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11. 发明授权

US10837103B2 Scratch-resistant materials and articles including the same 有权
公开(公告)号：US10837103B2
公开(公告)日：2020-11-17
申请号：US15696559
申请日：2017-09-06
申请人： CORNING INCORPORATED
发明人： Kaveh Adib , Robert Alan Bellman , Charles Andrew Paulson , James Joseph Price
IPC分类号： C23C16/30 , C23C16/36 , C23C16/40 , C23C16/34 , C23C16/32
CPC分类号： C23C16/308 , C23C16/30 , C23C16/325 , C23C16/345 , C23C16/36 , C23C16/402
摘要： Embodiments of this disclosure pertain to a coating material comprising silicon and/or aluminum, hydrogen and any two or more of oxygen, nitrogen, carbon, and fluorine. The coating material exhibits a hardness of about 17 GPa or greater and an optical band gap of about 3.5 eV or greater. In some embodiments, the coating material includes, in atomic %, silicon and/or aluminum in an amount of about 40 or greater, hydrogen in an amount in the range from about 1 to about 25, nitrogen in an amount of about 30 or greater, oxygen in an amount in the range from about 0 to about 7.5, and carbon in an amount in the range from about 0 to about 10. The coating material may optionally include fluorine and/or boron. Articles including the coating material are also described and exhibit an average transmittance of about 85% or greater over an optical wavelength regime in the range from about 380 nm to about 720 nm and colorlessness.

12. 发明授权

US10436945B2 Durable and scratch-resistant anti-reflective articles 有权
公开(公告)号：US10436945B2
公开(公告)日：2019-10-08
申请号：US15657772
申请日：2017-07-24
申请人： CORNING INCORPORATED
发明人： Shandon Dee Hart , Karl William Koch, III , Charles Andrew Paulson , James Joseph Price
IPC分类号： G02B1/115 , G02B1/11 , G02B1/14 , G02B5/02 , C03C17/34 , C03C21/00 , G02B1/18 , G02B27/00
摘要： Embodiments of durable, anti-reflective articles are described. In one or more embodiments, the article includes a substrate and an optical coating disposed on the major surface. The optical coating includes an anti-reflective coating and a scratch-resistant coating forming an anti-reflective surface. The article exhibits a maximum hardness of 12 GPa or greater, as measured on the anti-reflective surface by a Berkovich Indenter Hardness Test along an indentation depth of about 100 nm or greater. The articles of some embodiments exhibit a single side average light reflectance measured at the anti-reflective surface of about 8% or less over an optical wavelength regime in the range from about 400 nm to about 800 nm and a reference point color shift in transmittance or reflectance of less than about 2. In some embodiments, the article exhibits an angular color shift of about 5 or less at all angles from normal incidence to an incident illumination angle that is 20 degrees or greater.

13. 发明申请

US20190039946A1 GLASS-FILM LAMINATES WITH CONTROLLED FAILURE STRENGTH 审中-公开
公开(公告)号：US20190039946A1
公开(公告)日：2019-02-07
申请号：US16156437
申请日：2018-10-10
申请人： Corning Incorporated
发明人： John Frederick Bayne , Zhanjun Gao , Shandon Dee Hart , Guangli Hu , James Joseph Price , Chandan Kumar Saha
IPC分类号： C03C17/09 , C03C17/34 , C03C17/25 , C03C17/245 , C03C21/00
摘要： A glass-film laminate or article having a narrow failure distribution or a Weibull modulus of greater than 10. In embodiments, the glass-film laminate or article includes at least one first film disposed on a strengthened glass substrate. A first film or any additional films can exhibit an average strain-to-failure that is less than the strain-to-failure of the strengthened glass substrate. In embodiments, the first first film is adhered to the glass substrate such that the first film does not exhibit visible delamination from the glass substrate. Methods of forming glass-film laminates or articles with a desired strength level and narrow failure strength distrubution are also disclosed.

