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11. 发明授权

US07030188B2 Multi-phase polypropylene compositions 有权
标题翻译：多相聚丙烯组合物
公开(公告)号：US07030188B2
公开(公告)日：2006-04-18
申请号：US10816389
申请日：2004-04-01
申请人： Maged G. Botros , Mark P. Mack , James H. Meas , Clifford C. Lee
发明人： Maged G. Botros , Mark P. Mack , James H. Meas , Clifford C. Lee
IPC分类号： C08L51/06
CPC分类号： C08L23/10 , C08F255/02 , C08K7/14 , C08L23/0861 , C08L23/12 , C08L23/16 , C08L25/12 , C08L27/06 , C08L27/08 , C08L51/06 , C08L55/02 , C08L67/00 , C08L69/00 , C08L71/00 , C08L77/00 , C08L2205/00 , C08L2205/02 , C08L2205/03 , C08L2205/035 , C08L2666/24 , C08L2666/02 , C08L2666/04
摘要： Improved multi-phase polypropylene composites are provided. The compositions are comprised of a polypropylene base resin, a non-compatible dispersed phase which can be a polymer or filler material and a propylene-ethylene copolymer grafted with a carboxylic acid or carboxylic acid derivative.
摘要翻译：提供改进的多相聚丙烯复合材料。组合物由聚丙烯基础树脂，可以是聚合物或填料材料的不相容的分散相和用羧酸或羧酸衍生物接枝的丙烯 - 乙烯共聚物组成。

12. 发明授权

US06844402B1 Preparation of olefin-acrylic copolymers with late transition metal catalysts 有权
标题翻译：用过渡金属催化剂制备烯烃 - 丙烯酸共聚物
公开(公告)号：US06844402B1
公开(公告)日：2005-01-18
申请号：US10733631
申请日：2003-12-11
申请人： Jia-Chu Liu , Mark P. Mack , Shao-Hua Guo
发明人： Jia-Chu Liu , Mark P. Mack , Shao-Hua Guo
IPC分类号： C08F210/00 , C08F210/02 , C08F4/52
CPC分类号： C08F210/02 , C08F10/00 , C08F220/12 , C08F4/7042
摘要： A process for making olefin-acrylic copolymers is disclosed. The process comprises polymerizing an olefin and an acrylic monomer in the presence of an activator and a Group 8-10 late transition metal complex. The late transition metal catalyst contains an isoindoline ligand.
摘要翻译：公开了制备烯烃 - 丙烯酸共聚物的方法。该方法包括在活化剂和第8-10族晚期过渡金属络合物的存在下聚合烯烃和丙烯酸类单体。后期过渡金属催化剂含有异二氢吲哚配体。

13. 发明授权

US06838410B2 Catalysts for making polyolefins 失效
标题翻译：制造聚烯烃的催化剂
公开(公告)号：US06838410B2
公开(公告)日：2005-01-04
申请号：US10382233
申请日：2003-03-05
申请人： Shaotian Wang , Clifford C. Lee , Mark P. Mack , Gregory G. Hlatky , Sandor Nagy , Barbara M. Tsuie , Craig C. Meverden
发明人： Shaotian Wang , Clifford C. Lee , Mark P. Mack , Gregory G. Hlatky , Sandor Nagy , Barbara M. Tsuie , Craig C. Meverden
IPC分类号： C08F4/642 , C08F4/659 , C08F210/16 , B01J31/00 , B01J37/00 , C08F4/02 , C08F4/60
CPC分类号： C08F210/16 , C08F4/65908 , C08F4/65912 , C08F4/65916 , Y02P20/52 , Y10S526/943 , C08F4/6592 , C08F210/08 , C08F2500/10 , C08F2500/08 , C08F2500/03 , C08F210/14 , C08F2500/01 , C08F2500/17
摘要： A process for making ethylene copolymers is disclosed. Ethylene copolymerizes with an α-olefin in the presence of a catalyst system comprising an activator and a silica-supported, bridged indenoindolyl metal complex having “open architecture.” The supported complex incorporates comonomers with exceptional efficiency, and the process gives ethylene copolymers having high molecular weights (Mw>100K) and very low densities (
摘要翻译：公开了制备乙烯共聚物的方法。在包含活化剂和具有“开放结构”的二氧化硅负载的桥连茚并吲哚基金属络合物的催化剂体系的存在下，乙烯与α-烯烃共聚。支持的络合物以卓越的效率引入共聚单体，该方法得到具有高分子量（Mw> 100K）和非常低密度（<0.910G / CM 3）的乙烯共聚物。还描述了包括连接吲哚吲哚基骨架的吲哚基氮的开放式结构催化剂。另外，负载和未负载的茚并[1,2-b]吲哚基催化剂在弹性体聚丙烯和乙烯共聚物的制备中提供了卓越的活性。

