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11. 发明授权

US07220888B2 Method for producing hydrocarbons having a modified carbon skeleton 失效
标题翻译：具有改性碳骨架的烃的制造方法
公开(公告)号：US07220888B2
公开(公告)日：2007-05-22
申请号：US10451739
申请日：2002-01-05
申请人： Dominic Vanoppen , Ekkehard Schwab , Jean-Marie Basset , Jean Thivolle-Cazat , Mostapha Taoufik , Michael Schulz , Arthur Höhn
发明人： Dominic Vanoppen , Ekkehard Schwab , Jean-Marie Basset , Jean Thivolle-Cazat , Mostapha Taoufik , Michael Schulz , Arthur Höhn
IPC分类号： C07C6/08
CPC分类号： C07C6/10 , C07C6/08 , C07C2531/12
摘要： The invention relates to a method for producing hydrocarbons having a modified carbon skeleton by reacting aliphatic hydrocarbons a) with themselves, b) with another aliphatic hydrocarbon or c) with aromatic alkyl substituted hydrocarbons, in the presence of a metal organic catalyst or the hybrid thereof, at a temperature of between 20–400° C. and a pressure of between 0.2–100 bars, wherein the reaction takes place in the presence of hydrogen.
摘要翻译：本发明涉及一种生产具有改性碳骨架的碳氢化合物的方法，该方法通过使脂族烃a）与其自身反应，b）与另一种脂族烃或c）与芳族烷基取代的烃在金属有机催化剂或其混合物存在下反应在20-400℃的温度和0.2-100巴的压力之间，其中反应在氢的存在下进行。

12. 发明授权

US06783693B1 Hydraulic fluids, containing cyclic carboxylic acid derivatives 失效
标题翻译：含有环状羧酸衍生物的液压油
公开(公告)号：US06783693B1
公开(公告)日：2004-08-31
申请号：US09959160
申请日：2001-10-18
申请人： Bayram Aydin , Uwe Fidorra , Arthur Höhn , Ladislaus Meszaros , Jan Nouwen , Knut Oppenländer , Michael Roida , Michael Stösser , Bernd Wenderoth
发明人： Bayram Aydin , Uwe Fidorra , Arthur Höhn , Ladislaus Meszaros , Jan Nouwen , Knut Oppenländer , Michael Roida , Michael Stösser , Bernd Wenderoth
IPC分类号： C09K500
CPC分类号： C10M129/20 , C10M107/34 , C10M107/52 , C10M129/14 , C10M133/08 , C10M133/32 , C10M133/38 , C10M133/44 , C10M145/26 , C10M169/044 , C10M2207/024 , C10M2207/044 , C10M2209/103 , C10M2209/1033 , C10M2209/104 , C10M2209/1045 , C10M2209/105 , C10M2209/1055 , C10M2209/106 , C10M2209/1065 , C10M2209/107 , C10M2209/1075 , C10M2209/1085 , C10M2209/1095 , C10M2215/042 , C10M2215/202 , C10M2215/22 , C10M2215/221 , C10M2215/223 , C10M2215/225 , C10M2215/226 , C10M2215/30 , C10M2227/061 , C10M2229/003 , C10N2240/08
摘要： Hydraulic fluids, in particular brake fluids for motor vehicles, comprising from 0.01 to 50 wt % of one or more cyclic carboxylates, or cyclic carboxamides, which can carry a linear or branched C1-bis C20 alkyl group on the nitrogen atom.
摘要翻译：液压流体，特别是用于机动车辆的制动液，包含0.01至50重量％的一种或多种环状羧酸酯，或环状羧酰胺，其可以在氮原子上带有直链或支链的C 1 -C 20烷基。

