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11. 发明授权

US4610898A Process for bake coating the surfaces of solid substances 失效
标题翻译：烘烤涂布固体物质表面的工艺
公开(公告)号：US4610898A
公开(公告)日：1986-09-09
申请号：US714043
申请日：1985-03-19
申请人： Dieter Engel , Josef Mondt , Helmut Rinno
发明人： Dieter Engel , Josef Mondt , Helmut Rinno
IPC分类号： B05D7/14 , B05D3/02 , B05D7/24 , B05D7/26 , C09D5/00 , C09D5/02 , C09D201/00
CPC分类号： C09D5/02
摘要： Process for bake coating the surfaces of solid materials by applying the required amount of an aqueous dispersion to the surface to be coated, the dispersion containing, as the binder, a coarse-grained, crosslinkable dispersion copolymer formed from olefinically unsaturated monomers and, if appropriate, further customary lacquer formulation constituents, and the crosslinkable dispersion copolymer being composed of a mixture of at least 2 components which can contain identical or different monomer units, of which at least one component A, which is coarse-grained, has a relatively low average molecular weight, and at least one component B, which can be coarse-grained or fine-grained, has a relatively high average high molecular weight, and the ratio by weight of the components A:B being preferably within the range from 99:1 to 1:1, drying the applied amount of dispersion at a temperature below its minimum film-formation temperature and cross-linking the dried coating by baking at a temperature above the glass transition temperature of the copolymer.
摘要翻译：通过将所需量的水分散体施加到待涂覆的表面上来烘烤涂覆固体材料的表面的方法，该分散体含有作为粘合剂的由烯属不饱和单体形成的粗粒度可交联的分散体共聚物，如果合适，进一步的常规漆配方组分，以及可交联分散共聚物由至少两种可以含有相同或不同单体单元的组分的混合物组成，其中至少一种粗粒度的组分A具有相对较低的平均值分子量和至少一种可以是粗粒度或细粒度的组分B具有相对高的平均高分子量，并且组分A:B的重量比优选在99:1的范围内至1：1，在低于其最低成膜温度的温度下干燥所施加的分散体量，并通过在温度下烘烤使干燥的涂层交联高于共聚物的玻璃化转变温度。

12. 发明授权

US4558092A Aqueous dispersion of sulfo-containing polymers for cement additive applications 失效
标题翻译：用于水泥添加剂应用的含磺基聚合物的水分散体
公开(公告)号：US4558092A
公开(公告)日：1985-12-10
申请号：US498942
申请日：1983-05-27
申请人： Rolf Reinecke , Helmut Rinno , Gerhart Schultz
发明人： Rolf Reinecke , Helmut Rinno , Gerhart Schultz
IPC分类号： C04B24/26 , C04B24/16 , C08F2/22 , C08F20/00 , C08F20/38 , C08F20/52 , C08F220/38 , C08F220/54 , C08F220/58 , C08F246/00 , C08L57/04 , C08L41/00
CPC分类号： C08F220/54 , C04B24/163 , C08F246/00
摘要： An aqueous plastics dispersion is manufactured by copolymerization of several olefinically unsaturated monomers, one of them at least being free from amide and sulfo groups, one of them at least having an amide group and one of them at least having a sulfo group. Copolymerization is carried out in an aqueous medium under usual conditions. The resulting copolymer has a second order transition temperature of 20.degree. C. at most. The plastics dispersion is compatible with cement and serves as additive in cement-containing building materials.
摘要翻译：通过几种烯属不饱和单体的共聚制造水性塑料分散体，其中一种至少不含酰胺基和磺基，其中一个至少具有酰胺基，其中一个至少具有磺基。在通常的条件下，在水性介质中进行共聚。所得共聚物的二阶转变温度最多为20℃。塑料分散体与水泥兼容，并用作含水泥建筑材料中的添加剂。

