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11. 发明申请

US20110151333A1 LITHIUM ION BATTERY 有权
公开(公告)号：US20110151333A1
公开(公告)日：2011-06-23
申请号：US12642313
申请日：2009-12-18
申请人： Ion C. Halalay , Stephen J. Harris , Timothy J. Fuller
发明人： Ion C. Halalay , Stephen J. Harris , Timothy J. Fuller
IPC分类号： H01M2/16 , H01M6/00
CPC分类号： H01M4/628 , H01M2/162 , H01M2/1653 , H01M4/622 , H01M10/0525 , H01M2220/30 , H01M2300/0025 , Y02E60/122 , Y02P70/54 , Y10T29/49108
摘要： In a lithium ion battery, one or more chelating agents may be attached to a microporous polymer separator for placement between a negative electrode and a positive electrode or to a polymer binder material used to construct the negative electrode, the positive electrode, or both. The chelating agents may comprise, for example, at least one of a crown ether, a podand, a lariat ether, a calixarene, a calixcrown, or mixtures thereof. The chelating agents can help improve the useful life of the lithium ion battery by complexing with unwanted metal cations that may become present in the battery's electrolyte solution while, at the same time, not significantly interfering with the movement of lithium ions between the negative and positive electrodes.

12. 发明授权

US08785054B2 Lithium ion battery 有权
标题翻译：锂离子电池
公开(公告)号：US08785054B2
公开(公告)日：2014-07-22
申请号：US12642313
申请日：2009-12-18
申请人： Ion C. Halalay , Stephen J. Harris , Timothy J. Fuller
发明人： Ion C. Halalay , Stephen J. Harris , Timothy J. Fuller
IPC分类号： H01M2/16 , H01M4/62
CPC分类号： H01M4/628 , H01M2/162 , H01M2/1653 , H01M4/622 , H01M10/0525 , H01M2220/30 , H01M2300/0025 , Y02E60/122 , Y02P70/54 , Y10T29/49108
摘要： In a lithium ion battery, one or more chelating agents may be attached to a microporous polymer separator for placement between a negative electrode and a positive electrode or to a polymer binder material used to construct the negative electrode, the positive electrode, or both. The chelating agents may comprise, for example, at least one of a crown ether, a podand, a lariat ether, a calixarene, a calixcrown, or mixtures thereof. The chelating agents can help improve the useful life of the lithium ion battery by complexing with unwanted metal cations that may become present in the battery's electrolyte solution while, at the same time, not significantly interfering with the movement of lithium ions between the negative and positive electrodes.
摘要翻译：在锂离子电池中，可以将一种或多种螯合剂连接到微孔聚合物隔板上以放置在负极和正极之间，或者连接到用于构造负极，正极或两者的聚合物粘合剂材料。螯合剂可以包括例如冠醚，podand，laric ether，杯芳烃，杯形糖或其混合物中的至少一种。螯合剂可以通过与可能存在于电池电解质溶液中的不需要的金属阳离子络合而有助于提高锂离子电池的使用寿命，同时不会显着干扰负离子和正极之间的锂离子的运动电极。

13. 发明授权

US08802301B2 Lithium ion battery electrolyte including a vitreous eutectic mixture 有权
标题翻译：锂离子电池电解质包括玻璃态共晶混合物
公开(公告)号：US08802301B2
公开(公告)日：2014-08-12
申请号：US12902120
申请日：2010-10-11
申请人： Ion C. Halalay , Damon R. Frisch , Olt E. Geiculescu , Darryl D Desmarteau , Stephen E Creager , Changqing Lu
发明人： Ion C. Halalay , Damon R. Frisch , Olt E. Geiculescu , Darryl D Desmarteau , Stephen E Creager , Changqing Lu
IPC分类号： H01M10/0568 , H01M10/0569
CPC分类号： H01M10/0568 , H01M10/0525 , H01M10/0569 , H01M2300/0045
摘要： An electrolyte for a lithium ion battery includes a vitreous eutectic mixture represented by the formula AxBy, where A is a salt chosen from a lithium fluoroalkylsulfonimide or a lithium fluoroarylsulfonimide, B is a solvent chosen from an alkylsulfonamide or an arylsulfonamide, and x and y are the mole fractions of A and B, respectively.
摘要翻译：用于锂离子电池的电解质包括由式AxBy表示的玻璃态共晶混合物，其中A是选自氟代烷基磺酰亚胺锂或氟化芳基磺酰亚胺的盐，B是选自烷基磺酰胺或芳基磺酰胺的溶剂，x和y是 A和B的摩尔分数。