13. 发明授权

US06462236B2 Preparation of amines 有权
标题翻译：胺的制备
公开(公告)号：US06462236B2
公开(公告)日：2002-10-08
申请号：US09983307
申请日：2001-10-24
申请人： Shelue Liang , Frank Funke , Arthur Höhn
发明人： Shelue Liang , Frank Funke , Arthur Höhn
IPC分类号： C07C20926
CPC分类号： C07C209/26 , C07C211/29
摘要： Amines of the formula (I) R1R2CH—NR3R4 (I) where R1, R2, R3 and R4 are each, independently of one another, hydrogen, straight-chain or branched C1-C12-alkyl, C3-C12-cycloalkyl, C6-C10-aryl or C7-C11-aralkyl, where at least one of the radicals R1 and R2 is aryl or aralkyl whose aromatic unit is substituted by at least one halogen, are prepared by catalytic, hydrogenative amination of carbonyl compounds of the formula (II) or alcohols of the formula (III) R1—C(═O)—R2 (II) R1—CH(OH)—R2 (III) by means of nitrogen compounds of the formula (IV) HNR3R4 (IV) where R1 to R4 are as defined above, in the presence of Co- and/or Ni-containing catalysts, in the additional presence of solid acid cocatalysts and in the absence of organic sulfur compounds.
摘要翻译：式（I）的胺其中R 1，R 2，R 3和R 4各自独立地为氢，直链或支链C 1 -C 12 - 烷基，C 3 -C 12 - 环烷基，C 6 -C 10 - 芳基或C 7 -C 12 - C 11 - 芳烷基，其中基团R 1和R 2中的至少一个是其芳族单元被至少一个卤素取代的芳基或芳烷基，其通过式（II）的羰基化合物的催化，氢化胺化或式（III）通过其中R 1至R 4如上所定义的式（Ⅳ）的氮化合物在存在Co和/或Ni的催化剂的情况下，在固体酸助催化剂的另外存在下，在不存在有机硫化合物。

14. 发明授权

US06627756B1 Preparation of pure triethylenediamine 有权
标题翻译：纯三亚乙基二胺的制备
公开(公告)号：US06627756B1
公开(公告)日：2003-09-30
申请号：US09613718
申请日：2000-07-11
申请人： Hartmut Riechers , Arthur Höhn , Joachim Simon , Ortmund Lang , Hartmut Schoenmakers , Matthias Rauls , Koen Claerbout
发明人： Hartmut Riechers , Arthur Höhn , Joachim Simon , Ortmund Lang , Hartmut Schoenmakers , Matthias Rauls , Koen Claerbout
IPC分类号： C07D48708
CPC分类号： C07D487/08
摘要： Pure triethylenediamine (TEDA) is prepared by vaporizing TEDA, introducing the gaseous TEDA into a liquid solvent and subsequently crystallizing the TEDA from the solution obtained in this way.
摘要翻译：通过蒸发TEDA，将气态TEDA引入液体溶剂中并随后从以这种方式获得的溶液中使TEDA结晶来制备纯三亚乙基二胺（TEDA）。

15. 发明授权

US06271430B1 Preparation of propene 有权
公开(公告)号：US06271430B1
公开(公告)日：2001-08-07
申请号：US09283201
申请日：1999-04-01
申请人： Peter Schwab , Arthur Höhn
发明人： Peter Schwab , Arthur Höhn
IPC分类号： C07C602
摘要： The present invention relates to a process for preparing propene by metathesis of olefins. The process comprises preparing propene by a) in a first reactor (R1), reacting 1-butene and 2-butene to give propene and 2-pentene in the presence of a metathesis catalyst comprising at least one compound of a metal of transition group VIb, VIIb, or VIII of the Periodic Table of elements, b) subsequently separating the propene, unreacted raffinate II, and 2-pentene formed in a) in a distillation column (D1), c) subsequently reacting the 2-pentene of b) with ethene to give propene and 1-butene in a reactor (R2) in the presence of a metathesis catalyst comprising at least one compound of a metal of transition group VIb, VIIb, or VIII of the Periodic Table of Elements, d) subsequently separating the propene and 1-butene formed in c), e) subsequently returning the 1-butene formed in d) to step a) and f) wherein unreacted raffinate II is taken off at the middle off take of column D1 in b) and partly returned to step a).