13. 发明授权

US4421889A Aqueous dispersion paints and process for making the same 失效
标题翻译：水分散体涂料及其制备方法
公开(公告)号：US4421889A
公开(公告)日：1983-12-20
申请号：US493803
申请日：1983-05-13
申请人： Helmut Braun , Helmut Rinno , Werner Stelzel
发明人： Helmut Braun , Helmut Rinno , Werner Stelzel
IPC分类号： C08F212/06 , C08F218/04 , C08F220/14 , C08F220/18 , C08F236/04 , C09D131/02 , C09D133/06 , C09D133/08 , C09D133/12 , C08L35/02 , C09D3/74
CPC分类号： C08F236/04 , C08F212/06 , C08F218/04 , C08F220/14 , C08F220/18 , C09D131/02 , C09D133/062 , C09D133/08 , C09D133/12
摘要： Dispersion paints with high wet adhesion are obtained if, as the binder thereof, an aqueous plastics dispersion is used, the polymer content of which includes monomeric units of an acetoacetic acid ester of an unsaturated alcohol, especially vinyl or allyl alcohol or a diester of a dihydroxy compound in which one acyl radical is acetoacetyl and the other acyl radical is an acrylic or methacrylic radical. The preparation of paints with a low pigment content is especially facilitated by the use of such a dispersion.
摘要翻译：如果作为粘合剂使用水性塑料分散体，其聚合物含量包括不饱和醇的乙酰乙酸酯，特别是乙烯基或烯丙醇或二酯的单体单元，得到具有高湿附着力的分散涂料二羟基化合物，其中一个酰基是乙酰乙酰基，另一个酰基是丙烯酸或甲基丙烯酸基。通过使用这种分散体特别容易地制备颜料含量低的油漆。

14. 发明授权

US4418207A Acetylacetoxyalkyl-allyl ethers 失效
标题翻译：乙酰氧基烷基 - 烯丙基醚
公开(公告)号：US4418207A
公开(公告)日：1983-11-29
申请号：US167004
申请日：1980-07-09
申请人： Helmut Braun , Helmut Rinno , Karl J. Rauterkus
发明人： Helmut Braun , Helmut Rinno , Karl J. Rauterkus
IPC分类号： C07C67/46 , C07C41/03 , C07C43/178 , C07C69/72 , C08F16/00 , C08F16/14 , C08F216/14
CPC分类号： C07C41/03 , C07C41/16 , C07C67/46 , C07C69/72 , C08F216/1416
摘要： Unsaturated acetoacetic acid esters are suitable as comonomers in the polymerization of unsaturated compounds in an aqueous medium. Particularly suitable are acetylacetoxyalkyl-allyl ethers which may be synthesized in an easy manner and correspond to the formulae ##STR1## Said allyl ether derivatives are especially prepared by reacting an allyl alcohol with an epoxide and reacting the resulting hydroxyalkyl-allyl ether with diketene. Both reaction steps are carried out at a temperature of from 0.degree. to 100.degree. C., preferably in the presence of a catalyst. The allyl ether derivatives may be copolymerized especially with vinyl compounds, such as vinyl esters, acrylic acid esters, olefins, vinyl halides and vinyl aromatic hydrocarbons.
摘要翻译：不饱和乙酰乙酸酯在水性介质中不饱和化合物的聚合中适合作为共聚单体。特别合适的是乙酰乙酰氧基烷基 - 烯丙基醚，其可以以容易的方式合成并对应于下式。所述烯丙基醚衍生物特别是通过使烯丙醇与环氧化物反应并使所得羟烷基 - 烯丙基醚与双烯酮。两个反应步骤都在0℃至100℃的温度下进行，优选在催化剂存在下进行。烯丙基醚衍生物可以特别与乙烯基化合物如乙烯基酯，丙烯酸酯，烯烃，乙烯基卤化物和乙烯基芳族烃共聚。

