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11. 发明申请

US20130217915A1 Catalyst and Method for Producing Acrylic Acid 有权
标题翻译：催化剂和生产丙烯酸的方法
公开(公告)号：US20130217915A1
公开(公告)日：2013-08-22
申请号：US13882265
申请日：2011-10-27
申请人： Yuta Nakazawa , Susumu Matsumoto , Tomoaki Kobayashi , Tatsuhiko Kurakami
发明人： Yuta Nakazawa , Susumu Matsumoto , Tomoaki Kobayashi , Tatsuhiko Kurakami
IPC分类号： C07C51/16
CPC分类号： C07C51/16 , B01J23/002 , B01J23/8877 , B01J27/199 , B01J35/0006 , B01J35/04 , B01J37/0036 , B01J37/0045 , B01J37/0244 , B01J2523/00 , C07C51/235 , C07C57/04 , B01J2523/17 , B01J2523/53 , B01J2523/55 , B01J2523/68
摘要： The present invention relates to a method for producing acrylic acid through vapor-phase contact oxidation of acrolein, wherein a reactor tube is divided into at least two catalyst layers, and catalysts having a higher activity are charged in the reactor tube sequentially toward an outlet port side from a material source gas inlet port side for a reaction therein to give acrylic acid, and wherein a catalyst activity-controlling method is a method comprising: a step of mixing a molybdenum-containing compound, a vanadium-containing compound, a copper-containing compound and an antimony-containing compound with water, then drying and calcining a resulting mixture, in which a catalytically-active element composition is kept constant but material source compounds are made to vary in type to give composite metal oxides having a different activity.
摘要翻译：本发明涉及一种通过丙烯醛的气相接触氧化制备丙烯酸的方法，其中将反应器管分成至少两个催化剂层，并且具有较高活性的催化剂依次连接到反应器管的出口一边从材料源气体入口侧进行反应，得到丙烯酸，其中催化剂活性控制方法是一种方法，包括：将含钼化合物，含钒化合物，铜 - 然后干燥和煅烧所得混合物，其中催化活性元素组合物保持恒定，但是使材料源化合物的类型变化，得到具有不同活性的复合金属氧化物。

12. 发明申请

US20130310604A1 Process For Producing Unsaturated Aldehyde And/or Unsaturated Carboxylic Acid 有权
标题翻译：生产不饱和醛和/或不饱和羧酸的方法
公开(公告)号：US20130310604A1
公开(公告)日：2013-11-21
申请号：US13982808
申请日：2012-01-16
申请人： Tatsuhiko Kurakami , Susumu Matsumoto , Atsushi Sudo , Kazuo Shiraishi , Masashi Hashiba
发明人： Tatsuhiko Kurakami , Susumu Matsumoto , Atsushi Sudo , Kazuo Shiraishi , Masashi Hashiba
IPC分类号： C07C51/25 , C07C45/38 , C07C51/235 , C07C45/35
CPC分类号： C07C51/235 , C07C45/35 , C07C45/38 , C07C51/252 , C07C47/22 , C07C57/04
摘要： There is provided a process for producing aerolein, acrylic acid, methacrolein, methacrylic acid in a safe and steady manner and in high yields, which avoids a phenomenon of occurrence of an abnormal reaction attributable to the fact that the temperature at a raw material gas outlet side becomes considerably higher than the temperature at a raw material gas inlet side, with regard to the temperature of a catalyst packed in a reaction tube at vapor-phase catalytic oxidation of propylene, isobutylene, or the like.In the process of using a reaction tube on which a plurality of catalyst layers formed in a raw material gas flow direction, a catalyst and a catalyst packing schedule are designed so that a relation between the raw material conversion rate at which the yield of the objective product becomes maximum and the raw material conversion rate at which a high and low correlation between maximum temperature of the catalyst layer present closest to a reaction gas inlet side Zin and maximum temperature of the catalyst layer present closest to a reaction gas outlet side Zout is reversed satisfies a specific condition of 0.5≦Cmax−Ccrs≦5, in which Cmax: a raw material conversion rate at which yield of the objective products becomes maximum; and Ccrs: a raw material conversion rate at which, when maximum temperature of the catalyst layer Zin is regarded as Tin, maximum temperature of the catalyst layer Zout is regarded as Tout, and the raw material conversion rate is changed, a high and low correlation between Tin and Tout is reversed.
摘要翻译：提供了以安全稳定的方式和高产率生产气溶胶，丙烯酸，甲基丙烯醛，甲基丙烯酸的方法，避免了由于原料气体出口处的温度导致的异常反应的发生现象相对于在丙烯，异丁烯等的气相催化氧化反应管中填充的催化剂的温度，原料气体入口侧的温度显着高于原料气体入口侧的温度。在使用在原料气体流动方向上形成有多个催化剂层的反应管的过程中，设计催化剂和催化剂填充进度，使得目的物的产率的原料转化率之间的关系产物变得最大，并且最接近反应气体入口侧的催化剂层的最高温度和最接近反应气体出口侧的催化剂层的最高温度之间的高低相关性的原料转化率反转满足0.5 @ Cmax-Ccrs @ 5的特定条件，其中Cmax：目标产物的产率变为最大的原料转化率; Ccrs：将催化剂层Zin的最高温度设为Tin时的原料转化率，将催化剂层Zout的最高温度设为Tout，将原料转化率变更为高，低相关 Tin和Tout之间是相反的。