14. 发明授权

US08524415B2 Carbon-titanium oxide electrocatalyst supports for oxygen reduction in PEM fuel cells 有权
标题翻译：碳氧化钛电催化剂载体用于PEM燃料电池中的氧还原
公开(公告)号：US08524415B2
公开(公告)日：2013-09-03
申请号：US12897472
申请日：2010-10-04
申请人： Mei Cai , Suresh K. Donthu , Martin S. Ruthkosky , Ion C. Halalay
发明人： Mei Cai , Suresh K. Donthu , Martin S. Ruthkosky , Ion C. Halalay
IPC分类号： H01M8/10 , H01M4/38 , H01M4/02 , H01M4/88 , B01J23/00
CPC分类号： H01M8/0243 , H01M4/9075 , H01M4/9083 , H01M8/0234 , H01M2008/1095 , Y02P70/56
摘要： A high surface area support material is formed of an intimate mixture of carbon clusters and titanium oxide clusters. A catalytic metal, such as platinum, is deposited on the support particles and the catalyzed material used as an electrocatalyst in an electrochemical cell such as a PEM fuel cell. The composite material is prepared by thermal decomposition and oxidation of an intimate mixture of a precursor carbon polymer, a titanium alkoxide and a surfactant that serves as a molecular template for the mixed precursors.
摘要翻译：高表面积的支撑材料由碳簇和氧化钛簇的紧密混合物形成。在诸如PEM燃料电池的电化学电池中的载体颗粒和用作电催化剂的催化材料上沉积催化金属如铂。复合材料通过前体碳聚合物，钛醇盐和用作混合前体的分子模板的表面活性剂的紧密混合物的热分解和氧化来制备。

15. 发明授权

US07940060B2 Method for measuring the amount of air in a fluid 有权
标题翻译：测量流体中空气量的方法
公开(公告)号：US07940060B2
公开(公告)日：2011-05-10
申请号：US11682345
申请日：2007-03-06
申请人： Ion C. Halalay , Eric W. Schneider
发明人： Ion C. Halalay , Eric W. Schneider
IPC分类号： G01R27/08
CPC分类号： G01N33/2888 , G01N27/06 , G01N27/221
摘要： One embodiment of the invention includes a method comprising measuring the level of a fluid in a system in a vehicle comprising measuring an electrical property of the fluid indicative of the amount of air in the fluid and comparing the measured electrical property to a reference. The measured electrical property may include at least one of electrical resistivity or electrical permittivity. Another embodiment of the invention includes a method comprising measuring an electrical property of a fluid, measuring an electrical property of an air-free fluid sample, and determining a volume fraction of air in the fluid using the electrical property of the fluid and the electrical property of the air-free fluid sample, wherein the electrical property comprises at least one of electrical resistivity or electrical permittivity. In some embodiments an indication can be provided when the slope of the electrical property versus time changes.
摘要翻译：本发明的一个实施例包括一种方法，其包括测量车辆系统中的流体的水平，包括测量表示流体中的空气量的流体的电特性，并将测量的电特性与参考值进行比较。测量的电性能可以包括电阻率或电介电常数中的至少一个。本发明的另一个实施例包括一种方法，其包括测量流体的电特性，测量无空气流体样品的电性能，以及使用流体的电性质和电气性质确定流体中空气的体积分数的空气流体样品，其中电性质包括电阻率或介电常数中的至少一种。在一些实施例中，当电特性对时间的斜率改变时可以提供指示。

