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11. 发明申请

US20070119341A1 Azo compound, aqueous dye solutions containing the same, inks and use thereof 有权
标题翻译：偶氮化合物，含有它们的染料溶液，油墨及其用途
公开(公告)号：US20070119341A1
公开(公告)日：2007-05-31
申请号：US10572334
申请日：2004-09-29
申请人： Hirokazu Kitayama , Yasuo Shirasaki , Takahiko Matsui , Hiroaki Ohno
发明人： Hirokazu Kitayama , Yasuo Shirasaki , Takahiko Matsui , Hiroaki Ohno
IPC分类号： C09D11/00 , C09D11/02 , C07D403/02
CPC分类号： C09B56/04 , C07D249/06 , C09B43/06 , C09B56/08 , C09B67/0073 , C09D11/328
摘要： An azo compound which is reduced in the copper ion content and exhibits hue and clarity suitable for ink-jet recording and which can give records having excellent light fastness, water resistance, and moisture proofness, and such ozone resistance as to control the fading and the discoloration; and water-base yellow inks containing the same. In particular, the azo compound represented by the formula (12) having a content of impurity copper ions of 100 ppm or below or salts thereof; and inks containing the same.
摘要翻译：一种偶氮化合物，其铜离子含量降低并且具有适合于喷墨记录的色调和透明度，并且可以给出具有优异的耐光性，耐水性和防潮性的记录，以及这样的耐臭氧性，以控制褪色和变色; 和含有其的水性黄色油墨。特别地，由式（12）表示的杂质铜离子含量为100ppm以下的偶氮化合物或其盐; 和含有它们的油墨。

12. 发明申请

US20080193660A1 Azo Compound, Ink Composition and Colored Article 有权
标题翻译：偶氮化合物，油墨组合物和有色物品
公开(公告)号：US20080193660A1
公开(公告)日：2008-08-14
申请号：US11666673
申请日：2005-11-10
申请人： Takahiko Matsui , Hiroaki Ohno , Yasuo Shirasaki
发明人： Takahiko Matsui , Hiroaki Ohno , Yasuo Shirasaki
IPC分类号： B05D1/26 , C09B31/00
CPC分类号： C09D11/16 , C09B33/26 , C09D11/328 , D06P5/30
摘要： [Problems] A compound of a black ink which has such excellent fastnesses of a recorded article as light fastness, ozone gas fastness and moisture fastness, excellent solubility, and storage stability as a recording liquid, when used for inkjet recording and writing tools, and an ink composition comprising the same are provided. [Method for solving the problems] An azo compound represented by the following Formula (1) or a salt thereof, and an ink composition comprising the same (wherein, each of R1, R2, R5, R6 and R7 independently represents a hydrogen atom, a carboxyl group, a sulfo group and the like, each of R3 and R4 independently represents a hydrogen atom, a sulfo group, a nitro group, a (C1 to C4) alkyl group (which may be substituted by a hydroxyl group or a (C1 to C4) alkoxy group), a (C1 to C4) alkoxy group (which may be substituted by a hydroxyl group, a (C1 to C4) alkoxy group, a sulfo group or a carboxyl group) and the like, and n represents 0 or 1, respectively).
摘要翻译： [问题]当用于喷墨记录和书写工具时，作为耐光性，耐臭氧气体牢度和耐湿牢度，优异的溶解度和作为记录液体的储存稳定性的记录物品具有如此优良的牢度的黑色油墨的化合物，以及提供包含该油墨组合物的油墨组合物。 [解决问题的方法]由下式（1）表示的偶氮化合物或其盐，以及含有该偶氮化合物的油墨组合物（其中，R 1，R 2， R 5，R 6，R 7和R 7独立地表示氢原子，羧基，磺基等，R 3和R 4各自独立地表示氢原子，磺基，硝基，（C 1〜C 4）烷基（可以被羟基或（C1-C4）烷氧基），（C1-C4）烷氧基（其可以被羟基，（C1-C4）烷氧基，磺基或羧基取代） n，分别表示0或1）。

