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11. 发明授权

US06967236B1 Methods of processing and synthesizing electrically conductive polymers and precursors thereof to form electrically conductive polymers having high electrical conductivity 失效
标题翻译：加工和合成导电聚合物及其前体以形成具有高电导率的导电聚合物的方法
公开(公告)号：US06967236B1
公开(公告)日：2005-11-22
申请号：US09036458
申请日：1998-03-06
申请人： Marie Angelopoulos , Yun-Hsin Liao
发明人： Marie Angelopoulos , Yun-Hsin Liao
IPC分类号： C08F6/00 , C08J3/00 , H01B1/00 , H01B1/12
CPC分类号： H01B1/128 , C08J3/093 , C08J2300/12 , C08J2379/02
摘要： The present invention is directed to methods of solvating electrically conducting polymers and electrically conducting polymers by processing these materials in selected solvents comprising at least one of the solvents being a fluorinated solvent. High solubility and conductivity in the hundreds of S/cm are achieved by these methods. Excellent coatings are attained. These materials have application in EMI shielding, electrodes for displays, contacts for devices, ESD protection, corrosion protection and resists.
摘要翻译：本发明涉及通过在选择的溶剂中处理这些材料来溶剂化导电聚合物和导电聚合物的方法，所述溶剂包括至少一种溶剂为氟化溶剂。通过这些方法可实现数百S / cm的高溶解度和导电性。获得优异的涂层。这些材料适用于EMI屏蔽，显示器用电极，器件触点，ESD保护，防腐蚀和抗蚀剂。

12. 发明授权

US06616863B1 Plasticized, antiplasticized and crystalline conducting polymers and precursors thereof 有权
标题翻译：增塑的，抗塑化的和结晶的导电聚合物及其前体
公开(公告)号：US06616863B1
公开(公告)日：2003-09-09
申请号：US09208528
申请日：1998-12-09
申请人： Marie Angelopoulos , Yun-Hsin Liao , Ravi F. Saraf
发明人： Marie Angelopoulos , Yun-Hsin Liao , Ravi F. Saraf
IPC分类号： H01B112
CPC分类号： C08G61/12 , H01B1/128
摘要： Materials containing precursors to electrically conductive polymers and electrically conductive polymers are described which have a high degree of crystallinity. The high degree of crystallinity is achieved by preparing the materials under conditions which provide a high degree of mobility to the polymer molecules permitting them to associate with one another to form a crystalline state. High levels of electrical conductivity are achieved in the electrically conductive materials without stretch orienting the material. The enhanced electrical conductivity is isotropic as compared to a stretch oriental film which has isotropic electrical conductivity.
摘要翻译：描述了具有高结晶度的导电聚合物和导电聚合物的前体的材料。通过在允许它们彼此结合以形成结晶状态的聚合物分子提供高度迁移率的条件下制备材料来实现高结晶度。在导电材料中实现高水平的导电性而不使材料拉伸取向。与具有各向同性电导率的拉伸东方薄膜相比，增强的导电性是各向同性的。

13. 发明授权

US5932143A Polycrystalline conducting polymers and precursors thereof having adjustable morphology and physical properties 失效
标题翻译：具有可调节形态和物理性质的多晶导电聚合物及其前体
公开(公告)号：US5932143A
公开(公告)日：1999-08-03
申请号：US620618
申请日：1996-03-22
申请人： Marie Angelopoulos , Yun-Hsin Liao , Ravi F. Saraf
发明人： Marie Angelopoulos , Yun-Hsin Liao , Ravi F. Saraf
IPC分类号： C08G61/12 , H01B1/12 , C08K5/54
CPC分类号： C08G61/12 , H01B1/128 , Y10T428/249958
摘要： Polycrystalline materials containing crystallies of precursors to electrically conductive polymers and electrically conductive polymers are described which have an adjustable high degree of crystallinity. The intersticial regions between the crystallites contains amorphous material containing precursors to electrically conductive polymers and/or electrically conductive polymers. The degree of crystallinity is achieved by preparing the materials under conditions which provide a high degree of mobility to the polymer molecules permitting them to associate with one another to form a crystalline state. This is preferable achieved by including additives, such as plasticizers and diluents, to the solution from which the polycrystalline material is formed. The morphology of the polycrystalline material is adjustable to modify the properties of the material such as the degree of crystallinity, crystal grain size, glass transition temperature, thermal coefficient of expansion and degree of electrical conductivity. High levels of electrical conductivity are achieved in in the electrically conductive polycrystalline materials without stretch orienting the material. The enhanced electrical conductivity is isotropic as compared to a stretch oriented film which has isotropic electrical conductivity.
摘要翻译：描述了具有可调节高结晶度的导电聚合物和导电聚合物的前体结晶的多晶材料。微晶之间的区域包含含有导电聚合物和/或导电聚合物的前体的无定形材料。通过在允许它们彼此结合以形成结晶状态的聚合物分子提供高度迁移率的条件下制备材料来实现结晶度。优选通过将诸如增塑剂和稀释剂的添加剂添加到形成多晶材料的溶液中来实现。可以调节多晶材料的形态，以改变材料的性质，例如结晶度，晶粒尺寸，玻璃化转变温度，热膨胀系数和电导率。在导电多晶材料中实现高水平的导电性，而不拉伸定向该材料。与具有各向同性电导率的拉伸取向膜相比，增强的导电性是各向同性的。