13. 发明申请

US20110237829A1 Method For Manufacturing Catalyst For Use In Production Of Methacrylic Acid 失效
标题翻译：制造用于生产甲基丙烯酸的催化剂的方法
公开(公告)号：US20110237829A1
公开(公告)日：2011-09-29
申请号：US13155863
申请日：2011-06-08
申请人： Atsushi Sudo , Tatsuhiko Kurakami , Toshitake Kojima , Shigeo Hayashimoto , Yasushi Kobayashi
发明人： Atsushi Sudo , Tatsuhiko Kurakami , Toshitake Kojima , Shigeo Hayashimoto , Yasushi Kobayashi
IPC分类号： C07C51/16 , B01J27/24 , B01J37/04 , B01J37/08 , B01J37/02 , B01J31/02 , C07C51/347
CPC分类号： C07C51/235 , B01J23/002 , B01J27/199 , B01J35/08 , B01J37/0045 , B01J37/0221 , B01J2231/70 , B01J2523/00 , C07C51/00 , C07C51/377 , C07C57/04 , B01J2523/15 , B01J2523/17 , B01J2523/51 , B01J2523/53 , B01J2523/55 , B01J2523/68
摘要： It is an object of the present invention to provide a catalyst having excellent performance and high mechanical strength for use in the production of methacrylic acid.A method for manufacturing a catalyst comprising essential active components of molybdenum, phosphorus, vanadium, cesium, ammonia, copper, and antimony for use in the production of methacrylic acid, comprising drying a slurry prepared by mixing a compound(s) containing the essential active components with water and then calcining the resulting dry powder and molding the calcined powder.
摘要翻译：本发明的目的是提供一种用于生产甲基丙烯酸的具有优异性能和高机械强度的催化剂。一种用于制造催化剂的方法，其包括用于生产甲基丙烯酸的钼，磷，钒，铯，氨，铜和锑的必需活性组分，包括干燥通过将含有必需活性物质的化合物用水组分，然后煅烧所得干粉，并将煅烧粉末成型。

