of highly refractory aromatic ring structures that involves contacting a highly refractory structure having at least one aryl linkage connecting a first heteroaryl moiety and a moiety selected from the group consisting of an aryl moiety and a second heteroaryl moiety with supercritical water having a temperature of from about 400.degree. C. to about 600.degree. C. in the presence of from about 3.4 MPa to about 18.6 MPa of CO to produce lower molecular weight products having decreased aromatic and heteroatom content. The process has utility for producing more valuable lower molecular weight products having a reduced aromatic heteroatom content from starting materials that are highly refractory and widely considered to be difficult to upgrade such as coals and asphaltenes, and model compounds containing the biaryl linkages.
摘要翻译：使高难度芳族环结构的杂原子去除增强氢化的方法包括将具有至少一个连接第一杂芳基部分的芳基与选自芳基部分和第二杂芳基部分的部分的至少一个芳基键接触的高度耐火结构与在约3.4MPa至约18.6MPa的CO存在下，温度为约400℃至约600℃的超临界水，以产生具有降低的芳族和杂原子含量的较低分子量产物。该方法可用于生产具有降低的芳族杂原子含量的低价分子量产物，所述低分子量产物具有高度耐火且被广泛认为难以升级的起始材料，例如煤和沥青质，以及含有联芳基键的模型化合物。

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