15. 发明授权

US4357455A Process for the preparation of copolymers containing hydroxyl groups and the use thereof 失效
标题翻译：制备含羟基的共聚物的方法及其用途
公开(公告)号：US4357455A
公开(公告)日：1982-11-02
申请号：US265793
申请日：1981-05-21
申请人： Josef Mondt , Helmut Rinno
发明人： Josef Mondt , Helmut Rinno
IPC分类号： C08F2/00 , C08F2/06 , C08F8/00 , C08F8/14 , C08F220/00 , C08F220/04 , C08G18/62 , C08F220/28 , C08F246/00
CPC分类号： C08F8/14
摘要： Process for preparing copolymers soluble in organic solvents and containing hydroxyl groups, by the polymerization and esterification of (a) at least one .alpha.,.beta.-olefinically unsaturated carboxylic acid with (b) at least one olefinically unsaturated copolymerizable monomer and (c) at least one epoxy group-containing compound, at an elevated temperature, in the presence of a polymerization catalyst and, advantageously, a polymerization modifier, characterized in that glycidol, ##STR1## is used as component (c), either alone or in admixture with one or more glycidyl esters with 12 to 19 carbon atoms and derived from saturated fatty acids, the number of epoxy groups being at least equivalent to the number of carboxyl groups, and in mixtures of glycidol with glycidyl esters, the number of equivalents of glycidyl esters is at most twice as great as the number of equivalents of glycidol. The invention further relates to the use of the products obtained for the preparation of air- or oven-drying coating compositions.
摘要翻译：通过（a）至少一种α，β-烯属不饱和羧酸与（b）至少一种烯属不饱和可共聚单体的聚合和酯化制备用于制备可溶于有机溶剂并含有羟基的共聚物的方法，（c）至少一种含环氧基团的化合物，在升高的温度下，在聚合催化剂和有利地，聚合改性剂存在下，其特征在于将缩水甘油作为组分（c），单独使用或与一种或更多的具有12至19个碳原子并且衍生自饱和脂肪酸的缩水甘油酯，环氧基的数目至少等于羧基数，并且在缩水甘油与缩水甘油酯的混合物中，缩水甘油酯的当量数为至少是缩水甘油的当量数的两倍。本发明还涉及获得用于制备空气或烘干涂料组合物的产品的用途。

16. 发明授权

US4193902A Finely particulate plastics dispersions prepared by metering a mixture containing four monomers into an aqueous liquor containing an anionic emulsifier 失效
标题翻译：通过将含有四种单体的混合物计量到含有阴离子乳化剂的含水液体中制备的细颗粒塑料分散体
公开(公告)号：US4193902A
公开(公告)日：1980-03-18
申请号：US866836
申请日：1978-01-04
申请人： Josef Mondt , Karl J. Rauterkus , Helmut Rinno
发明人： Josef Mondt , Karl J. Rauterkus , Helmut Rinno
IPC分类号： C08F212/08 , C08F220/12 , C09D125/14 , C09D133/06 , C09D133/12 , C08L33/08
CPC分类号： C09D133/12 , C08F212/08 , C08F220/12 , C09D125/14 , C09D133/064
摘要： A process is described by which plastics dispersions of high water and saponification resistance are obtained which, due to their small average particle size diameter of 0.01 to 0.06 microns are especially useful as primers for porous substrates. In their penetration characteristics, the present dispersions can be compared with conventional solvent-based primers at comparable solids content. The dispersions are obtained in a one-step polymerization process.
摘要翻译：通过这种方法描述了获得高水和抗皂化性的塑料分散体，由于其平均粒度直径为0.01至0.06微米，特别适用于多孔基材的底漆。在它们的渗透特性中，可以将现有的分散体与常规的溶剂型底漆进行比较，其含量相当。分散体是在一步聚合过程中获得的。

