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11. 发明申请

US20130139328A1 DISULFIDE OR THIOL POLYMERIC HAIR DYES 有权
标题翻译： DISOLFIDE或THIOL POLYMERIC HAIR DYES
公开(公告)号：US20130139328A1
公开(公告)日：2013-06-06
申请号：US13816527
申请日：2011-08-15
申请人： Sophie Marquais-Bienewald , Christian Cremer , Beate Frohling
发明人： Sophie Marquais-Bienewald , Christian Cremer , Beate Frohling
IPC分类号： C09B67/20
CPC分类号： C09B67/0063 , A61K8/817 , A61K8/84 , A61K8/91 , A61Q5/10 , C09B62/78 , C09B69/101 , C09B69/106
摘要： The present invention relates to the reaction product of (A) a polymeric backbone with (B) A chromophore; and with (C) at least one sulfide containing compound. Very good dyeing results are obtained with this new technology.
摘要翻译：本发明涉及（A）聚合物主链与（B）A发色团的反应产物; 和（C）至少一种含硫化物的化合物。使用这种新技术可以获得非常好的染色结果。

12. 发明授权

US08118883B2 Polymeric hair dyes 有权
标题翻译：聚合染发剂
公开(公告)号：US08118883B2
公开(公告)日：2012-02-21
申请号：US12812785
申请日：2009-01-07
申请人： Sophie Marquais-Bienewald , Christian Cremer , Olof Wallquist , Robert Hochberg
发明人： Sophie Marquais-Bienewald , Christian Cremer , Olof Wallquist , Robert Hochberg
IPC分类号： A61Q5/10 , C07D213/09
CPC分类号： C09B69/106 , A61K8/4946 , A61K8/69 , A61K8/84 , A61K2800/57 , A61Q5/02 , A61Q5/065 , A61Q5/12
摘要： Disclosed are polymeric dyes obtained by the reaction of (a) a basic polycondensate with (b) an electrophilic dye of formula (2) P—X—Ya+ Ana+; wherein the basic polycondensate (a) is obtained by the reaction of (a1) an amine of formula (I) in the presence of an anhydrous solvent with an ammonium salt (a2) with a cyanamide: Wherein P, X, Y, a+, a, a1, a2, An, R1, R2, R3, R4, R5, R6 and A are defined in the claims and in the disclosure. The present invention also relates to compositions comprising these polymeric dyes, to a process for their use for dyeing of organic materials, such as keratin fibers, wool, leather, silk, cellulose or polyamides.
摘要翻译：公开了通过（a）碱性缩聚物与（b）式（2）的亲电子染料P-X-Ya + Ana +的反应获得的聚合染料; 其中碱性缩聚物（a）通过（a1）式（I）的胺在无水溶剂与铵盐（a2）的存在下与氨基氰反应而获得：其中P，X，Y，a +， a，a1，a2，an，R1，R2，R3，R4，R5，R6和A在权利要求书和本公开内容中定义。本发明还涉及包含这些聚合染料的组合物，其用于染色有机材料如角蛋白纤维，羊毛，皮革，丝绸，纤维素或聚酰胺的方法。

