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11. 发明授权

US6160154A Method and catalyst system for producing aromatic carbonates 失效
标题翻译：用于生产芳族碳酸酯的方法和催化剂体系
公开(公告)号：US6160154A
公开(公告)日：2000-12-12
申请号：US301698
申请日：1999-04-29
申请人： James Lawrence Spivack , Donald Wayne Whisenhunt, Jr. , James Norman Cawse , Bruce Fletcher Johnson , Marsha Mottel Grade , Grigorii Lev Soloveichik , John Yaw Ofori , Eric James Pressman
发明人： James Lawrence Spivack , Donald Wayne Whisenhunt, Jr. , James Norman Cawse , Bruce Fletcher Johnson , Marsha Mottel Grade , Grigorii Lev Soloveichik , John Yaw Ofori , Eric James Pressman
IPC分类号： B01J31/20 , B01J23/89 , B01J31/28 , C07B61/00 , C07C68/00 , C07C69/96
CPC分类号： B01J31/2234 , B01J23/89 , B01J31/0231 , B01J31/0235 , B01J2231/321 , B01J2531/16 , B01J2531/38 , B01J2531/46 , B01J2531/54 , B01J2531/62 , B01J2531/72 , B01J2531/824 , B01J2531/842 , B01J2531/847 , C07C68/005 , C07C69/96
摘要： A method and catalyst system for economically producing aromatic carbonates from aromatic hydroxy compounds. In one embodiment, the present invention provides a method of carbonylating aromatic hydroxy compounds by contacting at least one aromatic hydroxy compound with oxygen and carbon monoxide in the presence of a carbonylation catalyst system that includes a catalytic amount of an inorganic co-catalyst containing copper. In various alternative embodiments, the carbonylation catalyst system can include an effective amount of a palladium source and an effective amount of a halide composition. Further alternative embodiments can include catalytic amounts of various inorganic co-catalyst combinations.
摘要翻译：用于从芳族羟基化合物经济地生产芳族碳酸酯的方法和催化剂体系。在一个实施方案中，本发明提供了一种通过在包含催化量的含铜无机助催化剂的羰基化催化剂体系的存在下使至少一种芳族羟基化合物与氧和一氧化碳接触而使芳族羟基化合物羰基化的方法。在各种替代实施方案中，羰基化催化剂体系可以包括有效量的钯源和有效量的卤化物组合物。另外的替代实施方案可以包括催化量的各种无机助催化剂组合。

12. 发明授权

US06440893B1 Method and catalyst composition for producing aromatic carbonates 失效
标题翻译：用于生产芳族碳酸酯的方法和催化剂组合物
公开(公告)号：US06440893B1
公开(公告)日：2002-08-27
申请号：US09822158
申请日：2001-03-30
申请人： Kirill Vladimirovich Shalyaev , Bruce Fletcher Johnson , Donald Wayne Whisenhunt, Jr. , Grigorii Lev Soloveichik
发明人： Kirill Vladimirovich Shalyaev , Bruce Fletcher Johnson , Donald Wayne Whisenhunt, Jr. , Grigorii Lev Soloveichik
IPC分类号： B01J3028
CPC分类号： B01J31/0239 , B01J21/063 , B01J23/14 , B01J23/44 , B01J23/72 , B01J31/0251 , B01J31/128 , B01J31/2234 , B01J31/26 , B01J2219/0004 , B01J2231/321 , B01J2531/16 , B01J2531/38 , B01J2531/46 , B01J2531/72 , B01J2531/824 , C07C51/252 , C07C51/44 , C07C51/48 , C07C68/005 , C07C69/96 , C07C57/04
摘要： A method and catalyst composition for economically producing aromatic carbonates from aromatic hydroxy compounds is disclosed. The present invention provides a method for carbonylating aromatic hydroxy compounds, comprising the step of contacting at least one aromatic hydroxy compound with oxygen and carbon monoxide in the presence of a halide-free carbonylation catalyst composition comprising an effective amount of at least one Group 8, 9, or 10 metal source, an effective amount of a first inorganic co-catalyst comprising at least one Group 14 metal source, an effective amount of a salt co-catalyst, and optionally an effective amount of a second inorganic co-catalyst selected from the group consisting of a Group 4 metal source, a Group 7 metal source, a Group 11 metal source, and a lanthanide element source, and optionally an effective amount of a base. A significant advantage of the present method and catalyst compositions is that no halide is present or required in the reaction mixture for catalytic activity.
摘要翻译：公开了一种用于从芳族羟基化合物经济地生产芳族碳酸酯的方法和催化剂组合物。本发明提供了一种芳族羟基化合物的羰基化方法，包括使至少一种芳香族羟基化合物与氧和一氧化碳在不含卤化物的羰基化催化剂组合物存在下接触的步骤，该组合物包含有效量的至少一种第8族， 9或10个金属源，有效量的第一无机助催化剂，其包含至少一种第14族金属源，有效量的盐助催化剂和任选的有效量的第二无机助催化剂，其选自由4族金属源，7族金属源，11族金属源和镧系元素源组成的组，以及任选的有效量的碱。本发明方法和催化剂组合物的显着优点是在反应混合物中不存在或需要用于催化活性的卤化物。