14. 发明申请

US20180186693A1 STRENGTHENED GLASS ARTICLES HAVING ETCHED FEATURES AND METHODS OF FORMING THE SAME 审中-公开
公开(公告)号：US20180186693A1
公开(公告)日：2018-07-05
申请号：US15906225
申请日：2018-02-27
申请人： Corning Incorporated
发明人： Johannes Moll , James Joseph Price , Alranzo Boh Ruffin , Sergio Tsuda , Robert Stephen Wagner , James Joseph Watkins
IPC分类号： C03C23/00 , B44C1/22 , B41M5/24 , C03C21/00
CPC分类号： C03C23/0025 , B41M5/24 , B44C1/227 , B44C1/228 , C03C21/002 , Y10T428/24479 , Y10T428/24521
摘要： Strengthened glass articles having laser etched features, electronic devices, and methods of fabricating etched features in strengthened glass articles are disclosed. In one embodiment, a strengthened glass article includes a first strengthened surface layer and a second strengthened surface layer under a compressive stress and extending from a first surface and a second surface, respectively, of the strengthened glass article to a depth of layer, and a central region between the first strengthened surface layer and the second strengthened surface layer that is under tensile stress. The strengthened glass article further includes at least one etched feature formed by laser ablation within the first surface or the second surface having a depth that is less than the depth of layer and a surface roughness that is greater than a surface roughness of the first surface or second surface outside of the at least one etched feature.

15. 发明申请

US20170369992A1 SCRATCH-RESISTANT MATERIALS AND ARTICLES INCLUDING THE SAME 审中-公开
公开(公告)号：US20170369992A1
公开(公告)日：2017-12-28
申请号：US15696559
申请日：2017-09-06
申请人： CORNING INCORPORATED
发明人： Kaveh Adib , Robert Alan Bellman , Charles Andrew Paulson , James Joseph Price
IPC分类号： C23C16/30 , C23C16/34 , C23C16/32 , C23C16/40 , C23C16/36
摘要： Embodiments of this disclosure pertain to a coating material comprising silicon and/or aluminum, hydrogen and any two or more of oxygen, nitrogen, carbon, and fluorine. The coating material exhibits a hardness of about 17 GPa or greater and an optical band gap of about 3.5 eV or greater. In some embodiments, the coating material includes, in atomic %, silicon and/or aluminum in an amount of about 40 or greater, hydrogen in an amount in the range from about 1 to about 25, nitrogen in an amount of about 30 or greater, oxygen in an amount in the range from about 0 to about 7.5, and carbon in an amount in the range from about 0 to about 10. The coating material may optionally include fluorine and/or boron. Articles including the coating material are also described and exhibit an average transmittance of about 85% or greater over an optical wavelength regime in the range from about 380 nm to about 720 nm and colorlessness.

16. 发明申请

US20160368812A1 STRENGTHENED GLASS ARTICLES AND METHODS OF MAKING 审中-公开
公开(公告)号：US20160368812A1
公开(公告)日：2016-12-22
申请号：US15215073
申请日：2016-07-20
申请人： Corning Incorporated
发明人： Kristen L. Barefoot , James Joseph Price , Jose Mario Quintal , Ronald Leroy Stewart
IPC分类号： C03C3/095 , C03C3/093 , C03C4/18 , C03C3/085 , C03C3/087 , C03C3/091 , C03C3/083
CPC分类号： C03C3/095 , C03C3/064 , C03C3/078 , C03C3/083 , C03C3/085 , C03C3/087 , C03C3/091 , C03C3/093 , C03C4/18 , C03C21/002 , C03C2204/00 , Y10T428/31 , Y10T428/315
摘要： A strengthened glass article having a central tension that is below a threshold value above which the glass exhibits frangible behavior. The central tension varies non-linearly with the thickness of the glass. The glass article may be used as cover plates or windows for portable or mobile electronic devices such as cellular phones, music players, information terminal (IT) devices, including laptop computers, and the like.

