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    • 12. 发明授权
    • Method for making tabular silver halide grains
    • 制备片状卤化银颗粒的方法
    • US5595864A
    • 1997-01-21
    • US274363
    • 1994-07-13
    • Marc Van den ZegelMarcel Mestdagh
    • Marc Van den ZegelMarcel Mestdagh
    • G03C1/00G03C1/005G03C1/015G03C1/035G03C5/16G03C5/29G03C5/30
    • G03C1/0051G03C5/16G03C5/30Y10S430/167
    • A photographic material has been coated on at least one side of a support with in at least one photosensitive layer hexagonal and/or circular tabular silver halide emulsion crystals occupying at least 70% of the total projected area of all grains, having a thickness of 0.15 to 0.30 .mu.m, a coefficient of variation of the tabular grains between 0.15 and 0.45 and an average aspect ratio of at least 2:1, prepared in the absence of ammonia by growing the nuclei, prepared at a pBr value between 1.0 and 2.0 and consuming less than 10% by weight of silver nitrate, during a first growth step at a pBr value between 1.0 and 2.5 consuming at least 10% by weight of silver nitrate and during a second growth step at a pBr value higher than 2.7 during the addition of at least 40% of the total amount of silver nitrate used. The loss in sensitivity and gradation after development of said material in a diluted cheap developer after exposing said photographic material containing said emulsion grains is neglectable in comparison with the characteristics obtained after development in stronger high quality developers.
    • 照相材料已经涂覆在载体的至少一侧上,在至少一个感光层中,六面体和/或圆形片状卤化银乳剂晶体占据所有晶粒的总投影面积的至少70%,其厚度为0.15 在0.30和2.0之间制备的片状颗粒在0.15和0.45之间的变异系数和在不存在氨的情况下通过生长核制备的平均纵横比为至少2:1,pBr值为1.0-2.0,以及 消耗少于10重量%的硝酸银,在第一生长步骤中,pBr值在1.0和2.5之间消耗至少10重量%的硝酸银,并且在第二个生长步骤期间,在加入期间,pBr值高于2.7 至少占所用硝酸银总量的40%。 在曝光含有所述乳剂颗粒的照相材料之后,在稀释的便宜显影剂中,所述材料在显影后的敏感度和等级的损失与较强的高质量显影剂开发后获得的特性相比是可忽略的。