13. 发明授权

US06372683B2 Method and catalyst system for producing aromatic carbonates 失效
标题翻译：用于生产芳族碳酸酯的方法和催化剂体系
公开(公告)号：US06372683B2
公开(公告)日：2002-04-16
申请号：US09757247
申请日：2001-01-10
申请人： Kirill Vladimirovich Shalyaev , Grigorii Lev Soloveichik , Bruce Fletcher Johnson , Donald Wayne Whisenhunt, Jr.
发明人： Kirill Vladimirovich Shalyaev , Grigorii Lev Soloveichik , Bruce Fletcher Johnson , Donald Wayne Whisenhunt, Jr.
IPC分类号： B01J3100
CPC分类号： C07C68/005 , C07C69/96
摘要： A method and catalyst system for producing aromatic carbonates from aromatic hydroxy compounds. In one embodiment, the method includes the step of contacting at least one aromatic hydroxy compound with oxygen and carbon monoxide in the presence of a carbonylation catalyst system having catalytic amounts of the following components: a Group VIII B metal source; a combination of inorganic co-catalysts including a copper source and at least one of a titanium source or a zirconium source; an onium chloride composition; and a base. Alternative embodiments include inorganic co-catalyst combinations of a lead source and at least one of a titanium source or a manganese source.
摘要翻译：用于由芳族羟基化合物制备芳族碳酸酯的方法和催化剂体系。在一个实施方案中，该方法包括在具有催化量的以下组分的羰基化催化剂体系的存在下使至少一种芳族羟基化合物与氧和一氧化碳接触的步骤：VIIIB族金属源; 包括铜源和至少一种钛源或锆源的无机助催化剂的组合; 氯化铟组合物; 和一个基地。替代实施方案包括铅源和钛源或锰源中的至少一种的无机助催化剂组合。

14. 发明授权

US06365538B1 Method and catalyst system for producing aromatic carbonates 失效
标题翻译：用于生产芳族碳酸酯的方法和催化剂体系
公开(公告)号：US06365538B1
公开(公告)日：2002-04-02
申请号：US09495538
申请日：2000-01-31
申请人： Kirill Vladimirovich Shalyaev , Grigorii Lev Soloveichik , Bruce Fletcher Johnson , Donald Wayne Whisenhunt, Jr.
发明人： Kirill Vladimirovich Shalyaev , Grigorii Lev Soloveichik , Bruce Fletcher Johnson , Donald Wayne Whisenhunt, Jr.
IPC分类号： B01J3100
CPC分类号： B01J31/26 , B01J31/0202 , B01J31/0204 , B01J31/06 , B01J31/2234 , B01J31/2409 , B01J2231/34 , B01J2531/16 , B01J2531/38 , B01J2531/42 , B01J2531/48 , B01J2531/72 , B01J2531/824 , B01J2531/842 , B01J2531/847 , C07C68/005 , C07C69/96
摘要： A method and catalyst system for producing aromatic carbonates from aromatic hydroxy compounds. In one embodiment, the method includes the step of contacting at least one aromatic hydroxy compound with oxygen and carbon monoxide in the presence of a carbonylation catalyst system having catalytic amounts of the following components: a Group VIII B metal source; an alkaline metal chloride; a polyether; and a base. Alternative embodiments substitute a catalytic amount of a nitrile promoter for the polyether.
摘要翻译：用于由芳族羟基化合物制备芳族碳酸酯的方法和催化剂体系。在一个实施方案中，该方法包括在具有催化量的以下组分的羰基化催化剂体系的存在下使至少一种芳族羟基化合物与氧和一氧化碳接触的步骤：VIIIB族金属源; 碱金属氯化物; 聚醚和一个基地。替代实施例将催化量的腈促进剂替代为聚醚。