14. 发明授权

US08017547B2 Method for manufacturing catalyst for use in production of methacrylic acid 有权
标题翻译：用于生产甲基丙烯酸的催化剂的制备方法
公开(公告)号：US08017547B2
公开(公告)日：2011-09-13
申请号：US11919911
申请日：2006-05-11
申请人： Atsushi Sudo , Tatsuhiko Kurakami , Toshitake Kojima , Shigeo Hayashimoto , Yasushi Kobayashi
发明人： Atsushi Sudo , Tatsuhiko Kurakami , Toshitake Kojima , Shigeo Hayashimoto , Yasushi Kobayashi
IPC分类号： B01J23/00
CPC分类号： C07C51/235 , B01J23/002 , B01J27/199 , B01J35/08 , B01J37/0045 , B01J37/0221 , B01J2231/70 , B01J2523/00 , C07C51/00 , C07C51/377 , C07C57/04 , B01J2523/15 , B01J2523/17 , B01J2523/51 , B01J2523/53 , B01J2523/55 , B01J2523/68
摘要： It is an object of the present invention to provide a catalyst having excellent performance and high mechanical strength for use in the production of methacrylic acid.A method for manufacturing a catalyst comprising essential active components of molybdenum, phosphorus, vanadium, cesium, ammonia, copper, and antimony for use in the production of methacrylic acid, comprising drying a slurry prepared by mixing a compound(s) containing the essential active components with water and then calcining the resulting dry powder and molding the calcined powder.
摘要翻译：本发明的目的是提供一种用于生产甲基丙烯酸的具有优异性能和高机械强度的催化剂。一种用于制造催化剂的方法，其包括用于生产甲基丙烯酸的钼，磷，钒，铯，氨，铜和锑的必需活性组分，包括干燥通过将含有必需活性物质的化合物用水组分，然后煅烧所得干粉，并将煅烧粉末成型。

15. 发明授权

US08969618B2 Process for producing unsaturated aldehyde and/or unsaturated carboxylic acid 有权
标题翻译：不饱和醛和/或不饱和羧酸的制备方法
公开(公告)号：US08969618B2
公开(公告)日：2015-03-03
申请号：US13982808
申请日：2012-01-16
申请人： Tatsuhiko Kurakami , Susumu Matsumoto , Atsushi Sudo , Kazuo Shiraishi , Masashi Hashiba
发明人： Tatsuhiko Kurakami , Susumu Matsumoto , Atsushi Sudo , Kazuo Shiraishi , Masashi Hashiba
IPC分类号： C07C51/25 , C07C45/35 , C07C51/235 , C07C45/38
CPC分类号： C07C51/235 , C07C45/35 , C07C45/38 , C07C51/252 , C07C47/22 , C07C57/04
摘要： A catalyst and a catalyst packing schedule are designed so that a relation between the raw material conversion rate at which the yield of the objective product becomes maximum and the raw material conversion rate at which a high and low correlation between maximum temperature of the catalyst layer present closest to a reaction gas inlet side Zin and maximum temperature of the catalyst layer present closest to a reaction gas outlet side Zout is reversed satisfies a specific condition of 0.5≦Cmax−Ccrs≦5, in which Cmax: a raw material conversion rate at which yield of the objective products becomes maximum; and Ccrs: a raw material conversion rate at which, when maximum temperature of the catalyst layer Zin is regarded as Tin, maximum temperature of the catalyst layer Zout is regarded as Tout, and the raw material conversion rate is changed, a high and low correlation between Tin and Tout is reversed.
摘要翻译：设计催化剂和催化剂填充进度，使得目标产物的产率变得最大的原料转化率与存在催化剂层的最高温度之间的高低相关性的原料转化率之间的关系最接近反应气体入口侧的Zin和最接近反应气体出口侧的催化剂层的最高温度Zout反过来满足特定条件为0.5＆amp; NlE; Cmax-Ccrs＆nlE; 5，其中Cmax：原料转化率目标产品的产量变得最大; Ccrs：将催化剂层Zin的最高温度设为Tin时的原料转化率，将催化剂层Zout的最高温度设为Tout，将原料转化率变更为高，低相关 Tin和Tout之间是相反的。

