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11. 发明授权

US06673882B2 Supported single-site catalysts useful for olefin polymerization 失效
标题翻译：用于烯烃聚合的支持的单中心催化剂
公开(公告)号：US06673882B2
公开(公告)日：2004-01-06
申请号：US09781464
申请日：2001-02-12
申请人： Jia-Chu Liu
发明人： Jia-Chu Liu
IPC分类号： C08F442
CPC分类号： C08F10/00 , C08F4/659 , C08F4/65912 , C08F110/02 , Y10S526/943 , C08F4/65916 , C08F2500/12 , C08F2500/03 , C08F2500/18
摘要： A method for making supported single-site catalysts useful for olefin polymerization is disclosed. An organometallic complex that contains a nitrogen-functional heterocyclic ligand is first prepared and reacted with an alumoxane. This product is then combined, preferably with high-intensity mixing, with a slurry of inorganic support, followed by solvent removal to give a supported catalyst. By introducing the alumoxane at the right time during preparation, and by judicious selection and chemical treatment of the inorganic support, one can make catalysts with high activity and good aging properties. The supported catalysts give olefin polymers with a favorable balance of physical properties, including low density, narrow molecular weight distribution, good melt-flow properties, and high bulk density.
摘要翻译：公开了一种制备用于烯烃聚合的负载型单中心催化剂的方法。首先制备含有氮官能杂环配体的有机金属络合物，并与铝氧烷反应。然后将该产物与优选与高强度混合的无机载体浆料混合，然后除去溶剂得到负载型催化剂。通过在制备过程中合适的时间引入铝氧烷，通过对无机载体的合理选择和化学处理，可以制备具有高活性和良好老化性能的催化剂。负载型催化剂得到物理性能良好平衡的烯烃聚合物，包括低密度，窄分子量分布，良好的熔体流动性能和高堆积密度。

12. 发明授权

US06562973B1 Method for making late transition metal catalysts for olefin polymerization 失效
标题翻译：烯烃聚合后期过渡金属催化剂的制备方法
公开(公告)号：US06562973B1
公开(公告)日：2003-05-13
申请号：US09930629
申请日：2001-08-15
申请人： Jia-Chu Liu
发明人： Jia-Chu Liu
IPC分类号： C07F1500
CPC分类号： C07F15/045 , C07F15/025 , C07F15/065
摘要： Methods for making Group VIII metal bis(imine) complexes are disclosed. Each method uses a single reactor that is equipped with an internal filter to facilitate preparation and purification of the complex under an inert atmosphere. The complexes, which are useful in catalyst systems for olefin polymerization, are prepared in either one or two reaction steps. Surprisingly, the single-reactor approach to preparation and purification enables the efficient preparation of exceptionally high (>90%) yields of desirable Group VIII metal bis(imine) complexes.
摘要翻译：公开了制备VIII族金属双（亚胺）络合物的方法。每种方法使用装有内部过滤器的单个反应器，以便于在惰性气氛下制备和纯化络合物。可用于烯烃聚合的催化剂体系中的络合物在一个或两个反应步骤中制备。令人惊奇的是，单反应器的制备和纯化方法使得能够有效地制备所需的第VIII族金属双（亚胺）络合物的异常高（> 90％）产率。

13. 发明授权

US07091272B2 Olefin polymerization with pyridine moiety-containing single-site catalysts 失效
标题翻译：含有吡啶部分的单中心催化剂进行烯烃聚合
公开(公告)号：US07091272B2
公开(公告)日：2006-08-15
申请号：US10855921
申请日：2004-05-27
申请人： Jia-Chu Liu
发明人： Jia-Chu Liu
IPC分类号： C08J3/34 , C08K9/04
CPC分类号： C08F110/02 , C08F4/659 , C08F4/65908 , C08F4/65912 , C08F4/6592 , C08F10/00 , C08F4/64048 , C08F4/65916 , C08F2500/01 , C08F2500/18
摘要： An olefin polymerization process is disclosed. The polymerization is performed in the presence of a clay, an activator, and a transition metal complex that has at least one pyridine moiety-containing ligand. The presence of clay increases the catalyst activity. The process is suitable for making ultra-high molecular weight polyethylenes (UHMWPE). The UHMWPE produced has increased bulk density.
摘要翻译：公开了烯烃聚合方法。聚合在粘土，活化剂和具有至少一个含吡啶部分的配体的过渡金属络合物的存在下进行。粘土的存在增加了催化剂活性。该方法适用于制造超高分子量聚乙烯（UHMWPE）。生产的UHMWPE增加堆积密度。

