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    • 11. 发明申请
      US20080295688A1 Process for Extracting (Chlorinated) Hydrocarbon-Free Hydrogen Chloride and Phosgene-Free (Chlorinated) Hydrocarbons from a Hydrogen Chloride Stream Containing (Chlorinated) Hydrocarbons and Phosgene 有权
    • Process for Extracting (Chlorinated) Hydrocarbon-Free Hydrogen Chloride and Phosgene-Free (Chlorinated) Hydrocarbons from a Hydrogen Chloride Stream Containing (Chlorinated) Hydrocarbons and Phosgene
    • 从含有（氯化）碳氢化合物和光气的氯化氢流中提取（氯化）无碳氢化合物和无光气（氯化）烃的方法
    • US20080295688A1
    • 2008-12-04
    • US12159797
    • 2007-01-25
    • Martin Sesing , Heiner Schelling , Jurgen Ciprian , Filip Deberdt , Martin Karches , Olga Schubert
    • Martin Sesing , Heiner Schelling , Jurgen Ciprian , Filip Deberdt , Martin Karches , Olga Schubert
    • B01D53/02
    • C01B7/0718
    • Process for recovering (chloro)hydrocarbon-free hydrogen chloride and phosgene-free (chloro)hydrocarbons from a hydrogen chloride stream comprising (chloro)hydrocarbons and phosgene, which comprises i) in a first step, connecting a first adsorber and a second adsorber in series and passing the fresh hydrogen chloride stream comprising phosgene and (chloro)hydrocarbons firstly through the first adsorber and subsequently through the second adsorber until essentially no more (chloro)hydrocarbon is adsorbed by the first adsorber, ii) in a second step, passing the fresh hydrogen chloride stream through the second adsorber while the first adsorber is regenerated, with essentially phosgene-free (chloro)hydrocarbon being obtained in the regeneration, iii) in a third step, passing the fresh hydrogen chloride steam firstly through the second adsorber and subsequently through the regenerated first adsorber until essentially no more (chloro)hydrocarbon is adsorbed by the second adsorber, iv) in a fourth step, passing the fresh hydrogen chloride stream through the first adsorber while the second adsorber is regenerated, with essentially phosgene-free (chloro)hydrocarbon being obtained in the regeneration, with the steps i) to iv) being able to be carried out one or more times in succession.
    • 从含有（氯）烃和光气的氯化氢流中回收（氯）无烃氯化氢和无光气（氯）烃的方法，其包括i）在第一步骤中，将第一吸附剂和第二吸附剂连接在 串联并通过包含光气和（氯）烃的新鲜氯化氢料流首先通过第一吸附器并随后通过第二吸附器，直到基本上不再有（氯）烃被第一吸附器吸附，ii）在第二步中， 新鲜的氯化氢流通过第二吸附器，同时第一吸附器被再生，在再生中获得基本上无光气（氯）烃; iii）在第三步骤中，将新鲜的氯化氢蒸汽首先通过第二吸附器，随后 通过再生的第一吸附器直到基本上不再有（氯）烃被第二吸附器吸附，iv） 第四步，使新鲜的氯化氢流通过第一吸附器，同时再生第二吸附器，在再生中获得基本上无光气的（氯）烃，步骤i）至iv）能够进行一次 或更多次。
    • 基本信息 添加关注 加入工作空间 PDF全文 PDF下载 全文下载 相似专利 双屏查看 权利要求书 说明书全文 Global Dossier Espacenet 法律信息 同族专利 专利引用
    • 15. 发明申请
      US20070135650A1 Method for the production of defined mixtures of thf, bdo and gbl by gas phase hydrogenation 失效
    • Method for the production of defined mixtures of thf, bdo and gbl by gas phase hydrogenation
    • US20070135650A1
    • 2007-06-14
    • US10581074
    • 2004-12-04
    • Markus Rosch , Rolf Pinkos , Michael Hesse , Stephan Schlitter , Henrik Junicke , Olga Schubert , Alexander Weck , Gunther Windecker
    • Markus Rosch , Rolf Pinkos , Michael Hesse , Stephan Schlitter , Henrik Junicke , Olga Schubert , Alexander Weck , Gunther Windecker
    • C07D307/02
    • C07D307/33 , C07D307/08
    • The present invention provides a process for variably preparing mixtures of optionally alkyl-substituted BDO, GBL and THF by two-stage hydrogenation in the gas phase of C4 dicarboxylic acids and/or derivatives thereof, which comprises a) in a first step in the gas phase, hydrogenating a gas stream of C4 dicarboxylic acids and/or derivatives thereof over a catalyst at a pressure of from 2 to 100 bar and a temperature of from 200° C. to 300° C. in a first reactor in the presence of a catalyst in the form of shaped catalyst bodies having a volume of less than 20 mm3, said catalyst from 5 to 95% by weight of oxide of copper and from 5 to 95% by weight of an oxide having acidic sites, to give a stream mainly containing of optionally alkyl-substituted GBL and THF, b) removing any succinic anhydride formed by partial condensation, c) converting the products remaining predominantly in the gas phase in the partial condensation, THF, water and GBL, under the same pressure or under a pressure reduced by the pressure drops in the hydrogenation circuit and at a temperature of from 150 to 240° C., in a second reactor over a catalyst which ≦95% by weight of CuO and from 5 to 95% by weight of one or more oxides selected from the group of ZnO, Al2O3, SiO2, TiO2, ZrO2, CeO2, MgO, CaO, SrO, BaO, La2O3 and Mn2O3 to give a stream comprising a mixture of BDO, GBL and THF, d) removing the hydrogen from the products and recycling it into the hydrogenation, e) distillatively separating the products, THF, BDO, GBL and water, if appropriate recycling a GBL-rich stream into the second reactor or if appropriate discharging it, and working up BDO, THF and GBL distillatively, and setting the ratio of the products, THF, GBL and BDO, relative to one another within the range from 10 to 100% by weight of THF, from 0 to 90% by weight of GBL and from 0 to 90% by weight of BDO only by varying the temperatures in the two hydrogenation zones and also if appropriate the GBL recycle stream.