13. 发明授权

US07427319B2 Azo compound, ink composition, and colored object 有权
标题翻译：偶氮化合物，油墨组合物和有色物体
公开(公告)号：US07427319B2
公开(公告)日：2008-09-23
申请号：US11629314
申请日：2005-06-21
申请人： Takashi Yoneda , Hiroaki Ohno , Yasuo Shirasaki
发明人： Takashi Yoneda , Hiroaki Ohno , Yasuo Shirasaki
IPC分类号： C09D11/00 , C09D11/02 , C09B33/28 , B41J2/01
CPC分类号： C09B43/16 , C09D11/328
摘要： The present invention relates to an azo compound represented by the following formula (1): (wherein, in the formula (1), R1 represents a hydrogen atom; a hydroxyl group; a carboxyl group; a (C1-C4)alkyl group which may be substituted by a hydroxyl group or a (C1-C4)alkoxy group; or the like, and A represents an aliphatic amine residue having a carboxyl group or a sulfo group, respectively;) or a salt thereof; an ink composition containing the same; and an inkjet recording method and a colored object using the same. Said azo compound has a high color value and has a hue between yellow and red or a brown hue. The ink containing said azo compound has satisfactory storage stability, and exhibits, when printed therewith, a stable ejection property even on a thermal type inkjet printer, and gives a print of high quality (superior in light fastness, ozone gas fastness and moisture fastness).
摘要翻译：本发明涉及由下式（1）表示的偶氮化合物：其中，在式（1）中，R 1表示氢原子，羟基，羧基，（C 1 -C 4 -C 4）烷基，其可被羟基或（C 1 -C 4 - 或其盐，A表示分别具有羧基或磺基的脂族胺残基）;或其盐; 含有该油墨组合物的油墨组合物; 以及喷墨记录方法和使用其的着色物体。所述偶氮化合物具有高颜色值，并且具有黄色和红色之间的色调或棕色色调。含有所述偶氮化合物的油墨具有令人满意的储存稳定性，并且即使在热式喷墨打印机上印刷时也显示出稳定的喷射性能，并且提供高质量的印刷（耐光性，耐臭氧气体牢度和耐湿性优异）。

14. 发明申请

US20070257975A1 Azo Compound, Ink Composition, and Colored Object 有权
标题翻译：偶氮化合物，油墨组合物和有色物体
公开(公告)号：US20070257975A1
公开(公告)日：2007-11-08
申请号：US11629314
申请日：2005-06-21
申请人： Takashi Yoneda , Hiroaki Ohno , Yasuo Shirasaki
发明人： Takashi Yoneda , Hiroaki Ohno , Yasuo Shirasaki
IPC分类号： C09D11/00
CPC分类号： C09B43/16 , C09D11/328
摘要： The present invention relates to an azo compound represented by the following formula (1): (wherein, in the formula (1), R1 represents a hydrogen atom; a hydroxyl group; a carboxyl group; a (C1-C4)alkyl group which may be substituted by a hydroxyl group or a (C1-C4)alkoxy group; or the like, and A represents an aliphatic amine residue having a carboxyl group or a sulfo group, respectively;) or a salt thereof; an ink composition containing the same; and an inkjet recording method and a colored object using the same. Said azo compound has a high color value and has a hue between yellow and red or a brown hue. The ink containing said azo compound has satisfactory storage stability, and exhibits, when printed therewith, a stable ejection property even on a thermal type inkjet printer, and gives a print of high quality (superior in light fastness, ozone gas fastness and moisture fastness).
摘要翻译：本发明涉及由下式（1）表示的偶氮化合物：其中，在式（1）中，R 1表示氢原子，羟基，羧基，（C 1 -C 4 -C 4）烷基，其可被羟基或（C 1 -C 4 - 或其盐，A表示分别具有羧基或磺基的脂族胺残基）;或其盐; 含有该油墨组合物的油墨组合物; 以及喷墨记录方法和使用其的着色物体。所述偶氮化合物具有高颜色值，并且具有黄色和红色之间的色调或棕色色调。含有所述偶氮化合物的油墨具有令人满意的储存稳定性，并且即使在热式喷墨打印机上印刷时也显示出稳定的喷射性能，并且提供高质量的印刷（耐光性，耐臭氧气体牢度和耐湿性优异）。