14. 发明授权

US4433123A Polymerization process for drag reducing substances 失效
标题翻译：减阻剂聚合工艺
公开(公告)号：US4433123A
公开(公告)日：1984-02-21
申请号：US262870
申请日：1981-05-12
申请人： Mark P. Mack
发明人： Mark P. Mack
IPC分类号： C08F10/00 , C08F4/64
CPC分类号： C08F10/00
摘要： A method is provided for the production of ultrahigh molecular weight drag reducing substances and the like comprising:(a) preparing under an inert atmosphere a catalyst comprising: p1 (1) titanium halide of the general formula TiX.sub.m wherein m=2.5 to 4.0;(2) a co-catalyst of the formula AlR.sub.n X.sub.3-n where R is a hydrocarbon radical, X is a halogen or hydrogen and n is 2 or 3;(3) a phosphorous compound of the formula PR.sub.1 R.sub.2 R.sub.3 or P(OR.sub.1) (OR.sub.2) (OR.sub.3) where R.sub.1, R.sub.2, and R.sub.3 are, independently, aryl, alkyl, aralkyl, or alkaryl, containing from 1 to 12 carbon atoms and placing the catalyst in contact with;(b) alpha-monoolefinic hydrocarbons from C.sub.2 -C.sub.30 under suitable temperature conditions to provide a hydrocarbon soluble ultrahigh molecular weight polymer, then ceasing polymerization at a polymer content level of 20% by weight or less, based on the total reaction mixture.
摘要翻译：提供了一种生产超高分子量减阻物质等的方法，包括：（a）在惰性气氛下制备催化剂，该催化剂包含：p1（1）通式TiXm的卤化钛，其中m = 2.5至4.0; （2）式AlRnX3-n的助催化剂，其中R是烃基，X是卤素或氢，n是2或3; （3）通式为PR1R2R3或P（OR1）（OR2）（OR3）的磷化合物，其中R 1，R 2和R 3独立地为含有1至12个碳原子的芳基，烷基，芳烷基或烷芳基，催化剂接触; （b）在合适的温度条件下从C2-C30得到的α-单烯烃，以提供烃溶性超高分子量聚合物，然后基于总反应混合物停止聚合物含量为20重量％以下的聚合。

15. 发明授权

US4289679A Method for producing solutions of drag reducing substances 失效
标题翻译：制造减阻剂物质的方法
公开(公告)号：US4289679A
公开(公告)日：1981-09-15
申请号：US103317
申请日：1979-12-14
申请人： Mark P. Mack
发明人： Mark P. Mack
IPC分类号： C08J3/09 , C09K3/18 , C08J3/08 , C08K5/01
CPC分类号： C08J3/09 , C09K3/18 , C08J2323/02
摘要： A method of producing ultra-high molecular weight polymers useful as drag reducing substances or antimist agents comprising;(1) polymerizing an alpha-olefin or olefins from 2 to 30 carbon atoms with a Ziegler catalyst in a light hydrocarbon solvent;(2) adding a heavy hydrocarbon diluent or a non-solvent suspending agent to the resulting polymer or copolymer mixture, and(3) removing substantially all of the light hydrocarbon component.
摘要翻译：一种制备可用作减阻剂或抗凝剂的超高分子量聚合物的方法，包括：（1）在轻烃溶剂中用齐格勒催化剂聚合2-30个碳原子的α-烯烃或烯烃; （2）向所得聚合物或共聚物混合物中加入重质烃稀释剂或非溶剂悬浮剂，和（3）基本上除去所有的轻烃组分。