    • 基本信息 添加关注 加入工作空间 PDF全文 PDF下载 全文下载 相似专利 双屏查看 权利要求书 说明书全文 Global Dossier Espacenet 法律信息 同族专利 专利引用
    • 17. 发明授权
      US07442810B2 Method for the production of defined mixtures of THF, BDO and GBL by gas phase hydrogenation 失效
    • Method for the production of defined mixtures of THF, BDO and GBL by gas phase hydrogenation
    • 通过气相氢化制备THF，BDO和GBL的限定混合物的方法
    • US07442810B2
    • 2008-10-28
    • US10581074
    • 2004-12-04
    • Markus Roesch , Rolf Pinkos , Michael Hesse , Stephan Schlitter , Henrik Junicke , Olga Schubert , Alexander Weck , Gunther Windecker
    • Markus Roesch , Rolf Pinkos , Michael Hesse , Stephan Schlitter , Henrik Junicke , Olga Schubert , Alexander Weck , Gunther Windecker
    • C07D307/00 , C07D307/02
    • C07D307/33 , C07D307/08
    • A process for variably preparing mixtures of optionally alkyl-substituted BDO, GBL and THF by two-stage hydrogenation in the gas phase of C4 dicarboxylic acids and/or derivatives thereof, which comprises a) hydrogenating in a gas phase a gas stream of C4 dicarboxylic acids and/or derivatives thereof over a particular catalyst at a particular pressure and temperature to give a stream mainly containing of optionally alkyl-substituted GBL and THF, b) removing any succinct anhydride, c) converting the products remaining predominantly in the gas phase in the partial condensation, THF, water and GBL to give a stream comprising a mixture of BDO, GBL and THF, d) removing the hydrogen from the products and recycling it into the hydrogenation, e) distillatively separating the products, THF, BDO, GBL and water, if appropriate recycling a GBL-rich stream or if appropriate discharging it, and working up BDO, THF and GBL distillatively, and setting the ratio of the products, THF, GBL and BDO, relative to one another within the range from 10 to 100% by weight of THF, from 0 to 90% by weight of GBL and from 0 to 90% by weight of BDO only by varying the temperatures in the two hydrogenation zones and also if appropriate the GBL recycle stream.
    • 一种在可能地制备任选烷基取代的BDO，GBL和THF的混合物的方法，其通过在C 4 C 4羧酸和/或其衍生物的气相中进行两步氢化，其包括a）在 在特定的压力和温度下，将特定催化剂上的C 4 O 2羧酸和/或其衍生物的气流气相，得到主要含有烷基取代的GBL和THF的物流，b）除去 任何简单的酸酐，c）将部分冷凝，THF，水和GBL中主要保留在气相中的产物进行转化，得到包含BDO，GBL和THF的混合物的流，d）从产物中除去氢并将其再循环 进入氢化，e）蒸馏分离产物，THF，BDO，GBL和水，如果适当回收富含GBL的物流或适当排放，并蒸馏处理BDO，THF和GBL，并设定产物的比例 ，TH F，GBL和BDO相对于10重量％至100重量％的THF，0至90重量％的GBL​​和0至90重量％的BDO，仅通过改变两者中的温度 加氢区，如果合适的话也可以使用GBL再循环流。
    • 基本信息 添加关注 加入工作空间 PDF全文 PDF下载 全文下载 相似专利 双屏查看 权利要求书 说明书全文 Espacenet 法律信息 同族专利 专利引用
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