16. 发明授权

US06852869B2 Method for the production of polytetrahydrofuran with low color index 失效
标题翻译：低颜色指数生产聚四氢呋喃的方法
公开(公告)号：US06852869B2
公开(公告)日：2005-02-08
申请号：US10343982
申请日：2001-07-24
申请人： Christoph Sigwart , Anton Meier , Michael Hesse , Volkmar Menger , Klaus-Peter Pfaff , Arthur Höhn , Lothar Franz
发明人： Christoph Sigwart , Anton Meier , Michael Hesse , Volkmar Menger , Klaus-Peter Pfaff , Arthur Höhn , Lothar Franz
IPC分类号： C08G65/30 , C08G65/20 , C08G65/322 , C07D307/04
CPC分类号： C08G65/322 , C08G65/20
摘要： In a process for preparing polytetrahydrofuran, tetrahydrofuran copolymers, diesters or monoesters of these polymers having a low color number, the polymers obtained by cationic polymerization of tetrahydrofuran are hydrogenated in the presence of a macroporous, supported heterogeneous catalyst comprising at least one metal of groups 7 to 10 of the Periodic Table of the Elements as active metal.
摘要翻译：在具有低色数的这些聚合物的四氢呋喃共聚物，二酯或单酯的制备方法中，通过四氢呋喃的阳离子聚合获得的聚合物在大孔载体的非均相催化剂存在下氢化，所述催化剂包含至少一种第7族金属到元素周期表中的10个作为活性金属。

17. 发明授权

US06790995B2 Preparation of primary and secondary amines from nitriles 失效
标题翻译：从腈制备伯胺和仲胺
公开(公告)号：US06790995B2
公开(公告)日：2004-09-14
申请号：US10033912
申请日：2002-01-03
申请人： Joachim Pfeffinger , Michael Hüllmann , Arthur Höhn , Frank Funke , Frank Ohlbach , Till Gerlach
发明人： Joachim Pfeffinger , Michael Hüllmann , Arthur Höhn , Frank Funke , Frank Ohlbach , Till Gerlach
IPC分类号： C07C20948
CPC分类号： C07C213/02 , C07C209/48 , C07C211/11 , C07C215/08
摘要： Mixtures of primary amines of the formula (I) X—CH2—NH2 (I) and secondary amines of the formula (II) (X—CH2—)2NH (II) where X is C1-20-alkyl, C2-20-alkenyl or C3-8-cycloalkyl which may be unsubstituted or substituted by C1-20-alkyl, C3-8-cycloalkyl, C4-20-alkylcycloalkyl, C4-20-cycloalkylalkyl, C2-20-alkoxyalkyl, C6-14-aryl, C7-20-alkylaryl, C7-20-aralkyl, C1-20-alkoxy, hydroxy, C1-20-hydroxyalkyl, amino, C1-20-alkylamino, C2-20-dialkylamino, C2-12-alkenylamino. C3-8-cycloalkylamino, arylamino, diarylamino, aryl-C1-8-alkylamino, halogen, mercapto, C2-20-alkenyloxy, C3-8-cycloalkoxy, aryloxy and/or C2-8-alkoxycarbonyl are prepared by reacting nitriles of the formula (III) X—CN (III) with hydrogen at from 50 to 250° C. and pressures of from 5 to 350 bar in the presence of a Pd-containing catalyst comprising, based on the total weight of the catalyst, from 0.1 to 10% by weight of Pd on a support.
摘要翻译：式（I）的伯胺和式（II）的仲胺的混合物，其中X是可以未被取代或被C 1-20烷基取代的C 1-20 - 烷基，C 2-20 - 烯基或C 3-8 - 环烷基，C 3-8 - 环烷基，C 4-20 - 烷基环烷基，C 4-20 - 环烷基烷基，C 2-20烷氧基烷基，C 6-14 - 芳基，C 7-20 - 烷基芳基，C 7-20 - 芳烷基，C 1-20 - 烷氧基，羟基，C 1-20羟烷基，氨基，C 1-20烷基氨基，C 2-20 - 二烷基氨基，C 2-12 - 烯基氨基。 C 3-8 - 环烷基氨基，芳基氨基，二芳基氨基，芳基-C 1-8 - 烷基氨基，卤素，巯基，C 2-20 - 烯氧基，C 3-8 - 环烷氧基，芳氧基和/或C 2-8烷氧基羰基，（III）与氢气在50-250℃下反应，压力为5-350巴，在含Pd催化剂的存在下，基于催化剂的总重量计，为0.1-10重量％的Pd 在支持上。