16. 发明申请

US20100076160A1 Modifying tubular LDPE with free radical initiator 有权
标题翻译：用自由基引发剂改性管状LDPE
公开(公告)号：US20100076160A1
公开(公告)日：2010-03-25
申请号：US12284486
申请日：2008-09-23
申请人： Debra L. Beran , Mark P. Mack , Anil W. Saraf
发明人： Debra L. Beran , Mark P. Mack , Anil W. Saraf
IPC分类号： C08L23/30 , C08L23/26
CPC分类号： C08F8/00 , C08F2810/10 , C08F110/02 , C08F2500/09
摘要： A method of modifying a tubular low density polyethylene (LDPE) is disclosed. In the method ethylene is polymerized with a free radical initiator in a high pressure reactor to form an LDPE. The LDPE is then reacted with a free radical initiator to produce a modified polyethylene. The modified polymer has an increased long chain branching index as indicated by the increase in the gel permeation chromatography branching index.
摘要翻译：公开了改性管状低密度聚乙烯（LDPE）的方法。在该方法中，乙烯在高压反应器中与自由基引发剂聚合以形成LDPE。然后将LDPE与自由基引发剂反应以制备改性聚乙烯。改进的聚合物具有增加的长链支化指数，如凝胶渗透色谱分支指数的增加所示。

17. 发明申请

US20090099316A1 Preparation of multimodal polyethylene 有权
公开(公告)号：US20090099316A1
公开(公告)日：2009-04-16
申请号：US12315552
申请日：2008-12-04
申请人： Venki Chandrashekar , Mark P. Mack , Charles H. Gates, JR. , Charles S. Holland , Natalia Nagy , Sandor M. Nagy , Edward S. Vargas , Jean A. Merrick-Mack
发明人： Venki Chandrashekar , Mark P. Mack , Charles H. Gates, JR. , Charles S. Holland , Natalia Nagy , Sandor M. Nagy , Edward S. Vargas , Jean A. Merrick-Mack
IPC分类号： C08L23/06
CPC分类号： C08L23/04 , C08F4/65912 , C08F4/65916 , C08F4/65925 , C08F4/65927 , C08F10/02 , C08F110/02 , C08F210/16 , C08L23/06 , C08L23/0807 , C08F2/001 , C08F4/65904 , C08L23/00 , C08L2666/06 , C08F2500/05 , C08F2500/09 , C08F210/08
摘要： Disclosed is a polyethylene composition. The composition comprises single-site multimodal resin A and single-site multimodal resin B, wherein resin A differs from resin B in molecular weight, in monomeric composition, in density, in long chain branch concentration or distribution, or in combinations thereof. Disclosed is also a method for making the polyethylene composition. The method comprises polymerizing, in the presence of two or more single-site catalysts, ethylene or its mixture with a C3-C10 α-olefin to form a first multimodal resin and continuing the polymerization in the presence of the same catalysts but in a different hydrogen concentration, in a different monomer composition, or at a different temperature to form a second multimodal resin.