14. 发明授权

US08198396B2 Methods of fabricating plasticized, antiplasticized and crystalline conducting polymers and precursors thereof 有权
标题翻译：制造增塑的，抗增塑的和结晶的导电聚合物及其前体的方法
公开(公告)号：US08198396B2
公开(公告)日：2012-06-12
申请号：US12583030
申请日：2009-08-12
申请人： Marie Angelopoulos , Yun-Hsin Liao , Ravi F. Saraf
发明人： Marie Angelopoulos , Yun-Hsin Liao , Ravi F. Saraf
IPC分类号： C08G73/00 , C08G73/20 , H01B1/12 , C08F6/10
CPC分类号： H01B1/128
摘要： Methods of forming materials containing precursors to electrically conductive polymers and electrically conductive polymers are described which have a high degree of crystallinity. The high degree of crystallinity is achieved by preparing the materials under conditions which provide a high degree of mobility to the polymer molecules permitting them to associate with one another to form a crystalline state. High levels of electrical conductivity are achieved in in the electrically conductive materials without stretch orienting the material. The enhanced electrical conductivity is isotropic as compared to a stretch oriented film which has isotropic electrical conductivity. In the preferred embodiment, additives are added to a solution containing a solvent and the precursor or electrically conductive polymer. The additives are preferably plasticizer of diluents. As the solvent is removed the material dries and contains a higher degree of crystallinity than in the absence of the additive.
摘要翻译：描述了形成具有高结晶度的导电聚合物和导电聚合物前体的材料的方法。通过在允许它们彼此结合以形成结晶状态的聚合物分子提供高度迁移率的条件下制备材料来实现高结晶度。在导电材料中实现高水平的导电性而不使材料拉伸定向。与具有各向同性电导率的拉伸取向膜相比，增强的导电性是各向同性的。在优选的实施方案中，将添加剂加入到含有溶剂和前体或导电聚合物的溶液中。添加剂优选稀释剂的增塑剂。当除去溶剂时，与不存在添加剂相比，材料干燥并含有更高的结晶度。

15. 发明授权

US5969024A Methods of fabricating plasticized, antiplasticized and crystalline conducting polymers and precursors thereof 失效
公开(公告)号：US5969024A
公开(公告)日：1999-10-19
申请号：US620631
申请日：1996-03-22
申请人： Marie Angelopoulos , Yun-Hsin Liao , Ravi F. Saraf
发明人： Marie Angelopoulos , Yun-Hsin Liao , Ravi F. Saraf
IPC分类号： C08G61/12 , H01B1/12 , C08K5/54 , C08G73/00
CPC分类号： H01B1/128 , C08G61/12
摘要： Methods of forming materials containing precursors to electrically conductive polymers and electrically conductive polymers are described which have a high degree of crystallinity. The high degree of crystallinity is achieved by preparing the materials under conditions which provide a high degree of mobility to the polymer molecules permitting them to associate with one another to form a crystalline state. High levels of electrical conductivity are achieved in in the electrically conductive materials without stretch orienting the material. The enhanced electrical conductivity is isotropic as compared to a stretch oriented film which has isotropic electrical conductivity. In the preferred embodiment, additives are added to a solution containing a solvent and the precursor or electrically conductive polymer. The additives are preferably plasticizer of diluents. As the solvent is removed the material dries and contains a higher degree of crystallinity than in the absence of the additive.