17. 发明申请

US20160351837A1 MECHANICALLY FLEXIBLE AND DURABLE SUBSTRATES AND METHOD OF MAKING 审中-公开
标题翻译：机械柔性和耐用的基材及其制备方法
公开(公告)号：US20160351837A1
公开(公告)日：2016-12-01
申请号：US15232401
申请日：2016-08-09
申请人： Corning Incorporated
发明人： Sean Matthew Garner , Gregory Scott Glaesemann , James Joseph Price
IPC分类号： H01L51/00 , C03C4/00 , C03C17/34
CPC分类号： H01L51/0097 , C03C4/00 , C03C17/34 , H01L31/03926 , H01L2251/5338 , Y02E10/549
摘要： A flexible substrate are disclosed comprising an amorphous inorganic composition, wherein the substrate has a thickness of less than about 250 μm and has at least one of: a) a brittleness ratio less than about 9.5 (μm)−1/2, or b) a fracture toughness of at least about 0.75 MPa·(m)1/2. Electronic devices comprising such flexible devices are also disclosed. Also disclosed is a method for making a flexible substrate comprising selecting an amorphous inorganic material capable of forming a substrate having a thickness of less than about 250 μm and having at least one of: a) a brittleness ratio of less than about 9.5 (μm)−1/2, or b) a fracture toughness of at least about 0.75 MPa·(m)1/2; and then forming a substrate from the selected inorganic material.
摘要翻译：公开了一种柔性基底，其包括无定形无机组合物，其中所述基底具有小于约250μm的厚度，并且具有以下至少一种：a）脆性比小于约9.5（μm）-1/2，或b）断裂韧性至少约为0.75MPa·（m）1/2。还公开了包括这种柔性装置的电子设备。还公开了一种制造柔性基材的方法，包括选择能够形成厚度小于约250μm的基材的无定形无机材料，并具有以下中的至少一种：a）小于约9.5（μm）的脆性比， -1/2，或b）断裂韧性为至少约0.75MPa·（m）1/2; 然后从所选择的无机材料形成衬底。

18. 发明申请

US20160238743A1 LOW-COLOR SCRATCH-RESISTANT ARTICLES WITH A MULTILAYER OPTICAL FILM 审中-公开
标题翻译：具有多层光学膜的低颜色耐刮擦物品
公开(公告)号：US20160238743A1
公开(公告)日：2016-08-18
申请号：US15142508
申请日：2016-04-29
申请人： CORNING INCORPORATED
发明人： Robert Alan Bellman , Shandon Dee Hart , Karl William Koch, III , Charles Andrew Paulson , James Joseph Price
IPC分类号： G02B1/14 , C03C17/34 , G02B1/115
CPC分类号： G02B1/14 , C03C17/3435 , C03C2217/734 , C03C2217/78 , G02B1/10 , G02B1/105 , G02B1/113 , G02B1/115 , Y10T428/315
摘要： Embodiments of this disclosure pertain to articles that exhibit scratch-resistance and improved optical properties. In some examples, the article exhibits a color shift of about 2 or less, when viewed at an incident illumination angle in the range from about 0 degrees to about 60 degrees from normal under an illuminant. In one or more embodiments, the articles include a substrate, and an optical film disposed on the substrate. The optical film includes a scratch-resistant layer and an optical interference layer. The optical interference layer may include one or more sub-layers that exhibit different refractive indices. In one example, the optical interference layer includes a first low refractive index sub-layer and a second a second high refractive index sub-layer. In some instances, the optical interference layer may include a third sub-layer.
摘要翻译：本公开的实施方案涉及具有耐刮擦性和改善的光学性质的制品。在一些实例中，当在照射下照射角度约为0度至约60度的入射照明角度时，该物品呈现约2或更小的色移。在一个或多个实施例中，制品包括衬底和设置在衬底上的光学膜。光学膜包括防刮层和光学干涉层。光学干涉层可以包括呈现不同折射率的一个或多个子层。在一个示例中，光学干涉层包括第一低折射率子层和第二高折射率子层。在一些情况下，光学干涉层可以包括第三子层。