18. 发明授权

US07230054B2 Polymer resins with improved environmental stress crack resistance 有权
标题翻译：具有改善的环境应力开裂性的聚合物树脂
公开(公告)号：US07230054B2
公开(公告)日：2007-06-12
申请号：US10880263
申请日：2004-06-29
申请人： Harilaos Mavridis , Sameer D. Mehta , Mark P. Mack , Philip J. Garrison , Michael W. Lynch
发明人： Harilaos Mavridis , Sameer D. Mehta , Mark P. Mack , Philip J. Garrison , Michael W. Lynch
IPC分类号： C08L23/00
CPC分类号： C08F210/16 , C08L23/06 , C08L23/0815 , C08L2205/02 , C08L2205/025 , C08L2666/06 , C08F210/08 , C08F2500/12 , C08F2500/03 , C08F2500/13
摘要： Resins comprising a relatively high-density, low-molecular-weight polyethylene component and a relatively low-density, high-molecular-weight ethylene copolymer component and methods of making the resins are disclosed. The rheological polydispersity of the high-density component exceeds that of either the resin or the low-density component. The resins are valuable for making films, sheets, coatings, pipes, fibers, and molded articles having a favorable balance of good stiffness and excellent environmental stress crack resistance.
摘要翻译：公开了包含相对高密度，低分子量聚乙烯组分和相对低密度，高分子量乙烯共聚物组分的树脂和制备树脂的方法。高密度组分的流变多分散性超过树脂或低密度组分的多分散性。这些树脂对于制造具有良好的刚度和优异的耐环境应力开裂性的良好平衡的膜，片，涂料，管，纤维和模制品是有价值的。

19. 发明授权

US06559251B1 Process for making low-density polyolefins 失效
标题翻译：制备低密度聚烯烃的方法
公开(公告)号：US06559251B1
公开(公告)日：2003-05-06
申请号：US10211085
申请日：2002-08-02
申请人： Shaotian Wang , Clifford C. Lee , Mark P. Mack , Gregory G. Hlatky , Sandor Nagy , Barbara M. Tsuie
发明人： Shaotian Wang , Clifford C. Lee , Mark P. Mack , Gregory G. Hlatky , Sandor Nagy , Barbara M. Tsuie
IPC分类号： C08F464
CPC分类号： C08F210/16 , C08F4/65908 , C08F4/65912 , C08F4/65916 , Y02P20/52 , Y10S526/943 , C08F4/6592 , C08F210/08 , C08F2500/10 , C08F2500/08 , C08F2500/03 , C08F210/14 , C08F2500/01 , C08F2500/17
摘要： A process for making ethylene copolymers is disclosed. Ethylene copolymerizes with an &agr;-olefin in the presence of a catalyst system comprising an activator and a silica-supported, bridged indenoindolyl metal complex having “open architecture.” The supported complex incorporates comonomers with exceptional efficiency, and the process gives ethylene copolymers having high molecular weights (Mw>100K) and very low densities (
摘要翻译：公开了制备乙烯共聚物的方法。在包含活化剂和具有“开放结构”的二氧化硅负载的桥连茚并吲哚基金属络合物的催化剂体系的存在下，乙烯与α-烯烃共聚。支持的络合物以非常有效的方式引入共聚单体，该方法得到具有高分子量（Mw> 100K）和非常低密度（<0.910g / cm 3）的乙烯共聚物。还描述了包括连接吲哚吲哚基骨架的吲哚基氮的开放式结构催化剂。

20. 发明授权

US4886875A End-capping of polyarylate carboxyl acid ends by use of aromatic carbonates 失效
标题翻译：通过使用芳族碳酸酯封端聚芳酯羧酸末端
公开(公告)号：US4886875A
公开(公告)日：1989-12-12
申请号：US281036
申请日：1988-12-07
申请人： Frank P. Gay , Francis M. Logullo , Robert R. Luise , Mark P. Mack
发明人： Frank P. Gay , Francis M. Logullo , Robert R. Luise , Mark P. Mack
IPC分类号： C08G63/78 , C08G63/20 , C08G63/64 , C08G64/18
CPC分类号： C08G64/18 , C08G63/20
摘要： A process for improving the stability of a polyarylate resin by reducing the terminal carboxyl acid group concentration of the polyarylate resin, the process being comprised of melting a mixture of the polyarylate resin and an aromatic carbonate capping agent and reacting the mixture under heat and, if necessary, vacuum until the concentration of the terminal carboxyl acid groups is reduced to less than that of the polyarylate resin prior to end-capping. The process also results in a polyarylate resin with a decreased flammability rating when the aromatic carbonate capping agent is bromine substituted.

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