18. 发明授权

US06525223B2 Preparation of secondary amines from nitriles 失效
标题翻译：从腈制备仲胺
公开(公告)号：US06525223B2
公开(公告)日：2003-02-25
申请号：US10026900
申请日：2001-12-27
申请人： Joachim Pfeffinger , Michael Hüllmann , Arthur Höhn , Frank Funke , Frank Ohlbach , Till Gerlach
发明人： Joachim Pfeffinger , Michael Hüllmann , Arthur Höhn , Frank Funke , Frank Ohlbach , Till Gerlach
IPC分类号： C07C20948
CPC分类号： C07C209/48 , C07C211/11
摘要： Secondary amines of the formula (II) (X—CH2—)2NH (II) where X is a C1-20-alkyl, C2-20-alkenyl or C3-8-cycloalkyl group which may be unsubstituted or substituted by C1-20-alkyl, C3-8-cycloalkyl, C4-20-alkylcycloalkyl, C4-20-cycoalkylalkyl, C2-20-alkoxyalkyl, C6-14-aryl, C7-20-alkylaryl, C7-20-aralkyl, C1-20-alkoxy, hydroxy, C1-20-hydroxyalkyl, amino, C1-20-alkylamino, C2-20-dialkylamino, C2-12-alkenylamino, C3-8-cycloalkylamino, arylamino, diarylamino, aryl-C1-8-alkylamino, halogen, mercapto, C2-20-alkenyloxy, C3-8-cycloalkoxy, aryloxy and/or C2-8-alkoxycarbonyl, are prepared by reacting nitriles of the formula (III) X—CN (III) with hydrogen at from 20 to 250° C. and pressures of from 60 to 350 bar in the presence of an Rh-containing catalyst comprising from 0.1 to 5% by weight, based on the total weight of the catalyst, of Rh on a support to give mixtures of primary amines of the formula (I) X—CH2—NH2 (I) and secondary amines of the formula (II) (X—CH2—)2NH (II) and returning at least part of the primary amines separated from the mixtures obtained to the reaction.
摘要翻译：式（II）的仲胺，其中X是可以是未取代的或被C 1-20 - 烷基，C 3-8 - 环烷基，C 4 -C 18环烷基，C 3-8 - C 20-20烷基烷基，C 2-20 - 烷氧基烷基，C 6-14 - 芳基，C 7-20 - 烷基芳基，C 7-20 - 芳烷基，C 1-20 - 烷氧基，羟基，C 1-20 - 羟基烷基，氨基， C 1-20 - 烷基氨基，C 2-20 - 二烷基氨基，C 2-12 - 烯基氨基，C 3-8 - 环烷基氨基，芳基氨基，二芳基氨基，芳基-C 1-8 - 烷基氨基，卤素，巯基，C 2-20 - 烯氧基，环烷氧基，芳氧基和/或C 2-8 - 烷氧基羰基，通过在含Rh的催化剂存在下，使式（III）的腈与20至250℃的压力和60至350巴的压力反应来制备包含基于催化剂总重量的0.1至5重量％的Rh在载体上以得到式（I）的伯胺和式（II）的仲胺的混合物，并使至少部分从获得的混合物中分离出伯胺反应。