16. 发明授权

US5370825A Water-soluble electrically conducting polymers, their synthesis and use 失效
标题翻译：水溶性导电聚合物，其合成和用途
公开(公告)号：US5370825A
公开(公告)日：1994-12-06
申请号：US25490
申请日：1993-03-03
申请人： Marie Angelopoulos , Jeffrey D. Gelorme , Thomas H. Newman , Niranjan M. Patel , David E. Seeger
发明人： Marie Angelopoulos , Jeffrey D. Gelorme , Thomas H. Newman , Niranjan M. Patel , David E. Seeger
IPC分类号： C08G61/12 , C08G61/10 , C08G75/02 , C08G75/04 , C08J3/28 , C08L33/00 , C08L33/02 , C08L41/00 , C08L79/00 , C08L101/00 , C08L101/02 , C08L101/12 , G03F7/038 , G03F7/09 , H01B1/12 , H01B1/00
CPC分类号： G03F7/093 , G03F7/038 , H01B1/128
摘要： Disclosed is a novel composition of matter comprising a polyacid and a polymer containing repeating units which contain one or more basic atoms. The complex is water-soluble and electrically conductive. The complex is useful in providing organic discharge layers for use in electronic applications and fabrications.
摘要翻译：公开了一种包含多酸和含有含有一个或多个碱性原子的重复单元的聚合物的新物质组合物。该复合物是水溶性和导电性的。该复合物可用于提供用于电子应用和制造的有机放电层。

17. 发明授权

US06241913B1 Branched electrically conductive polymers and precursors and applications thereof 失效
标题翻译：支链导电聚合物及其前体及其应用
公开(公告)号：US06241913B1
公开(公告)日：2001-06-05
申请号：US08722283
申请日：1996-09-27
申请人： Marie Angelopoulos , Yun-Hsin Liao
发明人： Marie Angelopoulos , Yun-Hsin Liao
IPC分类号： H01B112
CPC分类号： C08G73/1071 , C08G2261/312 , C08L101/12 , H01B1/128
摘要： The present invention is directed to a polymer selected from a precursor to an electrically conductive polymer and an electrically conductive polymer. The polymer has a branched structure. The polymer is formed from polymerization of momomers of which at least one monomer has more than one polymerizable site. One of the polymerizable monomers or units can have structural formula X—(M)n where X is a base element of the unit, M is the polymerization functional site, n is the number of M sites; and n>1. The polymer can be formed from more than one polymerization unit having different base elements, polymerization functional units and different values of n.
摘要翻译：本发明涉及一种选自导电聚合物的前体和导电聚合物的聚合物。聚合物具有支链结构。聚合物由其中至少一个单体具有多于一个可聚合位点的单体的聚合形成。可聚合单体或单元之一可以具有结构式X-（M）n，其中X是单元的基础元素，M是聚合官能位点，n是M位点的数目; 而n> 1。聚合物可由多于一个具有不同碱基元素，聚合官能单元和不同n值的聚合单元形成。

18. 发明授权

US5928566A Plasticized, antiplasticized and crystalline conducting polymers 失效
标题翻译：增塑，抗塑化和结晶导电聚合物
公开(公告)号：US5928566A
公开(公告)日：1999-07-27
申请号：US620619
申请日：1996-03-22
申请人： Marie Angelopoulos , Yun-Hsin Liao , Ravi F. Saraf
发明人： Marie Angelopoulos , Yun-Hsin Liao , Ravi F. Saraf
IPC分类号： C08K5/10 , C08G61/12 , C08K5/09 , C08K5/103 , C08K5/28 , C08K5/42 , C08K5/5419 , C08L71/02 , C08L79/00 , C08L83/04 , C08L101/00 , H01B1/12
CPC分类号： C08G61/12 , H01B1/128
摘要： Materials containing precursors to electrically conductive polymers and electrically conductive polymers are described which have a high degree of crystallinity. The high degree of crystallinity is achieved by preparing the materials under conditions which provide a high degree of mobility to the polymer molecules permitting them to associate with one another to form a crystalline state. High levels of electrical conductivity are achieved in in the electrically conductive materials without stretch orienting the material. The enhanced electrical conductivity is isotropic as compared to a stretch oriented film which has isotropic electrical conductivity.
摘要翻译：描述了具有高结晶度的导电聚合物和导电聚合物的前体的材料。通过在允许它们彼此结合以形成结晶状态的聚合物分子提供高度迁移率的条件下制备材料来实现高结晶度。在导电材料中实现高水平的导电性而不使材料拉伸定向。与具有各向同性电导率的拉伸取向膜相比，增强的导电性是各向同性的。

