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11. 发明专利

JPH111306A PRODUCTION OF HYDROGEN PEROXIDE 失效
公开(公告)号：JPH111306A
公开(公告)日：1999-01-06
申请号：JP13134397
申请日：1997-05-21
申请人： ENICHEM SPA
发明人： BIANCHI DANIELE , BORTOLO ROSSELLA , D ALOISIO RINO , RICCI MARCO , SOATTINI SERGIO
IPC分类号： C01B15/00 , B01J31/22 , C01B15/027
摘要： PROBLEM TO BE SOLVED: To effectively and inexpensively produce hydrogen peroxide by reacting carbon monoxide, oxygen and water in an organic solvent immiscible with water in the presence of such a catalyst complex as to comprise palladium salt, non-coordinating organic or inorganic acid, and a ligand bondable with a specific palladium atom. SOLUTION: This method comprises: dissolving into 1 l of organic solvent immiscible water an organic solvent-soluble catalyst carrier comprising 0.001 to 0.5 mol. of palladium salt, non-coordinating organic or inorganic acid, and a ligand bondable with palladium atom of a monodentate or multidentate nitrogenized compound and having (1:1) to (60:1) molecular ratio of acid to palladium; adding carbon monoxide of >=1 atom and oxygen to the organic solvent so that a molecular ratio of the carbon monoxide to oxygen may be (1:99) to (12:88) and a volumetric ratio of water to the organic solvent may be (30:70) to (70:30); reacting the mixture at -20 to 100 deg.C for 15 min. to 10 hrs.; separating a water phase containing hydrogen peroxide and organic solvent phase; and thus obtaining the resultant water phase containing 2 to 10 wt.% of hydrogen peroxide.

12. 发明专利

JP2000202291A NOVEL CATALYST, PRODUCTION OF HYDROGEN PEROXIDE AND USE OF HYDROGEN PEROXIDE IN OXIDATION PROCESS 失效
公开(公告)号：JP2000202291A
公开(公告)日：2000-07-25
申请号：JP22161799
申请日：1999-08-04
申请人： ENICHEM SPA
发明人： PAPARATTO GIUSEPPE , D ALOISIO RINO , DE ALBERTI GIORDANO , FURLAN PIERO , ARCA VITTORIO , BUZZONI ROBERTO , LAURA MEDA
IPC分类号： B01J23/38 , B01J21/18 , B01J23/40 , B01J23/44 , B01J27/02 , B01J31/02 , B01J37/02 , C01B15/029
摘要： PROBLEM TO BE SOLVED: To enhance the productivity of hydrogen peroxide synthesis by using a catalyst comprising a group VIII metal supported on a catalyst carrier formed from an acidic activated carbon functionalized with sulfo groups. SOLUTION: The catalyst is prepared from a group VIII metal supported on an acidic activated carbon carrier functionalized with sulfo groups and hydrogen peroxide is produced from hydrogen and oxygen in a solvent in the presence of a catalyst system consisting of a promoter and the catalyst. The amount of the group VIII metal is 0.05-5 wt.% of that of the carrier and 0.1-1 wt.% sulfur is optionally contained in the functionalized activated carbon. The catalyst is obtained by bringing an activated carbon into contact with a sulfonating agent, washing the functionalized activated carbon, treating the sulfonated activated carbon with an oxidizing agent and carrying out washing and drying.

13. 发明申请

WO02092501A8 DIRECT SYNTHESIS OF HYDROGEN PEROXIDE IN A MULTICOMPONENT SOLVENT SYSTEM 审中-公开
标题翻译：过氧化氢在多元溶剂系统中的直接合成
公开(公告)号：WO02092501A8
公开(公告)日：2004-06-10
申请号：PCT/EP0204578
申请日：2002-04-25
申请人： ENI SPA , POLIMERI EUROPA SPA , PAPARATTO GIUSEPPE , DE ALBERTI GIORDANO , D ALOISIO RINO
发明人： PAPARATTO GIUSEPPE , DE ALBERTI GIORDANO , D ALOISIO RINO
IPC分类号： B01J23/44 , C01B15/029
CPC分类号： C01B15/029 , B01J23/44
摘要： A process is described for the production of hydrogen peroxide from hydrogen and oxygen in a reaction solvent containing a halogenated promoter and/or an acid promoter, in the presence of a heterogeneous catalyst based on one or more metals of the platinum group, wherein the reaction solvent consists of: (1) an alcohol or mixture of alcohols; (2) one or more c5-C32 hydrocarbons; and (3) optionally water. The process operates under high safety conditions with a high productivity and molar selectivity towards the formation of H2O2.
摘要翻译：描述了在基于一种或多种铂族金属的非均相催化剂的存在下，在含有卤化促进剂和/或酸助催化剂的反应溶剂中，从氢和氧生成过氧化氢的方法，其中反应溶剂包括：（1）醇或醇的混合物; （2）一种或多种c5-C32烃; 和（3）任选的水。该方法在高安全性条件下以高生产率和摩尔选择性形成H 2 O 2。