13. 发明申请

US20110088173A1 POLYMERIC HAIR DYES 有权
公开(公告)号：US20110088173A1
公开(公告)日：2011-04-21
申请号：US12812785
申请日：2009-01-07
申请人： Sophie Marquais-Bienewald , Christian Cremer , Olof Wallquist , Roberg Hochberg
发明人： Sophie Marquais-Bienewald , Christian Cremer , Olof Wallquist , Roberg Hochberg
IPC分类号： A61K8/41 , A61Q5/10 , C09B44/16
CPC分类号： C09B69/106 , A61K8/4946 , A61K8/69 , A61K8/84 , A61K2800/57 , A61Q5/02 , A61Q5/065 , A61Q5/12
摘要： Disclosed are polymeric dyes obtained by the reaction of (a) a basic polycondensate with (b) an electrophilic dye of formula (2) P—X—Ya+ Ana−; wherein the basic polycondensate (a) is obtained by the reaction of (a1) an amine of formula (I) in the presence of an anhydrous solvent with an ammonium salt (a2) with a cyanamide; wherein R1, R2, R3 and R4 independently from each other are hydrogen; or C1-C4alkyl, which may be substituted by amino, hydroxy, cyano or C1-C4alkoxy; A is C2-C20alkylene, which may be substituted or interrupted by one or more than one hetero atoms; P is a reactive grouping capable of reacting with a nitrogen nucleophile; X is a linkage group selected from C1-C30alkylene, C2-C12alkenylene, C5-C10arylene, C5-C10cycloalkylene and C1-C10alkylene(C5-C10arylene) which may be interrupted and/or terminated at one or both ends by one or more than one —O—, —S—, —N═, —N(R5)—, —S(O)—, SO2, —(CH2CH2—O)1-5—, —(CH2CH2CH2—O)1-5—, —C(O)—, —C(O)O—, —OC(O)—, (II), —CON(R5)—, —C(NR5R6)2—, —(R5)NC(O)—, —C(S)R5— or an optionally substituted, saturated or unsaturated, fused or non-fused aromatic or nonaromatic (hetero)cyclic bivalent radical optionally comprising at least one heteroatom; —O—; —S—; —N(R5)—; —S(O)—; —SO2—; —(CH2CH2—O)1-5—; —C(O)—; —C(O)O—, —OC(O)—; (III); —CON(R5)—; —SO2N(R5)—; —C(NR5R6)2—; —(R5)NC(O)—; —C(S)R5—; saturated or unsaturated, fused or non-fused aromatic or nonaromatic bivalent radical optionally comprising at least one heteroatom; which is optionally substituted by C1-C30alkyl, C1-C30alkoxy, C2-C12alkenyl, C5-C10aryl, C5-C10cycloalkyl, C1-C10alkyl(C5-C10arylene), halogen or hydroxy; or the direct bond; Y is a residue of an organic dye; R5 and R6 independently from each other are hydrogen; unsubstituted or substituted, straight-chain or branched, monocyclic or polycyclic, interrupted or uninterrupted d-C14alkyl; C2-C14alkenyl; C6-C10aryl; C6-C10aryl-C1-C10alkyl; or C5-C10alkyl(C5-C10aryl); a is 1, 2 or 3; and An is an anion. The dyes are distinguished by their depth of shade and their good fastness properties to washing, such as, for example, fastness to light, shampooing and rubbing.

