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11. 发明申请

US20060135731A1 Method for the preparation of bis(haloimides) 审中-公开
标题翻译：双（卤代酰亚胺）的制备方法
公开(公告)号：US20060135731A1
公开(公告)日：2006-06-22
申请号：US11232285
申请日：2005-09-21
申请人： James Silva , Farid Khouri
发明人： James Silva , Farid Khouri
IPC分类号： C08G8/02
CPC分类号： C07D209/48 , C08G73/12
摘要： Bis(halophthalimides) are prepared in a solvent such as ortho-dichlorobenzene or anisole, by a reaction at a temperature of at least 150° C. between at least one diamine compound and at least one halophthalic anhydride in the presence of imidization catalyst. The reaction produces a vapor stream comprising solvent and water formed as a by-product of the imidization reaction. A suitable vapor handling system comprising a partial reflux condenser is used to recycle the solvent, maintain the reactant concentration, conduct the reaction at a higher temperature, and effect more efficient conversion of reactants to product bis(halophthalimides). Reaction conditions disclosed may also be used to prepare organic polyimides.
摘要翻译：通过在酰亚胺化催化剂存在下，在至少一种二胺化合物和至少一种卤代邻苯二甲酸酐之间的至少150℃的温度下进行反应，在溶剂如邻二氯苯或苯甲醚中制备双（卤代邻苯二酰亚胺）。反应产生包含作为酰亚胺化反应的副产物形成的溶剂和水的蒸气流。使用包含部分回流冷凝器的合适的蒸汽处理系统来回收溶剂，保持反应物浓度，在较高温度下进行反应，并且使反应物更有效地转化成产物双（卤代邻苯二酰亚胺）。所公开的反应条件也可用于制备有机聚酰亚胺。

12. 发明申请

US20060066004A1 Method for controlling haze in an article comprising a polymer composition 有权
公开(公告)号：US20060066004A1
公开(公告)日：2006-03-30
申请号：US10955740
申请日：2004-09-30
申请人： William Richards , Farid Khouri , Thomas Guggenheim
发明人： William Richards , Farid Khouri , Thomas Guggenheim
IPC分类号： B29C47/00
CPC分类号： C08G73/10 , C08L79/00 , C08L79/08
摘要： A method for controlling haze in an article comprising a polymer composition, said method comprising providing a polymer composition comprising less than 25 parts per million alkali metal halide; and fabricating an article from said polymer composition.

13. 发明申请

US20050080228A1 Method for preparing polyimide and polyimide prepared thereby 有权
标题翻译：由此制备聚酰亚胺和聚酰亚胺的方法
公开(公告)号：US20050080228A1
公开(公告)日：2005-04-14
申请号：US10683226
申请日：2003-10-10
申请人： Norberto Silvi , Mark Giammattei , Paul Howson , Farid Khouri
发明人： Norberto Silvi , Mark Giammattei , Paul Howson , Farid Khouri
IPC分类号： C08G73/10 , C08G69/08
CPC分类号： C08G73/1028 , C08G73/1032
摘要： A method for preparing a polyimide includes introducing a mixture of an oligomer and a solvent to an extruder, removing solvent via at least one extruder vent, and melt kneading the oligomer to form a polyimide. The polyimide has a low residual solvent content. The method is faster than solution polymerization of polyimides, and it avoids the stoichiometric inaccuracies associated with reactive extrusion processes that use monomers as starting materials.
摘要翻译：制备聚酰亚胺的方法包括将低聚物和溶剂的混合物引入挤出机中，通过至少一个挤出机出口除去溶剂，并熔融捏合低聚物以形成聚酰亚胺。聚酰亚胺的残留溶剂含量低。该方法比聚酰亚胺的溶液聚合更快，并且避免了使用单体作为起始原料的反应挤出方法的化学计量不准确性。

14. 发明申请

US20070161821A1 METHOD FOR REMOVAL OF GUANIDINE COMPOUND FROM AQUEOUS MEDIA 失效
标题翻译：从水性介质中去除胍基化合物的方法
公开(公告)号：US20070161821A1
公开(公告)日：2007-07-12
申请号：US11684882
申请日：2007-03-12
申请人： David Hall , Thomas Guggenheim , James Silva , Farid Khouri , Matthew Littlejohn , Balakrishnan Ganesan , Ashok Shyadligeri , Pradeep Nadkarni
发明人： David Hall , Thomas Guggenheim , James Silva , Farid Khouri , Matthew Littlejohn , Balakrishnan Ganesan , Ashok Shyadligeri , Pradeep Nadkarni
IPC分类号： C07C277/06
CPC分类号： C02F9/00 , B01D61/027 , C02F1/281 , C02F1/283 , C02F1/44 , C02F2101/38 , C07C277/06 , C07C279/04
摘要： Disclosed is a method for removing a neutral or an ionic guanidine compound from aqueous media optionally comprising an alkali metal halide, wherein the method is selected from the group consisting of (a) adsorption onto a carbonaceous adsorbent, (b) adsorption onto a clay adsorbent, (c) filtration through a nanofiltration membrane, and (d) removal of water and calcination.
摘要翻译：公开了一种从任选地包含碱金属卤化物的水性介质中除去中性或离子胍化合物的方法，其中所述方法选自（a）吸附到含碳吸附剂上，（b）吸附到粘土吸附剂上，（c）通过纳滤膜过滤，和（d）去除水和煅烧。

