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11. 发明授权

US5231190A Squarylium compounds, and processes and intermediates for the synthesis of these compounds 失效
标题翻译： SQUARYLIUM化合物，以及合成这些化合物的方法和中间体
公开(公告)号：US5231190A
公开(公告)日：1993-07-27
申请号：US696222
申请日：1991-05-06
申请人： Donald A. McGowan , Paulina P. Garcia , John W. Lee , Thomas K. Spencer , Stephen J. Telfer , Michael J. Zuraw
发明人： Donald A. McGowan , Paulina P. Garcia , John W. Lee , Thomas K. Spencer , Stephen J. Telfer , Michael J. Zuraw
IPC分类号： C07D309/32 , C07D309/34 , C07D335/02 , C07D335/06 , C07D345/00 , C07D421/10 , C09B23/01 , C09B57/00 , G03G5/06 , G11B7/246 , G11B7/247
CPC分类号： G11B7/247 , C07D309/34 , C07D335/02 , C07D335/06 , C07D345/00 , C09B23/0025 , C09B23/0066 , C09B57/007 , G03G5/0611 , G11B7/246
摘要： Squarylium compounds of the formula: ##STR1## wherein Q.sup.1 and Q.sup.2 are each independently a pyrylium, thiopyrylium, selenopyrylium, benzpyrylium, benzthiopyrylium or benzselenopyrylium nucleus, and R.sup.1 and R.sup.2 are each independently an aliphatic or cycloaliphatic group, can be prepared by reacting a squaric acid derivative of the formula: ##STR2## with a compound of the formula Q.sup.2 CH.sub.2 R.sup.2 in the presence of a base. The derivatives of Formula II may be prepared by condensing a 2,3,4,4-tetrahalocyclobut-2-en-1-one with a compound of the formula Q.sup.1 CH.sub.2 R.sup.1 in the presence of a base to produce a compound of the formula: ##STR3## wherein Q.sup.1 and R.sup.1 are as defined above, and X represents chlorine or bromine, and hydrolyzing the compound of Formula III. Alternatively, the derivatives of Formula II may be prepared by reacting a diester, monoacid chloride monoester or diacid chloride of squaric acid with a compound of the formula Q.sup.1 CH.sub.2 R.sup.1 in the presence of a base, followed by hydrolysis of the resultant monoacid chloride or monoester derivative of the compound of Formula II to the parent compound.

12. 发明授权

US06482950B1 Squarylium compounds, and processes and intermediates for the synthesis of these compounds 失效
标题翻译：方酸化合物，以及用于合成这些化合物的方法和中间体
公开(公告)号：US06482950B1
公开(公告)日：2002-11-19
申请号：US08479077
申请日：1995-06-06
申请人： Paulina P. Garcia , John W. Lee , John L. Marshall , Donald A. McGowan , Anthony J. Puttick , Thomas K. Spencer , Stephen G. Stroud , Stephen J. Telfer , Michael J. Zuraw
发明人： Paulina P. Garcia , John W. Lee , John L. Marshall , Donald A. McGowan , Anthony J. Puttick , Thomas K. Spencer , Stephen G. Stroud , Stephen J. Telfer , Michael J. Zuraw
IPC分类号： C07D47100
CPC分类号： G11B7/247 , C07D309/34 , C07D335/02 , C07D335/06 , C07D345/00 , C09B23/0025 , C09B23/0066 , C09B57/007 , G03G5/0611 , G11B7/246
摘要： Squarylium compounds of the formula: wherein Q1 and Q2 are each independently a pyrylium, thiopyrylium, selenopyrylium, benzpyrylium, benzthiopyrylium or benzselenopyrylium nucleus, and R1 and R2 are each independently an aliphatic or cycloaliphatic group, can be prepared by reacting a squaric acid derivative of the formula: with a compound of the formula Q2CH2R2 in the presence of a base. The derivatives of Formula II may be prepared by condensing a 2,3,4,4-tetrahalocyclobut-2-en-1-one with a compound of the formula Q1CH2R1 in the presence of a base to produce a compound of the formula: wherein Q1 and R1 are as defined above, and X represents chlorine or bromine, and hydrolyzing the compound of Formula III. Alternatively, the derivatives of Formula II may be prepared by reacting a diester, monoacid chloride monoester or diacid chloride of squaric acid with a compound of the formula Q1CH2R1 in the presence of a base, followed by hydrolysis of the resultant monoacid chloride or monoester derivative of the compound of Formula II to the parent compound.
摘要翻译：下式的方酸化合物：其中Q1和Q2各自独立地是吡喃鎓，硫代吡喃鎓，硒代吡喃鎓，苯并吡喃鎓，苯并硫代吡喃鎓或苯并硒吡喃鎓核，R1和R2各自独立地是脂族或脂环族基团，可以通过将式中：在碱的存在下使用式Q2CH2R2的化合物。式II的衍生物可以通过在碱的存在下将2,3,4,4-四卤代环丁-2-烯-1-酮与式Q1CH2R1的化合物缩合来制备下式的化合物：其中 Q1和R1如上定义，X表示氯或溴，并水解式III化合物。或者，式II的衍生物可以通过在碱的存在下使方酸的二酯，单酰氯单酯或二酸氯化物与式Q1CH2R1的化合物反应制备，然后水解所得的单酰氯或单酯衍生物式II化合物与母体化合物。