19. 发明申请

US20140106146A1 ARTICLES HAVING RETAINED STRENGTH 审中-公开
标题翻译：具有保留强度的文章
公开(公告)号：US20140106146A1
公开(公告)日：2014-04-17
申请号：US14052055
申请日：2013-10-11
申请人： CORNING INCORPORATED
发明人： Heather Bossard Decker , Shandon Dee Hart , Guangli Hu , Fei Li , James Joseph Price , Chandan Kumar Saha
IPC分类号： G06F3/03
CPC分类号： C03C17/34 , C03C17/3417 , C03C17/3435 , C03C17/36 , C03C17/38 , C03C17/42 , C03C21/002 , C03C2217/425 , C03C2217/948 , G06F3/03 , Y10T428/24851 , Y10T428/24926 , Y10T428/2495 , Y10T428/24975 , Y10T428/24983 , Y10T428/24996 , Y10T428/24999
摘要： One or more aspects of the disclosure pertain to an article including a film disposed on a glass substrate, which may be strengthened, where the interface between the film and the glass substrate is modified, such that the article retains its average flexural strength, and the film retains key functional properties for its application. Some key functional properties of the film include optical, electrical and/or mechanical properties. The bridging of a crack from one of the film or the glass substrate into the other of the film or the glass substrate can be prevented by inserting a crack mitigating layer between the glass substrate and the film.
摘要翻译：本公开的一个或多个方面涉及一种包括设置在玻璃基板上的膜的物品，其可以被加强，其中膜和玻璃基板之间的界面被修改，使得制品保持其平均弯曲强度，并且电影保留了其应用的关键功能特性。膜的一些关键功能特性包括光学，电学和/或机械性质。可以通过在玻璃基板和膜之间插入裂纹缓解层来防止从薄膜或玻璃基板中的一个到玻璃基板的另一个中的裂纹的桥接。

20. 发明申请

US20130273324A1 STRENGTHENED GLASS ARTICLES HAVING ETCHED FEATURES AND METHODS OF FORMING THE SAME 有权
标题翻译：具有蚀刻特征的强化玻璃制品及其形成方法
公开(公告)号：US20130273324A1
公开(公告)日：2013-10-17
申请号：US13800033
申请日：2013-03-13
申请人： CORNING INCORPORATED
发明人： Johannes Moll , James Joseph Price , Alranzo Boh Ruffin , Sergio Tsuda , Robert Stephen Wagner , James Joseph Watkins
IPC分类号： C03C23/00
CPC分类号： C03C23/0025 , B41M5/24 , B44C1/227 , B44C1/228 , C03C21/002 , Y10T428/24479 , Y10T428/24521
摘要： Strengthened glass articles having laser etched features, electronic devices, and methods of fabricating etched features in strengthened glass articles are disclosed. In one embodiment, a strengthened glass article includes a first strengthened surface layer and a second strengthened surface layer under a compressive stress and extending from a first surface and a second surface, respectively, of the strengthened glass article to a depth of layer, and a central region between the first strengthened surface layer and the second strengthened surface layer that is under tensile stress. The strengthened glass article further includes at least one etched feature formed by laser ablation within the first surface or the second surface having a depth that is less than the depth of layer and a surface roughness that is greater than a surface roughness of the first surface or second surface outside of the at least one etched feature.
摘要翻译：公开了具有激光蚀刻特征的加强玻璃制品，电子装置和在加强玻璃制品中制造蚀刻特征的方法。在一个实施例中，加强的玻璃制品在压缩应力下包括第一加强表面层和第二增强表面层，并且分别从强化玻璃制品的第一表面和第二表面延伸到层的深度，第一强化表面层和处于拉伸应力的第二强化表面层之间的中心区域。所述强化玻璃制品还包括至少一个蚀刻特征，所述蚀刻特征通过在所述第一表面或所述第二表面内的激光烧蚀形成，所述蚀刻特征具有小于所述层的深度的深度和大于所述第一表面的表面粗糙度的表面粗糙度，在所述至少一个蚀刻特征之外的第二表面。

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