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11. 发明授权

US6046283A Rubber-modified rigid silicone resins and composites produced therefrom 失效
标题翻译：橡胶改性的刚性硅树脂及其制备的复合材料
公开(公告)号：US6046283A
公开(公告)日：2000-04-04
申请号：US67945
申请日：1998-04-28
申请人： Dimitris Elias Katsoulis , John Robert Keryk , Frederick Jerome McGarry , Bizhong Zhu
发明人： Dimitris Elias Katsoulis , John Robert Keryk , Frederick Jerome McGarry , Bizhong Zhu
IPC分类号： C08L83/05 , C08L83/04 , C08L83/07 , C08F283/00
CPC分类号： C08L83/04 , C08G77/12 , C08G77/14 , C08G77/16 , C08G77/18 , C08G77/20 , C08G77/26 , C08G77/70
摘要： Novel rubber-modified rigid silicone resins are disclosed. The novel resins are the copolymerized reaction product of (A) an organosilicon composition selected from the group consisting (I) an organosilicone resin, (II) hydrolyzable precursors of (I), and an hydrolyzate of (II), (B1) a first silicone rubber having a nonfunctional linear chain length between functional groups from 6 to 100 and (B2) a second silicone ruberr having terminal functional groups and a degree of polymerization from about 200 to 1,000. The novel rubber-modified rigid silicone resins of the invention show remarkably high fracture toughness, K.sub.Ic, and critical strain energy release rate G.sub.Ic.
摘要翻译：公开了新型橡胶改性的刚性硅树脂。新型树脂是（A）有机硅组合物的共聚反应产物，其选自（I）有机硅氧烷树脂，（II）（I）的可水解前体和（II）的水解产物，（B1）第一官能团之间具有6至100的非官能线性链长度的硅橡胶和（B2）具有末端官能团的第二硅氧烷残余物和约200至1,000的聚合度。本发明的新型橡胶改性刚性有机硅树脂显示出非常高的断裂韧性，KIc和临界应变能释放速率GIc。

12. 发明授权

US08356407B2 Method of releasing high temperature films and/or devices from metallic substrates 失效
标题翻译：从金属基板释放高温膜和/或器件的方法
公开(公告)号：US08356407B2
公开(公告)日：2013-01-22
申请号：US11991831
申请日：2006-08-30
申请人： Nicole Anderson , Dimitris Elias Katsoulis , Bizhong Zhu
发明人： Nicole Anderson , Dimitris Elias Katsoulis , Bizhong Zhu
IPC分类号： C08J5/18 , B32B27/00 , C09D183/04 , B29C41/00
CPC分类号： B22C3/00 , B29C37/0067 , C08J5/18 , C08J2383/04 , C09D183/04 , Y10T29/49124 , Y10T29/49155 , Y10T29/49227 , Y10T428/31663
摘要： Films and electronic devices can be released from metallic substrates by: (i) applying a coating of a polysilsesquioxane resin to a metallic substrate, (ii) heating the coated metallic substrate to a temperature sufficient to cure the polysilsesquioxane resin, (iii) applying a polymeric film to the cured coating on the metallic substrate, (iv) further heating the coated metallic substrate to a temperature sufficient to cure the polymeric film, (v) optionally fabricating electronic devices on the polymeric film, and (vi) releasing the polymeric film from the metallic substrate.
摘要翻译：薄膜和电子器件可以通过以下方式从金属基底释放：（i）将聚倍半硅氧烷树脂的涂层施加到金属基底上，（ii）将涂覆的金属基底加热至足以固化聚倍半硅氧烷树脂的温度，（iii）（iv）将涂覆的金属基底进一步加热到足以固化聚合物膜的温度，（v）任选地在聚合物膜上制造电子器件，和（vi）释放聚合物膜从金属基底。