13. 发明授权

US5977351A Benzpyrylium squarylium and croconylium dyes, and processes for their preparation and use 失效
公开(公告)号：US5977351A
公开(公告)日：1999-11-02
申请号：US65350
申请日：1993-05-20
申请人： Peter K. Chu , Serajul Haque , Anthony J. Puttick , Socorro M. Ramos , Robert P. Short , Stephen G. Stroud , Stephen J. Telfer , Michael J. Zuraw
发明人： Peter K. Chu , Serajul Haque , Anthony J. Puttick , Socorro M. Ramos , Robert P. Short , Stephen G. Stroud , Stephen J. Telfer , Michael J. Zuraw
IPC分类号： B41M5/26 , B41M5/385 , B41M5/392 , B41M5/40 , B41M5/46 , C09B57/00 , C09B57/02 , G11B7/244 , C07D345/00 , C07D311/04 , C07D335/04
CPC分类号： C09B57/007 , B41M5/465 , C09B57/02 , G11B7/244 , B41M5/26 , B41M5/3854 , B41M5/392
摘要： Dyes comprising an inner salt of a compound of the formula:Q.sup.1 =Z-Q.sup.2wherein:Q.sup.1 is a 4-(benz[b]-4H-pyrylium)methylidene, 4-(benz[b]-4H-thiopyrylium)methylidene or 4-(benz[b]-4H-selenopyrylium)methylidene grouping;Z is a 1,3-(2-hydroxy-4-oxo-2-cyclobutylidene) hydroxide or 1,3-(2-hydroxy-4,5-dioxo-2-cyclopentylidene) hydroxide ring; andQ.sup.2 is a 4-(benz[b]-4H-pyran-4-ylidene)methyl, 4-(benz[b]-4H-thiopyran-4-ylidene)methyl or 4-(benz[b]-4H-selenopyran-4-ylidene)methyl grouping;wherein at least one of the groupings Q.sup.1 and Q.sup.2 carries at its 2-position a substituent in which a non-aromatic carbon atom is bonded directly to the benzpyrylium, benzthiopyrylium or benzselenopyrylium nucleus, subject to the proviso that if this 2-substituent contains an aromatic nucleus, this aromatic nucleus is not conjugated with the benzpyrylium, benzthiopyrylium or benzselenopyrylium nucleus to which it is attached, are useful as visible and near infra-red absorbers, having high extinction coefficients and improved solubility in polymeric media.