16. 发明授权

US07465333B1 Cavitation process for products from precursor halides 有权
标题翻译：前体卤化物产品的气蚀过程
公开(公告)号：US07465333B1
公开(公告)日：2008-12-16
申请号：US11465180
申请日：2006-08-17
申请人： Ion C. Halalay , Michael P. Balogh , Michael K. Carpenter
发明人： Ion C. Halalay , Michael P. Balogh , Michael K. Carpenter
IPC分类号： B22F9/24 , B22F9/30 , B01J19/08 , B01J19/10 , C22B34/10 , C22B34/12 , B01D47/02 , C01G23/02 , B06B1/20
CPC分类号： B22F9/24 , Y10S423/12
摘要： A precursor halide compound is reduced to a predetermined product at substantially ambient conditions. The halide is added to an anhydrous liquid reaction medium containing one or more alkali metals or alkaline earth metals as reductants. The metal reductants are dispersed as very small globules in the liquid by cavitation of the liquid, such as by application of high intensity ultrasonic vibrations or high-shear mixing to the reaction vessel. Continued cavitation of the liquid medium affects low temperature reduction of the precursor halide(s) to produce a metal, metal alloy, metal compound, ceramic material, metal matrix-ceramic composite material, or the like. The practice may be applied, for example, to titanium tetrachloride, alone or with other chlorides, to produce titanium metal, titanium alloys (for example Ti-6Al-4V), and titanium compounds (TiSi2).
摘要翻译：在基本环境条件下将前体卤化物化合物还原成预定的产物。将卤化物加入到含有一种或多种碱金属或碱土金属作为还原剂的无水液体反应介质中。金属还原剂通过液体的空化作为非常小的小球分散在液体中，例如通过对反应容器施加高强度超声振动或高剪切混合。液体介质的持续气穴影响前体卤化物的低温还原，以产生金属，金属合金，金属化合物，陶瓷材料，金属基体陶瓷复合材料等。该实践可以例如单独或与其它氯化物一起应用于四氯化钛，以生产钛金属，钛合金（例如Ti-6Al-4V）和钛化合物（TiSi 2）。

17. 发明申请

US20080271569A1 CAVITATION PROCESS FOR TITANIUM PRODUCTS FROM PRECURSOR HALIDES 有权
标题翻译：来自前身的贵金属制品的加工工艺
公开(公告)号：US20080271569A1
公开(公告)日：2008-11-06
申请号：US11465174
申请日：2006-08-17
申请人： Ion C. Halalay , Michael P. Balogh
发明人： Ion C. Halalay , Michael P. Balogh
IPC分类号： B22F9/24
CPC分类号： B22F9/24 , Y10S423/12
摘要： A titanium halide and, optionally, other precursor halides compound are reduced to a predetermined titanium product, suitably at or near ambient conditions. Titanium tetrachloride, for example, is added to an anhydrous liquid reaction medium containing one or more alkali metals or alkaline earth metals as reductants. The metal reductants are dispersed as very small globules in the liquid by cavitation of the liquid reaction medium, such as by application of high intensity ultrasonic vibrations or high-shear mixing to the reaction vessel. Continued cavitation of the liquid medium affects relatively low temperature reduction of the precursor halide(s) to produce a titanium-containing product such as titanium metal, a titanium alloy or compound, or a titanium matrix-ceramic composite material, or the like.
摘要翻译：卤化钛和任选的其它前体卤化物化合物在适合于或接近环境条件下还原成预定的钛产品。例如，将四氯化钛加入到含有一种或多种碱金属或碱土金属作为还原剂的无水液体反应介质中。金属还原剂通过液体反应介质的空化作为非常小的小球分散在液体中，例如通过对反应容器施加高强度超声振动或高剪切混合。液体介质的持续气穴影响前体卤化物的相对低的温度降低以产生含钛产物如钛金属，钛合金或化合物，或钛基陶瓷复合材料等。