17. 发明授权

US4146516A Thixotropic mixture 失效
标题翻译：触变性混合物
公开(公告)号：US4146516A
公开(公告)日：1979-03-27
申请号：US794270
申请日：1977-05-05
申请人： Helmut Braun , Helmut Rinno , Werner Stelzel
发明人： Helmut Braun , Helmut Rinno , Werner Stelzel
IPC分类号： C08K5/00 , C08J3/02 , C08K3/00 , C08K3/34 , C08L31/00 , C08L31/04 , C08L33/00 , C08L33/02 , C08L33/04 , C09D5/04 , C09D157/00 , C08L1/26
CPC分类号： C09D5/04 , C09D157/00
摘要： Thixotropic mixture consisting of(a) one or several aqueous plastics dispersions containing a copolymer of .alpha.,.beta.-unsaturated compounds,(b) a hydroxyl groups-containing protective colloid,(c) a heavy metal chelate and(d) optionally further usual additives for the preparation of coating compositions,Wherein the copolymer of the aqueous plastics dispersion contains acetoacetate groups in an amount of from 0.35 to 7% by weight, calculated on the total weight of the copolymer.
摘要翻译：由（A）含有α，β-受体化合物的共聚物的一种或几种水性塑料分散体组成的触变混合物，（B）含羟基的保护性胶体，（C）重金属螯合物和（D）选择性的另外的添加剂用于制备涂料组合物，由于水性塑料分散体的共聚物含有按重量计0.35至7％的乙酸酯基团，以共聚物的总重计算。

18. 发明授权

US5679735A Process for the preparation of synthetic resin dispersions 失效
标题翻译：合成树脂分散体的制备方法
公开(公告)号：US5679735A
公开(公告)日：1997-10-21
申请号：US577551
申请日：1995-12-22
申请人： Ulrich Geissler , Helmut Rinno , Heinz-Josef Thevissen
发明人： Ulrich Geissler , Helmut Rinno , Heinz-Josef Thevissen
IPC分类号： C08F2/00 , C08F2/18 , C08F2/20 , C08F2/24 , C08F20/10 , C08F20/12 , C08F220/18 , C09D133/04 , C09D133/06 , C08F5/101 , C08L33/12 , C08L31/04
CPC分类号： C08F20/12
摘要： A process for the preparation of a synthetic resin dispersion stabilized by a protective colloid employing at least one initiator and based on a polymer of (a) a first monomer of at least one ester of acrylic acid or methacrylic acid and an alcohol containing 1 to 22 carbon atoms; and optionally, (b) a second monomer which can be copolymerized with the first monomers. The process comprises introducing at least 50% of the monomers based on the total weight of the monomers, at least 50% of the protective colloid based on the total weight of the protective colloid, and up to 50% of the initiator based on the total weight of the initiator into a reaction vessel to form an aqueous emulsion. Any remaining monomers and protective colloid and at least 50% of the initiator based on the total weight of the initiator are then added to the reaction vessel at a temperature of 30.degree. to 100.degree. C.
摘要翻译：一种制备由保护胶体稳定的合成树脂分散体的方法，所述合成树脂分散体使用至少一种引发剂，并且基于（a）至少一种丙烯酸或甲基丙烯酸酯的第一单体和含有1至22的醇的聚合物碳原子和（b）可与第一单体共聚的第二单体。该方法包括基于单体的总重量引入至少50％的单体，基于保护胶体的总重量，至少50％的保护胶体和基于总量的至多50％的引发剂引发剂的重量加入到反应容器中以形成水乳液。然后将任何剩余的单体和保护胶体和基于引发剂总重量的至少50％的引发剂在30至100℃的温度下加入到反应容器中。