19. 发明授权

US5958301A Methods of fabricating branched electrially conductive polymers and precursors thereof 失效
标题翻译：支化电导电聚合物及其前体的制备方法
公开(公告)号：US5958301A
公开(公告)日：1999-09-28
申请号：US722284
申请日：1996-09-27
申请人： Marie Angelopoulos , Yun-Hsin Liao
发明人： Marie Angelopoulos , Yun-Hsin Liao
IPC分类号： H01B1/12
CPC分类号： H01B1/128 , H01B1/127
摘要： The present invention is directed to a method for fabricating a polymer selected from a precursor to an electrically conductive polymer and an electrically conductive polymer. The polymer has a branched structure. According to the present invention the branched polymer is formed from polymerization of monomers of which at least one monomer has more than one polymerizable site. One of the polymerizable monomers or units can have structural formula X--(M).sub.n where X is a base element of the unit, M is the polymerization functional site, and n is the number of M sites; n>1. The polymer can be formed from more than one polymerizable unit having different base elements, polymerization functional sites and different values of n.
摘要翻译：本发明涉及一种制备选自导电聚合物和导电聚合物的前体的聚合物的方法。聚合物具有支链结构。根据本发明，支化聚合物由至少一种单体具有多于一个可聚合位点的单体的聚合形成。其中一个可聚合单体或单元可以具有结构式X-（M）n，其中X是单元的基础元素，M是聚合官能位点，n是M位点的数目; n> 1。聚合物可以由具有不同碱基元素，聚合官能位点和不同n值的多于一个可聚合单元形成。

20. 发明授权

US5202061A Electrically conductive polymeric materials and uses thereof 失效
标题翻译：导电聚合材料及其用途
公开(公告)号：US5202061A
公开(公告)日：1993-04-13
申请号：US717968
申请日：1991-06-20
申请人： Marie Angelopoulos , Wu-Song Huang , Richard D. Kaplan , Marie-Annick Le Corre , Stanley E. Perreault , Jane M. Shaw , Michel R. Tissier , George F. Walker
发明人： Marie Angelopoulos , Wu-Song Huang , Richard D. Kaplan , Marie-Annick Le Corre , Stanley E. Perreault , Jane M. Shaw , Michel R. Tissier , George F. Walker
IPC分类号： C08G61/12 , H01B1/12 , H01J29/86 , H01L23/498 , H01L23/60 , H05K9/00
CPC分类号： H05K9/0079 , C08G61/12 , H01B1/125 , H01B1/127 , H01B1/128 , H01J29/868 , H01L23/49894 , H01L23/60 , H05K9/0081 , H01L2924/0002
摘要： Structures containing conducting polymers and methods of fabrication thereof. Electrical conductivity can be induced in polymers selected from the group of substituted and unsubstituted polyanilines, polyparaphenylenvinyles, substituted and unsubstituted polythiophenes substituted and unsubstituted poly-p-phenylene sulfides, substituted polyfuranes, substituted polypyrroles, substituted polyselenophene, polyacetylines formed from soluble precursors, combinations thereof and blends thereof with other polymers. The polymer contains a doping precursor, selected from the group of onium salts, iodonium salts, triflate salts, borate salts and tosylate salts and sulfonoxylimides. Conductivity can be selectively induced in the polymer by selectively doping upon selective exposure to a source of energy such as electromagnetic radiation, an electron beam and heat. The electrically conductive polymers of the present invention are useful as electron discharge layers for electron beam applications, such as, SEM observations, as electromagnetic interference coatings on dielectric surfaces and as electron beam resist which acts as a discharge layer.
摘要翻译：含有导电聚合物的结构及其制造方法。可以在选自取代和未取代的聚苯胺，聚对苯二烯基乙烯基，取代和未取代的聚噻吩，取代和未取代的聚对苯硫醚，取代的聚呋喃，取代的聚吡咯，取代的聚硒酚，由可溶性前体形成的聚乙炔，其组合及其与其它聚合物的共混物。聚合物含有选自鎓盐，碘鎓盐，三氟甲磺酸盐，硼酸盐和甲苯磺酸盐和磺酰氧基酰亚胺的掺杂前体。通过在选择性地暴露于诸如电磁辐射，电子束和热能的能量源上选择性掺杂，可以在聚合物中选择性地诱导电导率。本发明的导电聚合物可用作用于电子束应用的电子放电层，例如SEM观察，作为电介质表面上的电磁干扰涂层和用作放电层的电子束抗蚀剂。

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