14. 发明授权

US5451478A Slide blank, and process for producing a slide therefrom 失效
标题翻译：滑动空白，以及用于从其制造滑块的过程
公开(公告)号：US5451478A
公开(公告)日：1995-09-19
申请号：US226657
申请日：1994-04-12
申请人： Roger A. Boggs , Yves G. Conturie , Edward P. Lindholm , Warren D. Slafer , Stephen J. Telfer , Michael J. Zuraw
发明人： Roger A. Boggs , Yves G. Conturie , Edward P. Lindholm , Warren D. Slafer , Stephen J. Telfer , Michael J. Zuraw
IPC分类号： B41M5/28 , B41M5/30 , B41M5/323 , B41M5/327 , B41M5/34 , B41M5/382 , B41M5/40 , B41M5/46 , G03C1/73 , G03C1/76
CPC分类号： B41M5/38214 , B41M5/323 , B41M5/3275 , B41M5/465
摘要： A slide blank comprises a support at least part of which is essentially transparent; an imageable layer superposed on one face of the support, the imageable layer not being substantially photosensitive but comprising a color-forming composition, which, upon imagewise exposure to actinic radiation, forms a colored material, thereby forming in the imageable layer an image which can be viewed in transmission; and a protective layer superposed on the imageable layer on the opposed side thereof from the support, at least part of the protective layer being essentially transparent; the support, imageable layer and protective layer being secured together to form a slide blank having a thickness of at least about 0.8 mm, and the thickness of the protective layer being such that no part of the imageable layer containing the color-forming composition is more than about 0.2 mm from one external surface of the slide blank. This slide blank can be imaged to produce a ready-mounted slide.
摘要翻译：滑动坯料包括其至少一部分基本上是透明的支撑件; 可成像层叠加在支撑体的一个面上，可成像层基本上不光敏，但包含成色组合物，其在成像曝光于光化辐射之后形成着色材料，从而在可成像层中形成可以在传播中被看待; 以及保护层，其与所述支撑体相对的一侧叠置在所述可成像层上，所述保护层的至少一部分基本上是透明的; 支撑件，可成像层和保护层被固定在一起以形成厚度为至少约0.8mm的滑动坯料，并且保护层的厚度使得不含有成色组合物的可成像层的部分更多比滑动坯料的一个外表面大约0.2mm。该幻灯片可以被成像以产生准备好的幻灯片。

15. 发明授权

US5422230A Slide blank, and process for producing a slide therefrom 失效
标题翻译：滑动空白，以及用于从其制造滑块的过程
公开(公告)号：US5422230A
公开(公告)日：1995-06-06
申请号：US226452
申请日：1994-04-12
申请人： Roger A. Boggs , Warren D. Slafer , Stephen J. Telfer , Michael J. Zuraw
发明人： Roger A. Boggs , Warren D. Slafer , Stephen J. Telfer , Michael J. Zuraw
IPC分类号： B41M5/28 , B41M5/30 , B41M5/323 , B41M5/46 , G03C1/73 , G03C7/00
CPC分类号： B41M5/30
摘要： A slide blank comprises a support; a mask layer having a substantially transparent central portion and a non-transparent peripheral portion surrounding the central portion; and an imageable layer which is not substantially photosensitive but is imageable to form an image which can be viewed in transmission. The support, mask layer and imageable layer are secured together so that the support and the imageable layer extend across essentially the entire transparent central portion of the mask layer, at least the portion of the support adjacent the central portion of the mask layer being substantially transparent. This slide blank can be imaged to produce a ready-mounted slide.
摘要翻译：滑动坯料包括支撑件; 掩模层，其具有基本上透明的中心部分和围绕所述中心部分的不透明周边部分; 以及可成像层，其基本上不是光敏的，但可成像，以形成可在透射中观看的图像。支撑体，掩模层和可成像层被固定在一起，使得支撑体和可成像层在掩模层的基本上整个透明中心部分上延伸，至少邻近掩模层中心部分的支撑部分基本上是透明的。该幻灯片可以被成像以产生准备好的幻灯片。