19. 发明授权

US5599597A Concrete molding with improved acid resistance 失效
公开(公告)号：US5599597A
公开(公告)日：1997-02-04
申请号：US358337
申请日：1994-12-16
申请人： Volkmar Berg , Helmut Rinno
发明人： Volkmar Berg , Helmut Rinno
IPC分类号： C04B24/00 , C04B24/16 , C04B24/24 , C04B24/26 , C04B24/42 , C04B28/02 , C04B111/23 , E03F3/04 , E03F11/00 , B32B27/00
CPC分类号： C04B24/003 , C04B24/16 , C04B24/163 , C04B24/243 , C04B24/2641 , C04B24/2664 , C04B24/2676 , C04B24/2688 , C04B24/42 , E03F11/00 , E03F3/04 , C04B2111/00068 , C04B2111/00422 , C04B2111/00586 , C04B2111/0075 , C04B2111/23 , C04B2111/56 , Y10S138/07 , Y10T428/131 , Y10T428/2804 , Y10T428/31855
摘要： Unreinforced or reinforced concrete moldings, for example concrete pipes, with improved corrosion resistance to acids and acidic sewage, improved permeation resistance to inorganic and organic liquids and gases and improved mechanical stability, produced by molding with machines, for example in press molding machines or extrusion machines or concrete pipe pressing machines, and allowing to harden plastic-viscous concrete mixtures of hydraulic inorganic binders, preferably cement, aggregates and water, where, in the preparation of the plastic-viscous concrete mixtures, to the latter has been added in a positive mixer an effective amount of an aqueous plastics dispersion based on anionic and hydrolysis-resistant copolymers of ethylenically unsaturated monomers, the minimum film forming temperature (MFT) of which is above the setting temperature of the concrete mixture, preferably above 23.degree. C. Use of the concrete moldings as concrete precast parts for many various applications, preferably as construction elements in building construction, road building, bridge building, civil engineering, in particular in sewage pipeline construction for underground sewer lines and service water lines.

20. 发明授权

US4921915A Dispersion polymers, biologically active dispersion polymers, a process for their preparation, and their use as diagnostic aids 失效
标题翻译：分散聚合物，生物活性分散聚合物，其制备方法及其用作诊断辅助剂
公开(公告)号：US4921915A
公开(公告)日：1990-05-01
申请号：US70543
申请日：1987-07-07
申请人： Michael Dengler , Wolfgang Kapmeyer , Helmut Rinno
发明人： Michael Dengler , Wolfgang Kapmeyer , Helmut Rinno
IPC分类号： C08F2/22 , C08F2/44 , C08F4/04 , C08F4/34 , C08F253/00 , C08F257/00 , G01N33/543 , G01N33/545
CPC分类号： G01N33/54313 , Y10S435/963 , Y10S436/909
摘要： Dispersion polymers composed of latex, which have on the particle surface a copolymer composed of monomers having terminal acetals of the formula ICH.sub.2 .dbd.CR.sub.1 --CO--NH--(CH.sub.2).sub.n --CH(OR.sub.2) (OR.sub.3) Iin whichn=1-6;R.sub.1 =H or CH.sub.3, andR.sub.2 and R.sub.3 are identical or different withR.sub.2 and R.sub.3 =--(CH.sub.2).sub.m --CH.sub.3 (m=0-7) orR.sub.2 and R.sub.3 =--CXYZ, X, Y and Z being (CH.sub.2).sub.p --CH.sub.3 and p being 1-3, with X, Y, Z being identical or different,and betaine compounds of the formula IICH.sub.2 .dbd.CR--(CH.sub.2).sub.a --(CO--X).sub.b --Z--(CH.sub.2).sub.c --Y IIwithR=H or CH.sub.3,X=--NH or --0,Y=SO.sub.3.sup.- or COO.sup.- ##STR1## a=0-6, b=0-1,c=1-12,are very suitable for the preparation of biologically active latex reagents which have a particularly high detection sensitivity and stability.
摘要翻译：由胶乳组成的分散聚合物，其在颗粒表面上具有由具有式I CH 2 = CR 1 -CO-NH-（CH 2）n -CH（OR 2）（OR 3）I的末端缩醛的单体组成的共聚物，其中n = 1 -6; R1 = H或CH3，R2和R3与R2和R3 = - （CH2）m-CH3（m = 0-7）相同或不同，或R2和R3 = -CYYZ，X，Y和Z为（CH2） p-CH3和p为1-3，X，Y，Z相同或不同，式II CH2 = CR-（CH2）a-（CO-X）bZ-（CH2）cY II的甜菜碱化合物与 R = H或CH 3，X = -NH或-O，Y = SO 3 - 或COO- 或 a = 0-6，b = 0-1，c = 1-12非常适合制备具有特别高检测灵敏度和稳定性的生物活性胶乳试剂。

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