15. 发明授权

US08512462B2 Azo compounds, ink compositions, and colored bodies 有权
标题翻译：偶氮化合物，油墨组合物和着色体
公开(公告)号：US08512462B2
公开(公告)日：2013-08-20
申请号：US13498431
申请日：2010-09-21
申请人： Takahiko Matsui , Takashi Yoshimoto , Hiroaki Ohno , Koji Hirota , Takashi Yoneda , Akira Kawaguchi
发明人： Takahiko Matsui , Takashi Yoshimoto , Hiroaki Ohno , Koji Hirota , Takashi Yoneda , Akira Kawaguchi
IPC分类号： C09D11/02 , C09B33/18 , B41J2/01
CPC分类号： C09B43/16 , C09D11/328 , Y10T428/24802
摘要： Azo compounds represented by general formula (1) or salts thereof are provided as highly water-soluble colorants which have hues of yellow, orange, brown or red, and excellent color development properties and which, when used in various recording processes, particularly in an inkjet recording process, ensure various excellent fastnesses such as light fastness, ozone fastness, and fading balance. Ink compositions containing the colorants are also provided. In general formula (1), R1 to R8 are each independently a hydrogen atom, C1-4 alkyl, C1-4 alkoxy, or the like; and X is C1-8 alkylenediamino, xylylenediamino, or the like.
摘要翻译：提供由通式（1）表示的偶氮化合物或其盐作为具有黄色，橙色，棕色或红色色调的高度水溶性着色剂，并具有优异的显色性，并且当用于各种记录方法时，特别是在喷墨记录工艺，确保耐光性，耐臭氧性和褪色平衡等各种优异的牢度。还提供含有着色剂的油墨组合物。在通式（1）中，R 1至R 8各自独立地为氢原子，C 1-4烷基，C 1-4烷氧基等; X是C 1-8亚烷基二氨基，亚二甲苯基二氨基等。

16. 发明申请

US20120202019A1 AZO COMPOUNDS, INK COMPOSITIONS, AND COLORED BODIES 有权
标题翻译： AZO化合物，墨水组合物和有色体系
公开(公告)号：US20120202019A1
公开(公告)日：2012-08-09
申请号：US13498431
申请日：2010-09-21
申请人： Takahiko Matsui , Takashi Yoshimoto , Hiroaki Ohno , Koji Hirota , Takashi Yoneda , Akira Kawaguchi
发明人： Takahiko Matsui , Takashi Yoshimoto , Hiroaki Ohno , Koji Hirota , Takashi Yoneda , Akira Kawaguchi
IPC分类号： C09B26/06 , B32B3/10 , B41J2/04
CPC分类号： C09B43/16 , C09D11/328 , Y10T428/24802
摘要： Azo compounds represented by general formula (1) or salts thereof are provided as highly water-soluble colorants which have hues of yellow, orange, brown or red, and excellent color development properties and which, when used in various recording processes, particularly in an inkjet recording process, ensure various excellent fastnesses such as light fastness, ozone fastness, and fading balance. Ink compositions containing the colorants are also provided. In general formula (1), R1 to R8 are each independently a hydrogen atom, C1-4 alkyl, C1-4 alkoxy, or the like; and X is C1-8 alkylenediamino, xylylenediamino, or the like.
摘要翻译：提供由通式（1）表示的偶氮化合物或其盐作为具有黄色，橙色，棕色或红色色调的高度水溶性着色剂，并具有优异的显色性，并且当用于各种记录方法时，特别是在喷墨记录工艺，确保耐光性，耐臭氧性和褪色平衡等各种优异的牢度。还提供含有着色剂的油墨组合物。在通式（1）中，R 1至R 8各自独立地为氢原子，C 1-4烷基，C 1-4烷氧基等; X是C 1-8亚烷基二氨基，亚二甲苯基二氨基等。