14. 发明申请

WO03014014A2 CATALYST AND ITS USE IN THE SYNTHESIS OF HYDROGEN PEROXIDE 审中-公开
标题翻译：催化剂及其在过氧化氢合成中的应用
公开(公告)号：WO03014014A2
公开(公告)日：2003-02-20
申请号：PCT/EP0208546
申请日：2002-07-30
申请人： ENI SPA , POLIMERI EUROPA SPA , PAPARATTO GIUSEPPE , DE ALBERTI GIORDANO , D ALOISIO RINO , BUZZONI ROBERTO
发明人： PAPARATTO GIUSEPPE , DE ALBERTI GIORDANO , D ALOISIO RINO , BUZZONI ROBERTO
IPC分类号： C01B15/00 , B01J21/18 , B01J23/40 , B01J23/42 , B01J23/44 , B01J27/053 , B01J31/06 , B01J31/28 , C01B15/029
CPC分类号： C01B15/029 , B01J21/18 , B01J23/40 , B01J23/42 , B01J23/44 , B01J27/053 , B01J31/06
摘要： The present invention relates to a catalyst consisting of: (a) one or more metals of the platinum group as active components; (b) one or more polyolefins; and (c) a carrier. The invention also relates to a process for the synthesis of hydrogen peroxide (H2O2) from hydrogen and oxygen which uses said catalyst and the use of the hydrogen peroxide solution in oxidation processes catalyzed by titanium silicalite. The process operates under high safety conditions with a high productivity and molar selectivity towards the formation of H2O2.
摘要翻译：本发明涉及一种由以下组成的催化剂：（a）一种或多种铂族金属作为活性组分; （b）一种或多种聚烯烃; 和（c）承运人。本发明还涉及从氢和氧合成过氧化氢（H 2 O 2）的方法，其使用所述催化剂，以及在由钛硅沸石催化的氧化过程中使用过氧化氢溶液。该方法在高安全性条件下以高生产率和摩尔选择性形成H 2 O 2。

15. 发明专利

DE60203900T2 未知
公开(公告)号：DE60203900T2
公开(公告)日：2005-08-25
申请号：DE60203900
申请日：2002-04-29
申请人： POLIMERI EUROPA SPA , ENI SPA
发明人： PAPARATTO GIUSEPPE , DE ALBERTI GIORDANO , D ALOISIO RINO
IPC分类号： C01B15/026 , B01J23/44 , C01B15/022 , C01B15/029 , C01B3/00
摘要： A process is described for the production of hydrogen peroxide from hydrogen and oxygen in a reaction solvent containing a halogenated promoter and/or an acid promoter, in the presence of a heterogeneous catalyst based on one or more metals of the platinum group, wherein the reaction solvent consists of: (1) an alcohol or mixture of alcohols; (2) an aliphatic ether having general formula (I); and (3) optionally water. The solvent mixture may also contain one or more C 5 -C 32 hydrocarbons. The process operates under high safety conditions with a high productivity and molar selectivity towards the formation of H 2 O 2 .

