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11. 发明公开

EP0805175A1 Oriented polyglycolic acid film and production process thereof 失效
标题翻译： Orientierte Folie ausPolyglykolsäureund Verfahren zu ihrer Herstellung
公开(公告)号：EP0805175A1
公开(公告)日：1997-11-05
申请号：EP97302904.4
申请日：1997-04-29
申请人： KUREHA KAGAKU KOGYO KABUSHIKI KAISHA
发明人： Kawakami, Yukichika , Sato, Nobuo , Hoshino, Mitsuru , Kouyama, Toshitaka , Shiiki, Zenya
IPC分类号： C08J5/18 , C08G63/06 , B65D65/46
CPC分类号： B29C55/06 , B29C55/143 , B29C55/28 , B29K2067/043 , B29K2067/046 , B29K2995/006 , C08G63/08 , C08J5/18 , C08J2367/04 , Y10S264/73 , Y10T428/249921 , Y10T428/25
摘要： The invention provides an oriented polyglycolic acid film formed from a thermoplastic resin material which comprises polyglycolic acid having a repeating unit represented by the following formula (1):
and the following physical properties:

(a) the melt viscosity, η* [as measured at a temperature of (the melting point, Tm of the polymer + 20°C) and a shear rate of 100/sec] being 500-100,000 Pa·s;
(b) the melting point, Tm being at least 150°C;
(c) the melt enthalpy, AHm being at least 20 J/g; and
(d) the density being at least 1.50 g/cm 3 as measured in an unoriented, crystallized form,
wherein the film has tensile strength of at least 150 MPa, and production processes thereof.
摘要翻译：本发明提供由热塑性树脂材料形成的取向聚乙醇酸膜，其包含具有下式（1）表示的重复单元的聚乙醇酸：＆lt; CHEM＆gt;和以下物理性质：（a）熔融粘度ηa 在（熔点，聚合物的Tm + 20℃）和100 / secu的剪切速率为500-10000Pa.s的温度下测量; （b）熔点Tm为至少150℃; （c）熔体焓AHm为至少20J / g; 和（d）以非取向的结晶形式测量的密度为至少1.50g / cm 3，其中所述膜具有至少150MPa的拉伸强度及其制备方法。

12. 发明公开

EP0508705A3 Processes for the production of arylene thioether oligomers and copolymers 失效
标题翻译：亚芳基二醇低聚物和共聚物的生产工艺
公开(公告)号：EP0508705A3
公开(公告)日：1993-01-07
申请号：EP92303017.5
申请日：1992-04-06
申请人： KUREHA KAGAKU KOGYO KABUSHIKI KAISHA
发明人： Sato, Hiroyuki , Hoshino, Mitsuru , Kawakami, Yukichika
IPC分类号： C08G75/02 , C08G81/02
CPC分类号： C08G75/0286 , C08G63/688
摘要： Disclosed herein are a process for the preparation of a carboxylated arylene thioether oligomer, in which an alkali metal sulfide is caused to act on a poly(arylene thioether) so as to depolymerize the poly(arylene thioether), thereby preparing an alkali thiolate-containing oligomer, and a carboxylating agent is then caused to act on the alkali thiolate-containing oligomer, thereby forming the carboxylated arylene thioether oligomer, and a process for the production of an arylene thioether copolymer, wherein the carboxylated arylene thioether oligomer alone, which has been obtained in accordance with this preparation process, or a mixture of the carboxylated oligomer in an amount of at least 50 wt.% and another carboxylic compound in an amount less than 50 wt.% is reacted with an alkylenediol or an alkylenediol and a polyester or an alkylene diol and a lactone.

13. 发明公开

EP0495457A3 Composition comprising polyarylene sulfide and polyamide 失效
标题翻译：包含聚亚锡硫化物和聚酰胺组合物的组合物
公开(公告)号：EP0495457A3
公开(公告)日：1992-10-21
申请号：EP92100509.6
申请日：1992-01-14
申请人： KUREHA KAGAKU KOGYO KABUSHIKI KAISHA
发明人： Kashiwadate, Ken , Hoshino, Mitsuru , Morinishi, Shuji , Kawakami, Yukichika
IPC分类号： C08L81/02 , C08L77/00
CPC分类号： C08L81/02 , C08L77/00
摘要： A composition is disclosed, comprising
(1) a polyamide as a dispersed phase and (2) a polyarylene sulfide as a continuous phase, wherein at least a part of the polyarylene sulfide has at least one modifying group directly bonded to the aromatic ring thereof, where the modifying group is selected from the group consisting of a carboxyl group, an alkali metal salt of a carboxyl group, and an alkaline earth metal salt of a carboxyl group, and where the modifying group is present at a ratio of 10 or more millimoles of the modifying group per kilogram of the polyamide. The composition has improved mechanical strength.