17. 发明申请

US20110063546A1 Azo Compound And Salt Thereof, And Dye-Containing Polarizing Film Comprising The Compound Or Salt 有权
公开(公告)号：US20110063546A1
公开(公告)日：2011-03-17
申请号：US12948395
申请日：2010-11-17
申请人： Yuichi Sadamitsu , Takuto Nishiguchi , Hiroaki Ohno
发明人： Yuichi Sadamitsu , Takuto Nishiguchi , Hiroaki Ohno
IPC分类号： G02F1/1335 , F21V9/14
CPC分类号： G02B5/305 , C09B56/04 , G02B5/30 , Y10T428/1041
摘要： Disclosed is an azo compound represented by the general formula (1) or a salt thereof: wherein R1 and R2 independently represent a hydrogen atom, a lower alkyl group or a lower alkoxy group; and n represents 1 or 2. Also disclosed are a dye-containing polarizing film and a dye-containing polarizing plate, each of which comprises a polarizing film base material and the azo compound contained in the base material.

18. 发明申请

US20100226008A1 Azo Compound, And Dye-Containing Polarizing Film Comprising The Same 有权
标题翻译：偶氮化合物和含有染料的偏光膜包括它
公开(公告)号：US20100226008A1
公开(公告)日：2010-09-09
申请号：US12739210
申请日：2008-10-30
申请人： Takahiro Higeta , Hiroaki Ohno , Yuichi Sadamitsu
发明人： Takahiro Higeta , Hiroaki Ohno , Yuichi Sadamitsu
IPC分类号： G02B5/30 , C07C245/10
CPC分类号： C07D249/22 , C09B31/072 , C09B31/08 , C09B31/20 , C09B31/22 , C09B31/30 , C09B45/28 , C09B56/08 , G02B5/3025 , G02B5/3033
摘要： Disclosed is an azo compound represented by the formula (1) or (2) or a salt thereof. The azo compound or the salt thereof has an excellent light-polarizing property, and is extremely useful as a dichroic dye for use in a polarizing plate that shows less color leakage in a visible light range or a polarizing plate for a liquid crystal projector comprising the aforementioned polarizing plate. (1) (2) wherein R1 represents a hydrogen atom, a lower alkyl group, a lower alkoxy group, a hydroxyl group, a sulfonate group or a carboxyl group; R2 to R5 independently represent a hydrogen atom, a lower alkyl group, a lower alkoxy group or an acetylamino group; X represents a benzoylamino group which may have a substituent, a phenylamino group which may have a substituent, a phenylazo group which may have a substituent, or a naphthotriazole group which may have a substituent; m represents a numeral number of 1 or 2; and n represents a numeral number of 0 or 1.
摘要翻译：公开了由式（1）或（2）表示的偶氮化合物或其盐。偶氮化合物或其盐具有优异的光偏振性，并且作为用于偏光板的二色性染料非常有用，该偏光板在可见光范围内显示较少的色漏，或用于液晶投影仪的偏振片包括上述偏振片。（1）（2）其中R1表示氢原子，低级烷基，低级烷氧基，羟基，磺酸酯基或羧基; R2至R5独立地表示氢原子，低级烷基，低级烷氧基或乙酰氨基; X表示可以具有取代基的苯甲酰氨基，可以具有取代基的苯基氨基，可以具有取代基的苯偶氮基或可具有取代基的萘并三唑基; m表示1或2的数字; n表示数字0或1。