15. 发明申请

US20070117962A1 High heat polyethersulfone compositions 审中-公开
标题翻译：高热聚醚砜组合物
公开(公告)号：US20070117962A1
公开(公告)日：2007-05-24
申请号：US11286521
申请日：2005-11-21
申请人： Daniel Steiger , Farid Khouri , Daniel Brunelle , Amy Koren
发明人： Daniel Steiger , Farid Khouri , Daniel Brunelle , Amy Koren
IPC分类号： C08G75/00
CPC分类号： C08G75/23 , C08G65/4056 , C08L81/06
摘要： High heat polyethersulfone compositions are provided which possess unexpectedly high glass transition temperatures. The polyethersulfone compositions comprise structural units derived from fluorenone bisphenols such as 9,9-bis(4-hydroxyphenyl)fluorene, and structural units derived from at least one biphenyl-bissulfone such as 4,4′-bis((4-chlorophenyl)sulfonyl)-1,1′-biphenyl. The novel polyethersulfone compositions may further comprise structural units derived from one or more biphenols such as 4,4′-biphenol, bisphenols such as BPA, or other electrophilic sulfone monomers, such as bis(4-chlorophenyl)sulfone. In one embodiment, the polyethersulfone composition of the present invention comprises structural groups derived exclusively from 9,9-bis(4-hydroxyphenyl)fluorene and 4,4′-bis((4-chlorophenyl)sulfonyl)-1,1′-biphenyl and exhibits a single glass transition of greater than 300° C.
摘要翻译：提供了具有出人意料的高玻璃化转变温度的高热聚醚砜组合物。聚醚砜组合物包含衍生自芴酮双酚的结构单元如9,9-双（4-羟基苯基）芴，以及衍生自至少一种联苯基 - 砜的结构单元，例如4,4'-双（（4-氯苯基）磺酰基）-1,1'-联苯。新型聚醚砜组合物还可以包含衍生自一种或多种双酚的结构单元，例如4,4'-联苯酚，双酚如BPA或其它亲电子砜单体如双（4-氯苯基）砜。在一个实施方案中，本发明的聚醚砜组合物包含仅由9,9-双（4-羟基苯基）芴衍生的结构基团和4,4'-双（（4-氯苯基）磺酰基）-1,1'-联苯并显示大于300℃的单一玻璃化转变。

16. 发明申请

US20060135733A1 Polycarbonate - ultem block copolymers 有权
标题翻译：聚碳酸酯 - 最终嵌段共聚物
公开(公告)号：US20060135733A1
公开(公告)日：2006-06-22
申请号：US11015216
申请日：2004-12-16
申请人： Farid Khouri , Julia Lee , Sheldon Shafer
发明人： Farid Khouri , Julia Lee , Sheldon Shafer
IPC分类号： C08G73/00
CPC分类号： C08G64/18 , C08G73/16
摘要： The present invention provides novel block copolycarbonates comprising residues from a hydroxy terminated polyetherimide or polyimide, residues from a dihydroxy compound, and residues from an activated carbonate. In a preferred embodiment of the present invention the polyetherimide or polyimide blocks exhibit high Mw while the resulting block copolycarbonate exhibits a single Tg. The novel block copolycarbonates of the present invention are produced under melt polymerization conditions in the presence an activated carbonate source.
摘要翻译：本发明提供新的嵌段共聚碳酸酯，其包含羟基封端的聚醚酰亚胺或聚酰亚胺的残基，二羟基化合物的残基和活化的碳酸酯的残基。在本发明的优选实施方案中，聚醚酰亚胺或聚酰亚胺嵌段表现出高的摩尔比，而所得的嵌段共聚碳酸酯表现出单一的T N。本发明的新型嵌段共聚碳酸酯在熔融聚合条件下在活性碳酸酯源存在下制备。

17. 发明申请

US20050049384A1 Novel approach to reduce cyclics formation in 3-CIPA based polyetherimide polymers 有权
标题翻译：基于3-CIPA的聚醚酰亚胺聚合物中循环形成的新方法
公开(公告)号：US20050049384A1
公开(公告)日：2005-03-03
申请号：US10647679
申请日：2003-08-25
申请人： Farid Khouri , Daniel Brunelle , Donald Johnson
发明人： Farid Khouri , Daniel Brunelle , Donald Johnson
IPC分类号： C07D209/48 , C08G73/12 , C08G8/02
CPC分类号： C07D209/48 , C08G73/12 , C08G73/124
摘要： Methods of reducing the amount of undesirable cyclic oligomer by-products in the production of polyetherimides are disclosed. The resulting polyetherimides have enhanced thermomechanical properties.
摘要翻译：公开了减少聚醚酰亚胺生产中不期望的环状低聚物副产物量的方法。得到的聚醚酰亚胺具有增强的热机械性能。

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