14. 发明公开

EP0459620A3 Production process of arylene thioether copolymer 失效
标题翻译：亚芳基共聚物的生产工艺
公开(公告)号：EP0459620A3
公开(公告)日：1992-02-26
申请号：EP91303615.8
申请日：1991-04-23
申请人： KUREHA KAGAKU KOGYO KABUSHIKI KAISHA
发明人： Kawakami, Yukichika , Hoshino, Mitsuru , Satake, Yoshikatsu
IPC分类号： C08G75/02
CPC分类号： C08G75/20 , C08G75/0227 , C08G75/024 , C08G75/0245 , C08G75/0295
摘要： Disclosed herein is a process for the production of an arylene thioether copolymer (C), wherein an alkali metal sulfide is caused to act on a poly(arylene thioether) (A) having predominant recurring units of the formula [I]:

wherein R denotes an alkyl group having 1-6 carbon atoms, and 1 stands for 0 or an integer of 1-4, in a water-containing polar organic solvent so as to depolymerize the poly(arylene thioether) (A), thereby preparing a prepolymer (B) having an alkali thiolate group on at least one terminal thereof and the resultant prepolymer (B) is then subjected to a polymerization reaction with at least one dihalogen-substituted aromatic compound.

15. 发明公开

EP0278788A3 PVC-based resin compositions and graft copolymers for use in these 失效
标题翻译：基于PVC的树脂组合物和在这些中使用的共聚物
公开(公告)号：EP0278788A3
公开(公告)日：1990-01-17
申请号：EP88301232.0
申请日：1988-02-15
申请人： KUREHA KAGAKU KOGYO KABUSHIKI KAISHA
发明人： Hoshino, Mitsuru , Yusa, Haruhiko , Suzuki, Katsumi
IPC分类号： C08L27/06 , C08F279/02
CPC分类号： C08F285/00 , C08L27/06 , C08L51/00 , C08F212/08 , C08L2666/24
摘要： A PVC-based resin composition comprises 3 - 30 wt.% of a graft copolymer and 97 - 70 wt.% of a PVC-based resin and has highly-balanced properties between impact resistance, transparency and stress-whitening resistance and excellent processing characteristics. The graft copolymer has been obtained by graft-polymerizing, in the presence of a latex containing 70 - 85 parts by weight of a rubbery butadiene-based polymer formed of 65 - 85 wt.% of butadiene, 15 - 35 wt.% of styrene and 0 - 3 wt.% of crosslinkable monomer, (i) 5 - 24 parts by weight of a first monomer mixture as a first-stage component, said first monomer mixture being composed of 70 - 97 wt.% of methyl methacrylate and 30 - 3 wt.% of an alkyl acrylate whose alkyl group has 1 - 8 carbon atoms; and then (ii) 3 - 21 parts by weight of a second monomer mixture as a second-stage component, said second monomer mixture being composed of 97 - 100 wt% of styrene and 0 - 3 wt.% of crosslinkable monomer. The sum of the first and second monomer mixtures and the rubbery butadiene-based polymer is 100 parts by weight. The monomers grafted in the first stage amount to 30 - 80 wt.% of the sum of the grafted monomers. The graft polymer is also new.

16. 发明公开

EP0278788A2 PVC-based resin compositions and graft copolymers for use in these 失效
标题翻译： Kunstharzmischungen auf PVC-Basis und zu ihrer Herstellung verwendbare Pfropfcopolymere。
公开(公告)号：EP0278788A2
公开(公告)日：1988-08-17
申请号：EP88301232.0
申请日：1988-02-15
申请人： KUREHA KAGAKU KOGYO KABUSHIKI KAISHA
发明人： Hoshino, Mitsuru , Yusa, Haruhiko , Suzuki, Katsumi
IPC分类号： C08L27/06 , C08F279/02
CPC分类号： C08F285/00 , C08L27/06 , C08L51/00 , C08F212/08 , C08L2666/24
摘要： A PVC-based resin composition comprises 3 - 30 wt.% of a graft copolymer and 97 - 70 wt.% of a PVC-based resin and has highly-balanced properties between impact resistance, transparency and stress-whitening resistance and excellent processing characteristics. The graft copolymer has been obtained by graft-polymerizing, in the presence of a latex containing 70 - 85 parts by weight of a rubbery butadiene-based polymer formed of 65 - 85 wt.% of butadiene, 15 - 35 wt.% of styrene and 0 - 3 wt.% of crosslinkable monomer, (i) 5 - 24 parts by weight of a first monomer mixture as a first-stage component, said first monomer mixture being composed of 70 - 97 wt.% of methyl methacrylate and 30 - 3 wt.% of an alkyl acrylate whose alkyl group has 1 - 8 carbon atoms; and then (ii) 3 - 21 parts by weight of a second monomer mixture as a second-stage component, said second monomer mixture being composed of 97 - 100 wt% of styrene and 0 - 3 wt.% of crosslinkable monomer. The sum of the first and second monomer mixtures and the rubbery butadiene-based polymer is 100 parts by weight. The monomers grafted in the first stage amount to 30 - 80 wt.% of the sum of the grafted monomers. The graft polymer is also new.
摘要翻译： PVC基树脂组合物包含3-30重量％的接枝共聚物和97-70重量％的PVC基树脂，并且在抗冲击性，透明度和耐应力白化性以及优异的加工特性之间具有高度平衡的性能。接枝共聚物通过在含有70-85重量份由65-85重量％丁二烯，15-35重量％苯乙烯形成的橡胶状丁二烯基聚合物的胶乳存在下进行接枝聚合而获得，和0-3重量％的可交联单体，（i）5-24重量份作为第一阶段组分的第一单体混合物，所述第一单体混合物由70-97重量％甲基丙烯酸甲酯和30重量％ - 3重量％的烷基具有1-8个碳原子的丙烯酸烷基酯; 然后（ii）3-21重量份作为第二阶段组分的第二单体混合物，所述第二单体混合物由97-100重量％的苯乙烯和0-3重量％的可交联单体组成。第一和第二单体混合物和橡胶状丁二烯类聚合物的总和为100重量份。在第一阶段中接枝的单体量为接枝单体总和的30-80重量％。接枝聚合物也是新的。