16. 发明申请

US20120329638A1 Method For Manufacturing Catalyst From Recovered Catalyst 审中-公开
标题翻译：从回收催化剂制备催化剂的方法
公开(公告)号：US20120329638A1
公开(公告)日：2012-12-27
申请号：US13582055
申请日：2011-03-28
申请人： Tatsuhiko Kurakami , Takayuki Iijima , Tomoaki Kobayashi , Toshitake Kojima
发明人： Tatsuhiko Kurakami , Takayuki Iijima , Tomoaki Kobayashi , Toshitake Kojima
IPC分类号： B01J27/28
CPC分类号： C07C51/235 , B01J27/199 , B01J27/285 , B01J35/023 , B01J37/0009 , B01J37/0045 , B01J38/68 , C07C51/252 , Y02P20/584 , C07C57/04
摘要： The present invention relates to a method for manufacturing a regenerated catalyst from a recovered catalyst from manufacturing process or a used catalyst of a heteropoly acid-based catalyst containing molybdenum, phosphorus, vanadium or copper as an essential component by the below-described Process a to Process f: Process a: a solution A is prepared by mixing a substance M with an aqueous solvent and removing a component insoluble in the solvent; Process b: the molar quantity of at least one component of molybdenum, phosphorus, vanadium or copper contained in the solution A is measured; Process c: an aqueous hydrogen peroxide solution is added to the solution A to obtain a solution B; Process d: the difference between the content obtained in Process b and the theoretical value of a required element is determined and the shortage amount of the catalyst component is added to the solution B to prepare a solution C; Process e: the solution C is dried to prepare catalyst granules D; and Process f: the catalyst granules D are molded and subsequently calcined to prepare a molded catalyst E, the manufacturing method is also simple, and the obtained said regenerated catalyst has performance equivalent to an unused target catalyst, leading to a large advantage that it can be used as it is in combination with an unused target catalyst.
摘要翻译：本发明涉及一种从制造方法回收的催化剂制造再生催化剂的方法或通过下述方法a至于含有钼，磷，钒或铜作为必要成分的杂多酸系催化剂的使用催化剂方法f：处理a：通过将物质M与水性溶剂混合并除去不溶于溶剂的组分来制备溶液A; 方法b：测量溶液A中所含的钼，磷，钒或铜的至少一种组分的摩尔量; 方法c：向溶液A中加入过氧化氢水溶液以获得溶液B; 方法d：确定方法b中获得的含量与所需要元素的理论值之间的差异，并将催化剂组分的不足量加入到溶液B中以制备溶液C; 方法e：将溶液C干燥以制备催化剂颗粒D; 和方法f：将催化剂颗粒D模塑并随后煅烧以制备模制催化剂E，制备方法也简单，所得到的所述再生催化剂具有与未使用的目标催化剂相当的性能，导致其可以可以与未使用的目标催化剂组合使用。

17. 发明授权

US08148291B2 Method for manufacturing catalyst for use in production of methacrylic acid 失效
标题翻译：用于生产甲基丙烯酸的催化剂的制备方法
公开(公告)号：US08148291B2
公开(公告)日：2012-04-03
申请号：US13155863
申请日：2011-06-08
申请人： Atsushi Sudo , Tatsuhiko Kurakami , Toshitake Kojima , Shigeo Hayashimoto , Yasushi Kobayashi
发明人： Atsushi Sudo , Tatsuhiko Kurakami , Toshitake Kojima , Shigeo Hayashimoto , Yasushi Kobayashi
IPC分类号： B01J23/00
CPC分类号： C07C51/235 , B01J23/002 , B01J27/199 , B01J35/08 , B01J37/0045 , B01J37/0221 , B01J2231/70 , B01J2523/00 , C07C51/00 , C07C51/377 , C07C57/04 , B01J2523/15 , B01J2523/17 , B01J2523/51 , B01J2523/53 , B01J2523/55 , B01J2523/68
摘要： It is an object of the present invention to provide a catalyst having excellent performance and high mechanical strength for use in the production of methacrylic acid. A method for manufacturing a catalyst comprising essential active components of molybdenum, phosphorus, vanadium, cesium, ammonia, copper, and antimony for use in the production of methacrylic acid, comprising drying a slurry prepared by mixing a compound(s) containing the essential active components with water and then calcining the resulting dry powder and molding the calcined powder.
摘要翻译：本发明的目的是提供一种用于生产甲基丙烯酸的具有优异性能和高机械强度的催化剂。一种用于制造催化剂的方法，其包括用于生产甲基丙烯酸的钼，磷，钒，铯，氨，铜和锑的必需活性组分，包括干燥通过将含有必需活性物质的化合物用水组分，然后煅烧所得干粉，并将煅烧粉末成型。

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