18. 发明授权

US07416579B2 Preparing nanosize platinum-titanium alloys 失效
标题翻译：制备纳米级铂钛合金
公开(公告)号：US07416579B2
公开(公告)日：2008-08-26
申请号：US11177840
申请日：2005-07-08
申请人： Ion C. Halalay , Michael Kevin Carpenter
发明人： Ion C. Halalay , Michael Kevin Carpenter
IPC分类号： B22F9/24 , B22F9/26 , B22F9/02 , B01J37/34 , B01D47/02 , B01J13/00
CPC分类号： B22F9/26 , B22F2998/00 , B22F2999/00 , Y10S977/775 , B22F1/0018 , B22F2201/013 , B22F2201/10 , B22F2202/01
摘要： Nanometer sized particles containing titanium and platinum are prepared by a sonochemical process. Compounds of the metals are dissolved, suspended, or diluted in a low vapor pressure liquid medium, preferably at a sub-ambient temperature. A reducing gas is bubbled through the liquid as it is subjected to cavitation to affect the reductive decomposition of the metal compounds. Titanium and platinum are co-precipitated in very small particles.
摘要翻译：通过声化学方法制备含钛和铂的纳米尺寸颗粒。金属的化合物在低蒸气压液体介质中溶解，悬浮或稀释，优选在亚环境温度下。当气体经受空化以还原分解金属化合物时，还原气体通过液体鼓泡。钛和铂在非常小的颗粒中共沉淀。

19. 发明授权

US07381240B2 Platinum particles with varying morphology 有权
标题翻译：具有不同形态的铂颗粒
公开(公告)号：US07381240B2
公开(公告)日：2008-06-03
申请号：US11560471
申请日：2006-11-16
申请人： Michael K. Carpenter , Ion C. Halalay
发明人： Michael K. Carpenter , Ion C. Halalay
IPC分类号： B22F9/20 , B22F9/24 , B22F9/02 , B01J37/34 , C22C5/04 , B01J13/00
CPC分类号： B22F1/0018 , B22F1/0048 , B22F9/26 , B22F2999/00 , B82Y30/00 , Y10S977/777 , Y10S977/948 , B22F2201/013 , B22F2201/10 , B22F2202/01
摘要： Nanometer to micrometer sized particles containing platinum and having selected morphologies are prepared by a sonochemical process. A compound of platinum is dissolved, suspended, or diluted in a suitable liquid medium at a predetermined concentration and the liquid is maintained at a predetermined temperature from sub-ambient temperatures to above ambient temperatures. A reducing gas is bubbled through the liquid as it is subjected to cavitation at a controlled power to affect the reductive decomposition of the platinum compound. The morphology of the precipitated platinum particles can be varied widely by varying the described concentration, temperature and power parameters.
摘要翻译：通过声化学方法制备纳米至微米级的含有铂并具有选定形态的颗粒。以预定浓度将铂化合物溶解，悬浮或稀释在合适的液体介质中，并将液体保持在从低于环境温度至高于环境温度的预定温度。当还原气体以受控的功率进行气蚀以使铂化合物还原分解时，还原气体被鼓泡通过液体。通过改变所述的浓度，温度和功率参数，可以广泛地改变沉淀的铂颗粒的形态。

20. 发明授权

US09095904B2 Titanium metal powder produced from titanium tetrachloride using an ionic liquid and high-shear mixing 有权
标题翻译：使用离子液体和高剪切混合从四氯化钛生产的钛金属粉末
公开(公告)号：US09095904B2
公开(公告)日：2015-08-04
申请号：US13611017
申请日：2012-09-12
申请人： Michael P. Balogh , Ion C. Halalay
发明人： Michael P. Balogh , Ion C. Halalay
IPC分类号： C22B34/12 , B22F9/24
CPC分类号： B22F9/24 , B22F2009/245 , C22B34/1272
摘要： Titanium tetrahalide (preferably titanium tetrachloride) is reduced to titanium metal particles by reaction with an alkali metal dispersed in a non-aqueous, organic ionic liquid. The dispersion is enhanced using high-shear mixing. By-product alkali metal chloride salt(s) is dissolved in the ionic liquid. Precipitated titanium metal powder is readily separated from the ionic liquid solution as a product. And the separated solution may be subjected to electrolysis to recover chlorine gas, electrodeposited alkali metal, and the ionic liquid. Other metal halides may be added with the titanium halide to form titanium-based alloys or other titanium based products.
摘要翻译：四卤化钛（优选四氯化钛）通过与分散在非水有机离子液体中的碱金属反应而还原成钛金属颗粒。使用高剪切混合增强了分散体。副产物碱金属氯化物盐溶解在离子液体中。析出的钛金属粉末作为产品容易从离子液体溶液中分离出来。并且分离的溶液可以经受电解以回收氯气，电沉积的碱金属和离子液体。其他金属卤化物可与钛卤化物一起加入以形成钛基合金或其它钛基产品。

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