16. 发明授权

US5236884A Thermal imaging methods and materials 失效
标题翻译：热成像方法与材料
公开(公告)号：US5236884A
公开(公告)日：1993-08-17
申请号：US696151
申请日：1991-05-06
申请人： Roger A. Boggs , Richard L. Cournoyer , Ernest W. Ellis , Sandra E. Russo-Rodriguez , Stephen J. Telfer , David P. Waller , Michael J. Zuraw
发明人： Roger A. Boggs , Richard L. Cournoyer , Ernest W. Ellis , Sandra E. Russo-Rodriguez , Stephen J. Telfer , David P. Waller , Michael J. Zuraw
IPC分类号： B41M5/34 , B41M5/28 , B41M5/30 , B41M5/323 , B41M5/46 , C09B55/00 , C09B57/00 , C09K9/02
CPC分类号： C09B57/002 , B41M5/323 , C09B55/002 , C09B55/009
摘要： Leuco dyes are provided which comprise the coupling product of a N-acyl substituted aromatic amino color developer and a dye-forming coupler moiety substituted at the coupling carbon with a thermally removable leaving group. Thermal imaging systems employing these leuco dyes have the advantage of reduced bubble formation relative to thermal imaging systems employing prior art leuco dyes containing a group which thermally fragments into one or more gases.

17. 发明授权

US08101006B2 Centrifugal atomization for producing zinc powder 有权
标题翻译：用于生产锌粉的离心雾化
公开(公告)号：US08101006B2
公开(公告)日：2012-01-24
申请号：US12148748
申请日：2008-04-22
申请人： Michael J. Zuraw , Peter B. Harris
发明人： Michael J. Zuraw , Peter B. Harris
IPC分类号： B22F9/10
CPC分类号： B22F9/10 , H01M4/42 , H01M4/50 , H01M6/04
摘要： A centrifugal impact atomization process for producing zinc or zinc alloy powder from molten zinc. A stream of molten zinc is injected onto the surface of a spinning disk contained within an atomization chamber. The disk has a cup shaped cavity having an open end, opposing closed end and integral side walls. The disk may have baffles protruding into the open cavity core within the disk. The baffles may have straight or curved side surfaces. The disk is rotated at high speeds between about 10,000 and 15,000 rpm (revolutions per minute). The oxygen content in the chamber is preferably between about 1 and 6 vol %. Zinc powder is produced having more smaller size particles. Zinc alkaline cells utilizing such zinc product as anode active material show improved performance, especially as power source in high discharge services such as digital cameras.
摘要翻译：用于从熔融锌生产锌或锌合金粉末的离心冲击雾化工艺。将熔融锌流注入到雾化室内的旋转盘的表面上。盘具有杯形空腔，其具有开口端，相对的封闭端和整体侧壁。盘可以具有突出到盘内的开口腔芯中的挡板。挡板可以具有直的或弯曲的侧表面。盘以约10,000至15,000rpm（每分钟转数）的高速旋转。室中的氧含量优选为约1至6体积％。生产具有更小尺寸颗粒的锌粉。使用这种锌产品作为阳极活性材料的锌碱性电池显示出改进的性能，特别是作为诸如数码相机的高放电服务中的电源。

18. 发明申请

US20070264572A1 Battery Anodes 审中-公开
标题翻译：电池阳极
公开(公告)号：US20070264572A1
公开(公告)日：2007-11-15
申请号：US11799136
申请日：2007-05-01
申请人： Michael J. Zuraw
发明人： Michael J. Zuraw
IPC分类号： H01M4/42 , C22C18/04
CPC分类号： H01M4/42 , B22F1/0048 , B22F9/10 , C22C18/00 , H01M4/244 , H01M4/48 , H01M4/50 , H01M2004/021 , H01M2004/027
摘要： Batteries, as well as related components and methods, are disclosed.
摘要翻译：公开了电池，以及相关组件和方法。

19. 发明申请

US20070148514A1 Fuel cells 审中-公开
标题翻译：燃料电池
公开(公告)号：US20070148514A1
公开(公告)日：2007-06-28
申请号：US11318374
申请日：2005-12-22
申请人： Zhiping Jiang , Javit A. Drake , Andrew G. Gilicinski , Michael J. Zuraw , Robert Pavlinsky , John Perry Scartozzi , John Walczyk , Anna Maria Bofinger
发明人： Zhiping Jiang , Javit A. Drake , Andrew G. Gilicinski , Michael J. Zuraw , Robert Pavlinsky , John Perry Scartozzi , John Walczyk , Anna Maria Bofinger
IPC分类号： H01M8/10 , H01M2/02
CPC分类号： H01M8/04208 , B60K15/03177 , H01M8/04082 , H01M8/1011 , Y02E60/523
摘要： Fuel cell systems, as well as related components and methods, are disclosed.
摘要翻译：公开了燃料电池系统以及相关组件和方法。