15. 发明授权

US06355824B2 Catalyst system for producing aromatic carbonates 失效
标题翻译：用于生产芳族碳酸酯的催化剂体系
公开(公告)号：US06355824B2
公开(公告)日：2002-03-12
申请号：US09729123
申请日：2000-12-04
申请人： Ben Purushotam Patel , Grigorii Lev Soloveichik , Donald Wayne Whisenhunt, Jr. , Kirill Vladimirovich Shalyaev
发明人： Ben Purushotam Patel , Grigorii Lev Soloveichik , Donald Wayne Whisenhunt, Jr. , Kirill Vladimirovich Shalyaev
IPC分类号： C07C6800
CPC分类号： C07C68/005 , C07C69/96
摘要： A method and catalyst system for producing aromatic carbonates from aromatic hydroxy compounds. In one embodiment, the method includes the step of contacting at least one aromatic hydroxy compound with oxygen and carbon monoxide in the presence of a carbonylation catalyst system having an effective amount of an iron source in the absence of a Group VIII B metal source. In various alternative embodiments, the carbonylation catalyst system can include at least one inorganic co-catalyst, as well as a halide composition and/or a base.
摘要翻译：用于由芳族羟基化合物制备芳族碳酸酯的方法和催化剂体系。在一个实施方案中，该方法包括在不存在第VIIIB族金属源的情况下，在具有有效量的铁源的羰基化催化剂体系存在下使至少一种芳族羟基化合物与氧和一氧化碳接触的步骤。在各种替代实施方案中，羰基化催化剂体系可以包括至少一种无机助催化剂，以及卤化物组合物和/或碱。

16. 发明授权

US06355597B1 Catalyst system for producing aromatic carbonates 失效
标题翻译：用于生产芳族碳酸酯的催化剂体系
公开(公告)号：US06355597B1
公开(公告)日：2002-03-12
申请号：US09559855
申请日：2000-04-27
申请人： James Lawrence Spivack , Donald Wayne Whisenhunt, Jr. , James Norman Cawse , Bruce Fletcher Johnson , Kirill Shalyaev
发明人： James Lawrence Spivack , Donald Wayne Whisenhunt, Jr. , James Norman Cawse , Bruce Fletcher Johnson , Kirill Shalyaev
IPC分类号： B01J2316
CPC分类号： C07C68/005 , C07C69/96
摘要： A catalyst system for economically producing aromatic carbonates from aromatic hydroxy compounds. In one embodiment, the present invention provides a carbonylation catalyst system that includes a catalytic amount of an inorganic co-catalyst containing bismuth. In various alternative embodiments, the carbonylation catalyst system can include an effective amount of a palladium source and an effective amount of a halide composition. Further alternative embodiments can include catalytic amounts of various inorganic co-catalyst combinations.
摘要翻译：用于从芳族羟基化合物经济地生产芳族碳酸酯的催化剂体系。在一个实施方案中，本发明提供了包含催化量的含有铋的无机助催化剂的羰基化催化剂体系。在各种替代实施方案中，羰基化催化剂体系可以包括有效量的钯源和有效量的卤化物组合物。另外的替代实施方案可以包括催化量的各种无机助催化剂组合。