13. 发明授权

US06310146B1 Silsesquioxane resin with high strength and fracture toughness and method for the preparation thereof 有权
$Silsesquioxane resin with high strength and fracture toughness and method for the preparation thereof$
标题翻译：具有高强度和断裂韧性的倍半硅氧烷树脂及其制备方法
公开(公告)号：US06310146B1
公开(公告)日：2001-10-30
申请号：US09345638
申请日：1999-07-01
申请人： Dimitris Elias Katsoulis , Zhongtao Li , Frederick Jerome McGarry , Bihn Thanh Nguyen , Bizhong Zhu
发明人： Dimitris Elias Katsoulis , Zhongtao Li , Frederick Jerome McGarry , Bihn Thanh Nguyen , Bizhong Zhu
IPC分类号： C08L8305
CPC分类号： C08L83/14 , C08G77/12 , C08G77/20 , C08L83/04 , C09D183/14 , C08L2666/44
摘要： A cured silsesquioxane resin and method for its preparation are disclosed. By using a silyl-terminated hydrocarbon in the hydrosilylation reaction curable composition used to prepare the cured silsesquioxane resin, the cured silsesquioxane resin has improved strength and toughness without significant loss of modulus. A typical silyl-terminated hydrocarbon useful in this invention is silphenylene.
摘要翻译：公开了一种固化的倍半硅氧烷树脂及其制备方法。通过在用于制备固化倍半硅氧烷树脂的氢化硅烷化反应固化性组合物中使用甲硅烷基封端的烃，固化的倍半硅氧烷树脂具有改善的强度和韧性，而没有显着的模量损失。用于本发明的典型甲硅烷基封端的烃是硅亚苯基。

14. 发明申请

US20090098393A1 Method of Releasing High Temperature Films and/or Devices from Metallic Substrates 失效
标题翻译：从金属基板上释放高温膜和/或器件的方法
公开(公告)号：US20090098393A1
公开(公告)日：2009-04-16
申请号：US11991831
申请日：2006-08-30
申请人： Nicole Anderson , Dimitris Elias Katsoulis , Bizhong Zhu
发明人： Nicole Anderson , Dimitris Elias Katsoulis , Bizhong Zhu
IPC分类号： B32B27/00 , B29C41/00
CPC分类号： B22C3/00 , B29C37/0067 , C08J5/18 , C08J2383/04 , C09D183/04 , Y10T29/49124 , Y10T29/49155 , Y10T29/49227 , Y10T428/31663
摘要： Films and electronic devices can be released from metallic substrates by: (i) applying a coating of a polysilsesquioxane resin to a metallic substrate, (ii) heating the coated metallic substrate to a temperature sufficient to cure the polysilsesquioxane resin, (iii) applying a polymeric film to the cured coating on the metallic substrate, (iv) further heating the coated metallic substrate to a temperature sufficient to cure the polymeric film, (v) optionally fabricating electronic devices on the polymeric film, and (vi) releasing the polymeric film from the metallic substrate.
摘要翻译：薄膜和电子器件可以通过以下方式从金属基底释放：（i）将聚倍半硅氧烷树脂的涂层施加到金属基底上，（ii）将涂覆的金属基底加热至足以固化聚倍半硅氧烷树脂的温度，（iii）（iv）将涂覆的金属基底进一步加热到足以固化聚合物膜的温度，（v）任选地在聚合物膜上制造电子器件，和（vi）释放聚合物膜从金属基底。

15. 发明申请

US20100093242A1 Composite Article Having Excellent Fire Resistance 审中-公开
标题翻译：具有优异耐火性能的复合材料
公开(公告)号：US20100093242A1
公开(公告)日：2010-04-15
申请号：US12527873
申请日：2008-02-21
申请人： Dimitris Elias Katsoulis , Widland Robert O'Brien , Aaron Seitz , Bizhong Zhu
发明人： Dimitris Elias Katsoulis , Widland Robert O'Brien , Aaron Seitz , Bizhong Zhu
IPC分类号： B32B27/08 , B32B9/04 , D03D25/00 , D04H13/00
CPC分类号： B32B17/10018 , B32B17/10036 , B32B17/10366 , B32B17/1055 , B32B17/10798 , B32B25/20 , C08J7/047 , C08J2483/00 , Y10T428/31663 , Y10T442/30 , Y10T442/60
摘要： A composite article includes a first window layer formed from a vitreous material and a reinforced silicone layer disposed adjacent the first window layer. The reinforced silicone layer includes a cured silicone composition and a fiber reinforcement. Due to the presence of the cured silicone composition in the reinforced silicone layer, the composite article exhibits excellent fire resistance and will not emit as much smoke and toxic gases as composite articles including primarily carbon-based materials. Further, due to the presence of the fiber reinforcement in the reinforced silicone layer, the composite article maintains excellent structural integrity even after a breach is formed in the composite article due to heat. As such, the composite articles of the subject invention may be suitable for load-bearing applications that are not possible with existing composite articles.
摘要翻译：复合制品包括由玻璃质材料形成的第一窗口层和邻近第一窗口层设置的增强硅树脂层。增强的硅氧烷层包括固化的硅氧烷组合物和纤维增强物。由于在增强的硅氧烷层中存在固化的硅氧烷组合物，复合制品表现出优异的耐火性，并且不会像主要包含碳基材料的复合制品那样排放与烟气和有毒气体一样多的烟雾和有毒气体。此外，由于增强硅树脂层中存在纤维增强物，所以即使在复合制品中由于热而形成破裂之后，复合制品也保持优异的结构完整性。因此，本发明的复合制品可适用于现有复合制品不可能的承载应用。