20. 发明授权

US5405976A Benzpyrylium squarylium and croconylium dyes, and processes for their preparation and use 失效
标题翻译： Benzyrylium squarylium和croconylium dye，及其制备和使用的方法
公开(公告)号：US5405976A
公开(公告)日：1995-04-11
申请号：US126427
申请日：1993-09-24
申请人： Stephen J. Telfer , Robert P. Short , Stephen G. Stroud , Anthony J. Puttick , Socorro; M. Ramos , Michael J. Zuraw
发明人： Stephen J. Telfer , Robert P. Short , Stephen G. Stroud , Anthony J. Puttick , Socorro; M. Ramos , Michael J. Zuraw
IPC分类号： B41M5/26 , B41M5/385 , B41M5/392 , B41M5/40 , B41M5/46 , C09B57/00 , C09B57/02 , G11B7/244 , C07D311/58 , C07D335/06 , C07D405/10
CPC分类号： B41M5/465 , C09B57/007 , C09B57/02 , G11B7/244 , B41M5/26 , B41M5/3854 , B41M5/392 , Y10S430/145
摘要： Dyes comprising an inner salt of a compound of the formula:Q.sup.1 =Z-Q.sup.2wherein:Q.sup.1 is a 4-(benz[b]-4H-pyrylium)methylidene, 4-(benz[b]-4H-thiopyrylium)methylidene or 4-(benz[b]-4H-selenopyrylium)methylidene grouping;Z is a 1,3-(2-hydroxy-4-oxo-2-cyclobutylidene) hydroxide or 1,3-(2-hydroxy-4,5-dioxo-2-cyclopentylidene) hydroxide ring; andQ.sup.2 is a 4-(benz[b]-4H-pyran-4-ylidene)methyl, 4-(benz[b]-4H-thiopyran-4-ylidene)methyl or 4-(benz[b]-4H-selenopyran-4-ylidene)methyl grouping;wherein at least one of the groupings Q.sup.1 and Q.sup.2 carries at its 2-position a substituent in which a non-aromatic carbon atom is bonded directly to the benzpyrylium, benzthiopyrylium or benzselenopyrylium nucleus, subject to the proviso that if this 2-substituent contains an aromatic nucleus, this aromatic nucleus is not conjugated with the benzpyrylium, benzthiopyrylium or benzselenopyrylium nucleus to which it is attached, are useful as visible and near infra-red absorbers, having high extinction coefficients and improved solubility in polymeric media.
摘要翻译：染料，其包含下式化合物的内盐：Q1 = Z-Q2其中：Q1是4-（苯并[b] -4H-吡喃鎓）亚甲基，4-（苯并[b] -4H-硫代吡啶鎓）亚甲基或 4-（苯并[b] -4H-硒代吡咯鎓）亚甲基; Z是1,3-（2-羟基-4-氧代-2-环亚丁基）氢氧化物或1,3-（2-羟基-4,5-二氧代-2-亚环戊基）氢氧化物环; 并且Q2是4-（苯并[b] -4H-吡喃-4-亚基）甲基，4-（苯并[b] -4H-噻喃-4-亚基）甲基或4-（苯并[b] 硒代吡喃-4-亚基）甲基; 其中分组Q1和Q2中的至少一个在其2-位上带有非芳族碳原子直接键合到苯并吡喃鎓，苯并硫代吡喃鎓或苯并硒吡喃鎓核的取代基，条件是如果该2-取代基含有芳香核，该芳香核不与其连接的苯并吡喃鎓，苯并硫代吡喃鎓或苯并硒吡喃鎓核共轭，可用作可见光和近红外吸收剂，具有高消光系数和在聚合物介质中改善的溶解性。

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