19. 发明申请

US20060235033A1 Quinoline derivatives and quinazoline derivatives inhibiting autophosphorylation of macrophage colony stimulating factor receptor 失效
标题翻译：喹啉衍生物和喹唑啉衍生物抑制巨噬细胞集落刺激因子受体的自磷酸化
公开(公告)号：US20060235033A1
公开(公告)日：2006-10-19
申请号：US10510961
申请日：2003-05-01
申请人： Kazuo Kubo , Hiroaki Ohno , Toshiyuki Isoe , Tsuyoshi Nishitoba
发明人： Kazuo Kubo , Hiroaki Ohno , Toshiyuki Isoe , Tsuyoshi Nishitoba
IPC分类号： A61K31/517 , A61K31/4704 , C07D239/88
CPC分类号： C07D215/233 , A61K31/47 , A61K31/4709 , A61K31/5377 , C07D417/12
摘要： An objective of the present invention is to provide compounds which have inhibitory activity against autophosphorylation of macrophage colony-stimulating factor receptors. The compounds of the present invention are represented by formula (I) and salt and solvate thereof: wherein X represents CH or N; Z represents O or S; R1, R2, and R3 represent H, optionally substituted alkoxy or the like; R4 represents H; R5, R6, R7, and R8 represent H, halogen, alkyl, alkoxy, trifluoromethyl or the like; R9 and R10 represent H, alkyl or the like; and any one of R11 and R12 represents H with the other representing alkyl and R13 represents an optionally substituted carbocyclic or heterocyclic ring or the like, or R11 represents H and R12 and R13 combine together to form a bicyclic carbocyclic ring.
摘要翻译：本发明的目的是提供对巨噬细胞集落刺激因子受体的自磷酸化具有抑制活性的化合物。本发明的化合物由式（I）表示，其盐和溶剂化物：其中X表示CH或N; Z表示O或S; R 1，R 2，R 3和R 3代表H，任选取代的烷氧基等; R 4表示H; R 5，R 6，R 7和R 8表示H，卤素，烷基，烷氧基，三氟甲基或类似物; R 9和R 10代表H，烷基等; 并且R 11和R 12中的任何一个代表H，另一个代表烷基，R 13表示任选取代的碳环或杂环或或者R 11表示H并且R 12和R 13结合在一起以形成双环碳环。

20. 发明授权

US5202449A Process for purifying 7-dimethylamino-6-demethyl-6-deoxytetracycline 失效
标题翻译：纯化7-二甲氨基-6-去甲基-6-脱氧木糖苷的方法
公开(公告)号：US5202449A
公开(公告)日：1993-04-13
申请号：US758274
申请日：1991-08-27
申请人： Ryoichi Hasegawa , Hiroaki Ohno , Kazuaki Sano , Yoshinori Saito , Hiroaki Nishiyama , Shin'ichi Umeda
发明人： Ryoichi Hasegawa , Hiroaki Ohno , Kazuaki Sano , Yoshinori Saito , Hiroaki Nishiyama , Shin'ichi Umeda
IPC分类号： C07C231/24
CPC分类号： C07C231/24
摘要： A process for purifying 7-dimenthylamino-6-demethyl-6-deoxytetracycline represented by the following formula, ##STR1## which comprises dissolving 7-dimethylamino-6-demethyl-6-deoxytetracycline or its hydrochloride having a lower purity in a mixed solvent of an alcohol and water by using hydrochloric acid and then adjusting the pH of the solution to 3.5 to 4.5 to recrystallize the hydrochloride having a higher purity.
摘要翻译：用于纯化由下式表示的7-二甲基氨基-6-脱甲基-6-脱氧四环素的方法，其包括将具有较低纯度的7-二甲基氨基-6-脱甲基-6-脱氧四环素或其盐酸盐溶于通过使用盐酸，然后将溶液的pH调节至3.5至4.5的醇和水的混合溶剂，使具有较高纯度的盐酸盐重结晶。

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