16. 发明申请

US20090090413A1 Cadmium Telluride-Based Photovoltaic Device And Method Of Preparing The Same 审中-公开
标题翻译：碲化镉基光伏器件及其制备方法
公开(公告)号：US20090090413A1
公开(公告)日：2009-04-09
申请号：US12297367
申请日：2007-04-18
申请人： Dimitris Elias Katsoulis , Bizhong Zhu
发明人： Dimitris Elias Katsoulis , Bizhong Zhu
IPC分类号： H01L31/00
CPC分类号： H01L31/0392 , C08G77/12 , C09D183/04 , H01L31/03925 , H01L31/03926 , H01L31/073 , H01L31/1836 , Y02E10/543
摘要： A cadmium telluride (CdTe)-based photovoltaic device includes a CdTe layer including cadmium and telluride. The CdTe-based photovoltaic device further includes a substrate including a silicone layer formed from a silicone composition. The substrate, because it includes the composition, is both flexible and sufficiently able to withstand annealing temperatures in excess of 350° C., and frequently in excess of 500° C., to obtain maximum efficiency of the device.
摘要翻译：基于碲化镉（CdTe）的光伏器件包括CdTe层，包括镉和碲化物。基于CdTe的光电器件还包括由硅氧烷组合物形成的硅氧烷层的衬底。由于它包括组合物，基材既柔软又足够能承受超过350℃的退火温度，并且经常超过500℃，以获得最大的器件效率。

17. 发明授权

US06368535B1 Condensation reaction curable silsesquioxane resin composition and methods for the synthesis and cure thereof 有权
标题翻译：缩合反应固化倍半硅氧烷树脂组合物及其合成和固化方法
公开(公告)号：US06368535B1
公开(公告)日：2002-04-09
申请号：US09369413
申请日：1999-08-06
申请人： Dimitris Elias Katsoulis , Bizhong Zhu
发明人： Dimitris Elias Katsoulis , Bizhong Zhu
IPC分类号： B29C7100
CPC分类号： C08G77/52 , C08G77/50 , C09D183/14
摘要： A condensation reaction curable silsesquioxane resin composition and methods for its preparation and cure are disclosed. By modifying the silsesquioxane resin with a silyl-terminated hydrocarbon, such as a silphenylene, the resulting silsesquioxane resin has improved strength and toughness without significant loss of modulus.
摘要翻译：公开了缩合反应固化倍半硅氧烷树脂组合物及其制备和固化方法。通过用甲硅烷基封端的烃如硅亚苯基改性倍半硅氧烷树脂，所得的倍半硅氧烷树脂具有改善的强度和韧性，而没有显着的模量损失。

18. 发明授权

US5830950A Method of making rubber-modified rigid silicone resins and composites produced therefrom 失效
标题翻译：制备橡胶改性的刚性硅树脂及其制备的复合材料的方法
公开(公告)号：US5830950A
公开(公告)日：1998-11-03
申请号：US775557
申请日：1996-12-31
申请人： Dimitris Elias Katsoulis , John Robert Keryk , Frederick Jerome McGarry , Bizhong Zhu
发明人： Dimitris Elias Katsoulis , John Robert Keryk , Frederick Jerome McGarry , Bizhong Zhu
IPC分类号： C08L83/04 , C08F283/00
CPC分类号： C08L83/04 , C08G77/12 , C08G77/14 , C08G77/16 , C08G77/18 , C08G77/20 , C08G77/26 , C08G77/70
摘要： Novel rubber-modified rigid silicone resins a novel method of making the same are disclosed. The resins are the copolymerized reaction product of (A) an organosilicon composition selected from the group consisting (I) an organosilicone resin, (II) hydrolyzable precursors of (I), and an hydrolyzate of (II) and (B) an silicone rubber. In the method of the invention, the copolymerization step is carried out in an organic solvent, preferably utilizing a relatively weak condensation catalyst. Thereafter, the solution is devolatilized and the composition cured by heating.
摘要翻译：公开了新型橡胶改性的刚性有机硅树脂的制备方法。树脂是（A）有机硅组合物的共聚合反应产物，其选自（I）有机硅氧烷树脂，（II）可水解的（I）前体和（II）的水解产物和（B）硅橡胶。在本发明的方法中，共聚步骤在有机溶剂中进行，优选利用较弱的缩合催化剂。此后，溶液脱挥发分，组合物通过加热固化。