17. 发明授权

EP0494518B1 Process for production of poly(arylene thioether) copolymer 失效
标题翻译：生产聚（亚芳基硫醚）共聚物的方法
公开(公告)号：EP0494518B1
公开(公告)日：1998-05-20
申请号：EP91311588.7
申请日：1991-12-12
申请人： KUREHA KAGAKU KOGYO KABUSHIKI KAISHA
发明人： Hoshino, Mitsuru , Kawakami, Yukichika , Katto, Takayuki
IPC分类号： C08G75/02
CPC分类号： C08G75/0218

18. 发明公开

EP0806283A3 Stretch blow molded container and production process thereof 失效
标题翻译：在拉伸吹塑成型及其制备的容器和方法
公开(公告)号：EP0806283A3
公开(公告)日：1998-03-25
申请号：EP97303144.6
申请日：1997-05-08
申请人： KUREHA KAGAKU KOGYO KABUSHIKI KAISHA
发明人： Kawakami, Yukichika , Sato, Nobuo , Hoshino, Mitsuru , Kouyama, Toshitaka , Shiiki, Zenya
IPC分类号： B29C49/00 , C08L67/04
CPC分类号： B65D1/0207 , B29B2911/1402 , B29B2911/14026 , B29B2911/14033 , B29B2911/1404 , B29B2911/14106 , B29B2911/14133 , B29C49/0005 , C08L67/04 , C08L2666/02
摘要： The invention provides a stretch blow molded container formed from a thermoplastic resin material which comprises polyglycolic acid having
(a) a repeating unit represented by the following formula (1):
(b) a melt viscosity, η* [as measured at a temperature of (the melting point, Tm of the polymer + 20°C) and a shear rate of 100/sec] of 500-100,000 Pa·s; (c) a melting point, Tm of at least 180°C; (d) a melt enthalpy, ΔHm of at least 20 J/g; and (e) a density of at least 1.50 g/cm 3 as measured in an unoriented, crystallized form, wherein the stretch blow molded container has tensile strength (in a circumferential direction) of at least 100 MPa and a carbon dioxide permeability (as measured at a temperature of 23°C and 80% relative humidity; in terms of the thickness of 50 µm) of 300 cc/m 2 ·day·atm or smaller at the body sidewall thereof, and a production process thereof.

19. 发明授权

EP0508705B1 Processes for the production of arylene thioether oligomers and copolymers 失效
标题翻译：一种制备共聚物和Arylenthioetheroligomeren过程
公开(公告)号：EP0508705B1
公开(公告)日：1997-06-25
申请号：EP92303017.5
申请日：1992-04-06
申请人： KUREHA KAGAKU KOGYO KABUSHIKI KAISHA
发明人： Sato, Hiroyuki , Hoshino, Mitsuru , Kawakami, Yukichika
IPC分类号： C08G75/02 , C08G81/02
CPC分类号： C08G75/0286 , C08G63/688

20. 发明公开

EP0494518A3 Process for production of poly(arylene thioether) copolymer 失效
标题翻译：生产聚（亚乙基三乙氧基）共聚物的方法
公开(公告)号：EP0494518A3
公开(公告)日：1993-01-07
申请号：EP91311588.7
申请日：1991-12-12
申请人： KUREHA KAGAKU KOGYO KABUSHIKI KAISHA
发明人： Hoshino, Mitsuru , Kawakami, Yukichika , Katto, Takayuki
IPC分类号： C08G75/02
CPC分类号： C08G75/0218
摘要： Disclosed herein is a process for the production of a granular poly(arylene thioether) copolymer by polymerizing an alkali metal sulfide with dihalo-aromatic compounds including at least one dihalo-aromatic carboxylic acid in a polar solvent containing water. Upon the polymerization, at least a part of the dihalo-aromatic carboxylic acid is converted into an alkaline earth metal salt in advance, the hydroxide and/or oxide of an alkaline earth metal is added together with the dihalo-aromatic carboxylic acid to the polymerization reaction system, or the hydroxide and/or oxide of an alkaline earth metal is added together with an alkaline earth metal salt of the dihalo-aromatic carboxylic acid and the dihalo-aromatic carboxylic acid to the polymerization reaction system.

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