17. 发明授权

US09496748B2 Integrated power system control method and related apparatus with energy storage element 有权
公开(公告)号：US09496748B2
公开(公告)日：2016-11-15
申请号：US13547250
申请日：2012-07-12
申请人： Christopher James Chuah , Herman Lucas Norbert Wiegman , Donald Wayne Whisenhunt, Jr. , Roger Neil Bull , Kalyan Bukkasamudram , Connor Brady , Mark Gotobed
发明人： Christopher James Chuah , Herman Lucas Norbert Wiegman , Donald Wayne Whisenhunt, Jr. , Roger Neil Bull , Kalyan Bukkasamudram , Connor Brady , Mark Gotobed
IPC分类号： H02J9/00 , H02J7/00 , H02J7/04 , H02J9/06 , H02J7/14 , H02J15/00
CPC分类号： H02J7/041 , H02J7/04 , H02J7/044 , H02J7/14 , H02J9/066 , H02J15/00 , Y02B10/72 , Y10T307/625 , Y10T307/696
摘要： Systems and methods for controlling a hybrid power architecture to provide fuel or energy savings. Recharge time of an energy storage device (ESD) is reduced through the application of a controlled potential and ESD recharge time management over the life of the hybrid system through manipulation of the ESD charge state window of operation. Fuel or energy savings is achieved by controlling the partial-state-of-charge (PSOC) window of the ESD based on a recharge resistance profile of the ESD and by controlling a charging potential applied to the ESD based on a recharge current and/or the estimated recharge resistance profile of the ESD.

18. 发明授权

US07989580B2 Phosphorescent iridium complexes 有权
标题翻译：磷光铱络合物
公开(公告)号：US07989580B2
公开(公告)日：2011-08-02
申请号：US12260378
申请日：2008-10-29
申请人： Kyle Erik Litz , Kelly Scott Chichak , Donald Wayne Whisenhunt, Jr.
发明人： Kyle Erik Litz , Kelly Scott Chichak , Donald Wayne Whisenhunt, Jr.
IPC分类号： C08G79/00 , C07F15/00 , C09K11/06 , C09K11/08
CPC分类号： C07F15/0046 , C07F15/0033 , C07F15/06 , Y10S428/917
摘要： Metal complexes of formula I and IA and polymers derived from the complexes are useful in optoelectronic devices wherein M is Ir, Co or Rh; is a cyclometallated ligand; R1 is hydrogen, alkyl, substituted alkyl, aryl, substituted aryl, arylalkyl, or substituted arylalkyl; R2 is hydrogen, alkyl, substituted alkyl, aryl, substituted aryl, arylalkyl, substituted arylalkyl; and at least one of R1 and R2 is other than hydrogen; R1a is hydrogen, alkyl, substituted alkyl, aryl, substituted aryl, arylalkyl, or substituted arylalkyl; R2a is hydrogen, alkyl, substituted alkyl, aryl, substituted aryl, arylalkyl, substituted arylalkyl; and at least one of R1a and R2a is substituted alkyl, substituted aryl, substituted arylalkyl, and at least one substitutent of the substituted alkyl, substituted aryl, or substituted arylalkyl is a polymerizable group.
摘要翻译：式I和IA的金属络合物和衍生自络合物的聚合物可用于其中M为Ir，Co或Rh的光电器件; 是环金属配体; R 1是氢，烷基，取代的烷基，芳基，取代的芳基，芳基烷基或取代的芳基烷基; R2是氢，烷基，取代的烷基，芳基，取代的芳基，芳基烷基，取代的芳基烷基; 并且R 1和R 2中的至少一个不是氢; R 1a是氢，烷基，取代的烷基，芳基，取代的芳基，芳基烷基或取代的芳基烷基; R2a是氢，烷基，取代的烷基，芳基，取代的芳基，芳基烷基，取代的芳烷基; 并且R 1a和R 2a中的至少一个是取代的烷基，取代的芳基，取代的芳烷基，并且取代的烷基，取代的芳基或取代的芳烷基的至少一个取代基是可聚合基团。