19. 发明申请

US20120045629A1 Vinylhydrogenpolysiloxane Adhesive Composition 审中-公开
标题翻译：乙烯基聚硅氧烷粘合剂组合物
公开(公告)号：US20120045629A1
公开(公告)日：2012-02-23
申请号：US13318747
申请日：2010-04-06
申请人： Nathan Greer , Marilyn Shope , Michitaka Suto , Bianxiao Zhong , Bizhong Zhu
发明人： Nathan Greer , Marilyn Shope , Michitaka Suto , Bianxiao Zhong , Bizhong Zhu
IPC分类号： B32B3/00 , C09J183/07
CPC分类号： C08G77/20 , B32B17/10 , B32B27/28 , B32B2383/00 , C08G77/12 , Y10T428/24802
摘要： Vinylhydrogenpolysiloxanes are provided. The vinylhydrogenpolysiloxanes comprise organopolysiloxanes having at least two silicon-bonded hydrogen atoms and at least two silicon-bonded vinyl groups. As a fraction of the total number of silicon atoms in the vinylhydrogenpolysiloxanes, about 25% to about 90% of the silicon atoms are bonded to a hydrogen atom and about 10% to about 45% are bonded to a vinyl group. The ratio of the number of silicon-bonded hydrogen groups to the number of silicon-bonded vinyl groups is about 1.3 to about 6. Also provided are silicone compositions comprising at least one vinylhydrogenpolysiloxane and a hydrosilylation catalyst; silicone adhesives comprising a cured product of at least one vinylhydrogenpolysiloxane; and laminates comprising at least one such silicone adhesive. When subjected to high temperatures or direct flame, the vinylhydrogenpolysiloxanes form chars that retain adhesion to various substrates.
摘要翻译：提供乙烯基聚硅氧烷。乙烯基氢聚硅氧烷包括具有至少两个与硅键合的氢原子和至少两个与硅键合的乙烯基的有机聚硅氧烷。作为乙烯基氢聚硅氧烷中硅原子总数的一部分，约25％至约90％的硅原子与氢原子结合，约10％至约45％与乙烯基结合。与硅键合的乙烯基基团的数量的比例为约1.3至约6.还提供了包含至少一种乙烯基氢聚硅氧烷和氢化硅烷化催化剂的硅氧烷组合物; 包含至少一种乙烯基氢聚硅氧烷的固化产物的硅氧烷粘合剂; 以及包含至少一种这种硅氧烷粘合剂的层压材料。当经受高温或直接火焰时，乙烯基氢聚硅氧烷形成保留对各种基材的粘合性的炭。

20. 发明申请

US20080051548A1 Reinforced Silicone Resin Film and Method of Preparing Same 失效
标题翻译：增强硅树脂薄膜及其制备方法
公开(公告)号：US20080051548A1
公开(公告)日：2008-02-28
申请号：US11794924
申请日：2006-02-01
申请人： Debbie Bailey , Dimitris Katsoulis , Michitaka Suto , Bizhong Zhu
发明人： Debbie Bailey , Dimitris Katsoulis , Michitaka Suto , Bizhong Zhu
IPC分类号： C08L83/04 , B32B25/20
CPC分类号： C08J5/04 , C08J5/24 , C08J2383/04 , C08J2383/14 , C09D183/04 , C09D183/14 , Y10T428/31598 , C08L83/00
摘要： A method of preparing a reinforced silicone resin film, the method comprising the steps of impregnating a fiber reinforcement in a hydrosilylation-curable silicone composition comprising a silicone resin, and heating the impregnated fiber reinforcement at a temperature sufficient to cure the silicone resin, wherein the reinforced silicone resin film comprises from 10 to 99% (w/w) of the cured silicone resin and the film has a thickness of from 15 to 500 μm; and a reinforced silicone resin film prepared according to the method.
摘要翻译：一种制备增强硅树脂薄膜的方法，该方法包括以下步骤：将纤维增强物浸渍在包含硅树脂的氢化硅烷化可固化的硅氧烷组合物中，并在足以固化硅树脂的温度下加热浸渍的纤维增强体，其中增强有机硅树脂膜包含10至99％（w / w）的固化的有机硅树脂，该膜的厚度为15至500μm; 和根据该方法制备的增强硅树脂膜。

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