14. 发明申请

US20050143538A1 LTMC polymerization of unsaturated monomers 有权
公开(公告)号：US20050143538A1
公开(公告)日：2005-06-30
申请号：US11064989
申请日：2005-02-24
申请人： Jia-Chu Liu , Shao-Hua Guo
发明人： Jia-Chu Liu , Shao-Hua Guo
IPC分类号： C08F210/00 , C08F210/02 , C08F212/00 , C08F214/00 , C08F216/00 , C08F218/00 , C08F220/00 , C08F4/44
CPC分类号： C08F210/02 , C08F220/12 , C08F220/10 , C08F2500/03 , C08F2500/02
摘要： A process for polymerizing unsaturated monomers is disclosed. The process comprises polymerizing, in the presence of a late transition metal catalyst (LTMC), a variety of unsaturated monomers which are traditionally, some of which are exclusively, made by free radical polymerizations. The LTMC polymerization provides the polymer with improved properties such as no free radical residue and narrow molecular weight distribution.

15. 发明申请

US20050143537A1 LTMC POLYMERIZATION OF UNSATURATED MONOMERS 有权
标题翻译：不饱和单体的LTMC聚合
公开(公告)号：US20050143537A1
公开(公告)日：2005-06-30
申请号：US10748582
申请日：2003-12-30
申请人： Jia-Chu Liu , Shao-Hua Guo
发明人： Jia-Chu Liu , Shao-Hua Guo
IPC分类号： C08F210/00 , C08F210/02 , C08F212/00 , C08F214/00 , C08F216/00 , C08F218/00 , C08F220/00 , C08F4/44
CPC分类号： C08F210/02 , C08F220/12 , C08F220/10 , C08F2500/03 , C08F2500/02
摘要： A process for polymerizing unsaturated monomers is disclosed. The process comprises polymerizing, in the presence of a late transition metal catalyst (LTMC), a variety of unsaturated monomers which are traditionally, some of which are exclusively, made by free radical polymerizations. The LTMC polymerization provides the polymer with improved properties such as no free radical residue and narrow molecular weight distribution.
摘要翻译：公开了聚合不饱和单体的方法。该方法包括在后期过渡金属催化剂（LTMC）的存在下聚合多种不饱和单体，这些单体通常是通过自由基聚合制成的。 LTMC聚合为聚合物提供了改进的性能，例如没有自由基残基和窄分子量分布。

16. 发明申请

US20050014915A1 Olefin polymerization with pyridine moiety-containing single-site catalysts 失效
标题翻译：含有吡啶部分的单中心催化剂进行烯烃聚合
公开(公告)号：US20050014915A1
公开(公告)日：2005-01-20
申请号：US10855921
申请日：2004-05-27
申请人： Jia-Chu Liu
发明人： Jia-Chu Liu
IPC分类号： C08F4/02 , C08F4/642 , C08F4/659 , C08F4/6592 , C08F10/00 , C08F110/02 , C08F4/44
CPC分类号： C08F110/02 , C08F4/659 , C08F4/65908 , C08F4/65912 , C08F4/6592 , C08F10/00 , C08F4/64048 , C08F4/65916 , C08F2500/01 , C08F2500/18
摘要： An olefin polymerization process is disclosed. The polymerization is performed in the presence of a clay, an activator, and a transition metal complex that has at least one pyridine moiety-containing ligand. The presence of clay increases the catalyst activity. The process is suitable for making ultra-high molecular weight polyethylenes (UHMWPE). The UHMWPE produced has increased bulk density.
摘要翻译：公开了烯烃聚合方法。聚合在粘土，活化剂和具有至少一个含吡啶部分的配体的过渡金属络合物的存在下进行。粘土的存在增加了催化剂活性。该方法适用于制造超高分子量聚乙烯（UHMWPE）。生产的UHMWPE增加堆积密度。

17. 发明授权

US06239239B1 Quinolinoxy and pyridinoxy single-site catalysts containing benzyl ligands 有权
标题翻译：含有苄基配体的喹啉氧基和吡啶氧基单中心催化剂
公开(公告)号：US06239239B1
公开(公告)日：2001-05-29
申请号：US09506023
申请日：2000-02-17
申请人： Jia-Chu Liu
发明人： Jia-Chu Liu
IPC分类号： C08F442
CPC分类号： C08F10/00 , C08F4/65908 , C08F4/65912 , C08F4/65916 , C08F4/659 , C08F4/64048 , C08F4/64055
摘要： An improved catalyst for polymerizing olefins is disclosed. The catalyst comprises a Group 4 transition metal, at least one quinolinoxy or pyridinoxy ligand, and at least one benzyl ligand. Particularly when used with an activator, the benzyl-containing catalysts have exceptional activities for polymerizing olefins.
摘要翻译：公开了一种用于聚合烯烃的改进的催化剂。催化剂包含第4族过渡金属，至少一种喹啉氧基或吡啶氧基配位体和至少一种苄基配体。特别是当与活化剂一起使用时，含苄基的催化剂具有用于聚合烯烃的特殊活性。

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