19. 发明授权

US06534432B1 Catalyst compositions for producing aromatic carbonates 有权
标题翻译：用于生产芳族碳酸酯的催化剂组合物
公开(公告)号：US06534432B1
公开(公告)日：2003-03-18
申请号：US09662355
申请日：2000-09-15
申请人： James Lawrence Spivack , Donald Wayne Whisenhunt, Jr. , James Norman Cawse , Bruce Fletcher Johnson
发明人： James Lawrence Spivack , Donald Wayne Whisenhunt, Jr. , James Norman Cawse , Bruce Fletcher Johnson
IPC分类号： B01J3100
CPC分类号： B01J31/2234 , B01J23/60 , B01J31/0231 , B01J31/0239 , B01J31/0251 , B01J31/0271 , B01J2231/34 , B01J2531/16 , B01J2531/26 , B01J2531/38 , B01J2531/46 , B01J2531/48 , B01J2531/54 , B01J2531/62 , B01J2531/72 , B01J2531/821 , B01J2531/822 , B01J2531/824 , B01J2531/842 , B01J2531/845 , B01J2531/847 , C07C68/005 , C07C69/96
摘要： A method and catalyst system for economically producing aromatic carbonates from aromatic hydroxy compounds. In one embodiment, the present invention provides a method of carbonylating aromatic hydroxy compounds by contacting at least one aromatic hydroxy compound with oxygen and carbon monoxide in the presence of a carbonylation catalyst system that includes a catalytic amount of an inorganic co-catalyst containing zinc. In various alternative embodiments, the carbonylation catalyst system can include an effective amount of a palladium source and an effective amount of a halide composition. Further alternative embodiments can include catalytic amounts of various inorganic co-catalyst combinations.
摘要翻译：用于从芳族羟基化合物经济地生产芳族碳酸酯的方法和催化剂体系。在一个实施方案中，本发明提供了一种通过在包含催化量的含锌无机助催化剂的羰基化催化剂体系的存在下使至少一种芳族羟基化合物与氧和一氧化碳接触而使芳族羟基化合物羰基化的方法。在各种替代实施方案中，羰基化催化剂体系可以包括有效量的钯源和有效量的卤化物组合物。另外的替代实施方案可以包括催化量的各种无机助催化剂组合。

20. 发明授权

US06440892B1 Method and catalyst composition for producing aromatic carbonates 失效
标题翻译：用于生产芳族碳酸酯的方法和催化剂组合物
公开(公告)号：US06440892B1
公开(公告)日：2002-08-27
申请号：US09822138
申请日：2001-03-30
申请人： Kirill Vladimirovich Shalyaev , Grigorii Lev Soloveichik , Donald Wayne Whisenhunt, Jr. , Bruce Fletcher Johnson
发明人： Kirill Vladimirovich Shalyaev , Grigorii Lev Soloveichik , Donald Wayne Whisenhunt, Jr. , Bruce Fletcher Johnson
IPC分类号： B01J3128
CPC分类号： B01J31/2226 , B01J21/063 , B01J23/44 , B01J23/72 , B01J31/0239 , B01J31/2234 , B01J2231/321 , B01J2531/16 , B01J2531/46 , B01J2531/824
摘要： The present invention provides a method and catalyst composition for carbonylating aromatic hydroxy compounds, comprising the step of contacting at least one aromatic hydroxy compound with oxygen and carbon monoxide in the presence of a carbonylation catalyst composition comprising an effective amount of at least one Group 8, 9, or 10 metal source, an effective amount of a combination of inorganic co-catalysts comprising at least one Group 4 metal source and at least one Group 11 metal source, an effective amount of at least one salt co-catalyst with an anion selected from the group consisting of carboxylate, benzoate, acetate, sulfate, and nitrate, wherein the carbonylation catalyst composition is free of a halide source.
摘要翻译：本发明提供了用于羰基化芳族羟基化合物的方法和催化剂组合物，其包括在羰基化催化剂组合物存在下使至少一种芳族羟基化合物与氧和一氧化碳接触的步骤，所述羰基化催化剂组合物包含有效量的至少一种第8族， 9或10个金属源，有效量的包含至少一种第4族金属源和至少一种第11族金属源的无机助催化剂的组合，有效量的至少一种选择了阴离子的盐助催化剂由羧酸盐，苯甲酸盐，乙酸盐，硫酸盐和硝酸盐组成的组，其中羰基化催化剂组合物不含卤化物源。

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