19. 发明授权

US06525222B2 Process for preparing amines 有权
标题翻译：制备胺的方法
公开(公告)号：US06525222B2
公开(公告)日：2003-02-25
申请号：US09729458
申请日：2000-12-05
申请人： Jan Nouwen , Arthur Höhn , Horst Neuhauser , Frank Funke , Stephan Andreas Schunk , Johann-Peter Melder , Knut Eger , Michael Hesse , Joachim Wulff-Döring
发明人： Jan Nouwen , Arthur Höhn , Horst Neuhauser , Frank Funke , Stephan Andreas Schunk , Johann-Peter Melder , Knut Eger , Michael Hesse , Joachim Wulff-Döring
IPC分类号： C07C20900
CPC分类号： C07C213/02 , C07C209/26 , C07C2601/08 , C07C2602/08 , C07C2602/10 , C07C211/35 , C07C211/42 , C07C217/58
摘要： Amines are prepared by reacting aldehydes or ketones at elevated temperature under elevated pressure with nitrogen compounds selected from the group of ammonia, primary and secondary amines, and with hydrogen in the presence of a catalyst, wherein the catalytically active mass of the catalyst contains, after its preparation and before the treatment with hydrogen, 22 to 45% by weight of oxygen-containing compounds of zirconium, calculated as ZrO2, 1 to 30% by weight of oxygen-containing compounds of copper, calculated as CuO, 5 to 50% by weight of oxygen-containing compounds of nickel, calculated as NiO, where the molar ratio of nickel to copper is greater than 1, 5 to 50% by weight of oxygen-containing compounds of cobalt, calculated as CoO, 0 to 5% by weight of oxygen-containing compounds of molybdenum, calculated as MoO3, and 0 to 10% by weight of oxygen-containing compounds of aluminum and/or manganese, calculated as Al2O3 or MnO2.
摘要翻译：通过使升高的温度下的醛或酮与选自氨，伯和仲胺的氮化合物和在催化剂存在下与氢气反应的醛或酮进行反应来制备胺，其中催化剂的催化活性物质含有其制备方法和用氢处理之前，按重量计22％至45％的锆的氧含量化合物，按ZrO2计算，按重量计为CuO的含氧化合物为铜，按CuO计为5〜50％按NiO计的含镍化合物的重量，其中镍与铜的摩尔比大于1.5至50重量％的以CoO计的含氧化合物的钴，0至5重量％按MoO3计算的含氧化合物的钼和0至10重量％的按Al2O3或MnO2计算的含铝和/或锰的含氧化合物。

20. 发明授权

US06563004B2 Process for preparing monoisopropylamine 失效
标题翻译：单异丙胺的制备方法
公开(公告)号：US06563004B2
公开(公告)日：2003-05-13
申请号：US09729461
申请日：2000-12-05
申请人： Jan Nouwen , Stefan Käshammer , Arthur Höhn , Frank Funke , Johann-Peter Melder , Frank Gutschoven , Philip Buskens
发明人： Jan Nouwen , Stefan Käshammer , Arthur Höhn , Frank Funke , Johann-Peter Melder , Frank Gutschoven , Philip Buskens
IPC分类号： C07C20926
CPC分类号： C07C209/26 , C07C211/06
摘要： Monoisopropylamine is prepared by reacting acetone with ammonia and with hydrogen at elevated temperature and elevated pressure in the presence of a catalyst, wherein the catalytically active mass of the catalyst comprises, after its preparation and before the treatment with hydrogen, from 20 to 90% by weight of aluminum oxide (Al2O3), zirconium dioxide (ZrO2), titanium dioxide (TiO2) and/or silicon dioxide (SiO2), from 1 to 70% by weight of oxygen-containing compounds of copper, calculated as CuO, from 1 to 70% by weight of oxygen-containing compounds of nickel, calculated as NiO, and from 1 to 70% by weight of oxygen-containing compounds of cobalt, calculated as CoO.
摘要翻译：通过使丙酮与氨和氢气在升高的温度和升高的压力下在催化剂存在下反应制备单异丙胺，其中催化活性物质在其制备之后和在用氢处理之前包含20-90％氧化铝（Al 2 O 3），二氧化锆（ZrO 2），二氧化钛（TiO 2）和/或二氧化硅（SiO 2）的重量，1至70重量％的以CuO计的氧含氧化合物，1至 70重量％的以NiO计的含氧化合物的镍和1-70重量％的以CoO计的钴的含氧化合物。

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