16. 发明专利

NO20035092A Direkte syntese av hydrogenperoksyd i et flerkomponent løsningsmiddelsystem 未知
公开(公告)号：NO20035092A
公开(公告)日：2004-01-16
申请号：NO20035092
申请日：2003-11-14
申请人： ENI SPA , VERSALIS SPA
发明人： D ALOISIO RINO , PAPARATTO GIUSEPPE , ALBERTI GIORDANO DE
IPC分类号： C01B15/026 , C01B15/029 , B01J23/44 , C01B15/022
CPC分类号： C01B15/029

17. 发明专利

DE60208384D1 未知
公开(公告)号：DE60208384D1
公开(公告)日：2006-02-02
申请号：DE60208384
申请日：2002-07-30
申请人： POLIMERI EUROPA SPA , ENI SPA
发明人： PAPARATTO GIUSEPPE , DE ALBERTI GIORDANO , D ALOISIO RINO , BUZZONI ROBERTO
IPC分类号： C01B15/00 , B01J21/18 , B01J23/40 , B01J23/42 , B01J23/44 , B01J27/053 , B01J31/06 , B01J31/28 , C01B15/029 , C01B21/26 , C07C249/04 , C07D301/12 , C07D303/04
摘要： The present invention relates to a catalyst consisting of: (a) one or more metals of the platinum group as active components; (b) one or more polyolefins; and (c) a carrier. The invention also relates to a process for the synthesis of hydrogen peroxide (H 2 O 2 ) from hydrogen and oxygen which uses said catalyst and the use of the hydrogen peroxide solution in oxidation processes catalyzed by titanium silicalite. The process operates under high safety conditions with a high productivity and molar selectivity towards the formation of H 2 O 2 .

18. 发明专利

DK1390288T3 未知
公开(公告)号：DK1390288T3
公开(公告)日：2005-06-13
申请号：DK02740557
申请日：2002-04-29
申请人： ENI SPA , POLIMERI EUROPA SPA
发明人： PAPARATTO GIUSEPPE , DE ALBERTI GIORDANO , D ALOISIO RINO
IPC分类号： C01B15/026 , B01J23/44 , C01B15/022 , C01B15/029 , C01B3/00
摘要： A process is described for the production of hydrogen peroxide from hydrogen and oxygen in a reaction solvent containing a halogenated promoter and/or an acid promoter, in the presence of a heterogeneous catalyst based on one or more metals of the platinum group, wherein the reaction solvent consists of: (1) an alcohol or mixture of alcohols; (2) an aliphatic ether having general formula (I); and (3) optionally water. The solvent mixture may also contain one or more C 5 -C 32 hydrocarbons. The process operates under high safety conditions with a high productivity and molar selectivity towards the formation of H 2 O 2 .

19. 发明专利

CA2446336C DIRECT SYNTHESIS OF HYDROGEN PEROXIDE IN A MULTICOMPONENT SOLVENT SYSTEM 未知
公开(公告)号：CA2446336C
公开(公告)日：2010-07-06
申请号：CA2446336
申请日：2002-04-29
申请人： ENI SPA , POLIMERI EUROPA SPA
发明人： PAPARATTO GIUSEPPE , DE ALBERTI GIORDANO , D ALOISIO RINO
IPC分类号： C01B15/026 , C01B15/029 , B01J23/44 , C01B15/022
摘要： A process is described for the production of hydrogen peroxide from hydrogen and oxygen in a reaction solvent containing a halogenated promoter and/or an acid promoter, in the presence of a heterogeneous catalyst based on one or more metals of the platinum group, wherein the reaction solvent consists of: (1) an alcohol or mixture of alcohols; (2) an aliphatic ether having general formula (I); and (3) optionally water. The solvent mixture may also contain one or more C5-C32 hydrocarbons. The process operates under high safety conditions with a high productivity and molar selectivity towards the formation of H2O2.

20. 发明专利

NO326991B1 未知
公开(公告)号：NO326991B1
公开(公告)日：2009-03-30
申请号：NO20040435
申请日：2004-01-30
申请人： ENI SPA
发明人： D ALOISIO RINO , PAPARATTO GIUSEPPE , ALBERTI GIORDANO DE , BUZZONI ROBERTO
IPC分类号： B01J23/40 , C01B15/00 , B01J21/18 , B01J23/42 , B01J23/44 , B01J27/053 , B01J31/06 , B01J31/28 , C01B15/029
摘要： The present invention relates to a catalyst consisting of: (a) one or more metals of the platinum group as active components; (b) one or more polyolefins; and (c) a carrier. The invention also relates to a process for the synthesis of hydrogen peroxide (H 2 O 2 ) from hydrogen and oxygen which uses said catalyst and the use of the hydrogen peroxide solution in oxidation processes catalyzed by titanium silicalite. The process operates under high safety conditions with a high productivity and molar selectivity towards the formation of H 2 O 2 .

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