14. 发明申请

US20090151091A1 Triarylmethane Dyes 有权
公开(公告)号：US20090151091A1
公开(公告)日：2009-06-18
申请号：US11992876
申请日：2006-09-27
申请人： Christian Cremer , Olof Wallquist
发明人： Christian Cremer , Olof Wallquist
IPC分类号： A61K8/46 , C07D403/06 , C07C233/88 , C07C229/54 , A61K8/49
CPC分类号： A61K8/46 , A61K8/49 , A61K8/492 , A61Q5/10 , C09B11/04 , C09B49/126
摘要： Disclosed are triarylmethane dyes of formula (1) D1-(Z1J)r-Y1—S-A, wherein A is hydrogen; a radical of formula (1b) *—S—Y2-(Z2)-D2; or a radical of formula (1c) *—S—Y3; Y1 and Y2 independently from each other are unsubstituted or substituted, straight-chain or branched, interrupted or uninterrupted C1-C10alkylene; C5-C10cycloalkylene; C5-C10arylene; or —C5-C10arylene-(C1-C10alkylene); Y3 is an unsubstituted or substituted, straight-chain or branched, interrupted or uninterrupted C1C10alkyl; C5-C10cycloalkyl; C5-C10aryl; or —C5-C10aryl-(C1-C10alkyl); Z1 and Z2 independently from each other are *—(CH2)p—C(O)—**; *—(CH2CH2—O)—**; *—(CH2)p—C(O)O—**; *—(CH2)p—OCO—**; —(CH2)p—N(R1)—**; —(CH2)p—CON(R1)—**; —(CH2)p—(R1)NC(O)—**; -0-; —S—; —S(O)—; —S(O)2—; or a cationic biradical of a substituted or unsubstituted aromatic or heteroaromatic compound of the formula (1a); (1b); (1c); (1d); or (1e); wherein the asterix * indicates the linkage to D1 and/or D2; the asterix ** indicates the linkage to Y1 and/or Y2; W1 is N or a radical of CR5; R1, R2, R3, R4 and R5 independently from each other are hydrogen; C1-C14alkyl; C2-C14alkenyl; C5-C10aryl; C5-C10aryl-(C1-C10alkyl); or —C1-C10alkyl(C5-C10aryl); D1 and D2 independently from each other are hydrogen; or the residue of an organic dye selected from the radical of formula (1f), wherein B1 and B2, independently from each other are C6-C10aryl; or a 5-7-membered heterocyclic compound, which may be substituted by C1-C12alkyl, C1C12alkoxy, phenyl, hydroxy, halogen, sulfonic acid, carboxylate, or by the radical —NR6R7 or —OR6; B3 is C6-C10arylene, or a bivalent radical of a 5-7-membered heterocyclic compound, which may be substituted by C1-C12alkyl, C1-C12alkoxy, phenyl, hydroxy, halogen, sulfonic acid, carboxylate, or by the radical —NR6R7 or —OR6; R6 and R7 independently from each other are hydrogen; or C1-C12alkyl, which may be substituted by hydroxy or C6-C10aryl; or R6 and R7 together with the linking nitrogen atom form a 5 to 7 membered heterocyclic ring; or R6 and R7 together with the linking nitrogen atom form a piperidine ring of formula (1b)* 1H **. wherein the asterix(*) is directed to Z1 or Z2 respectively; and the asterix(**) is directed to the linking nitrogen atom; wherein one of D1 and D2 is not hydrogen; An is an anion; p is a number from O to 5; r is O or 1; and s is a number from 1 to 5. The compounds are useful for the dyeing of organic materials, such as keratin fibers, preferably human hair.

15. 发明授权

US08221508B2 Polymeric hair dyes 有权
标题翻译：聚合染发剂
公开(公告)号：US08221508B2
公开(公告)日：2012-07-17
申请号：US13133234
申请日：2009-12-04
申请人： Sophie Marquais-Bienewald , Christian Cremer , Olof Wallquist , Xian-Zhi Zhou , Barbara Wagner
发明人： Sophie Marquais-Bienewald , Christian Cremer , Olof Wallquist , Xian-Zhi Zhou , Barbara Wagner
IPC分类号： A61Q5/10 , C07D213/22
CPC分类号： A61K8/64 , A61K8/645 , A61K8/65 , A61K2800/4322 , A61Q5/065 , C09B69/10 , C09B69/101 , C09B69/106
摘要： Polymeric dye comprising oligo and polypeptides selected from natural or synthetic aminoacids bearing at least one covalently bounded cationic dye. Very good dyeing results on human hair are obtained with these dyes.
摘要翻译：包含寡核苷酸和多肽的聚合染料选自具有至少一种共价结合阳离子染料的天然或合成氨基酸。用这些染料获得人毛发上的非常好的染色结果。

16. 发明授权

US08118882B2 Polymeric hair dyes 有权
标题翻译：聚合染发剂
公开(公告)号：US08118882B2
公开(公告)日：2012-02-21
申请号：US12812782
申请日：2009-01-07
申请人： Christian Cremer , Sophie Marquais-Bienewald , Olof Wallquist
发明人： Christian Cremer , Sophie Marquais-Bienewald , Olof Wallquist
IPC分类号： A61Q5/10 , C07D213/09
CPC分类号： C09B69/101 , C09B1/32 , C09B1/34 , C09B69/106
摘要： Disclosed are cationic oligomeric dye, comprising a low molecular weight polyamine comprising the repeating units (1a) or (1b), wherein at least 90% of the polyamine molecules are selected from tetramines, pentamines and hexamines; and R is the residue of a cationic dye, which is covalently bonded, optionally via a linker, to the nitrogen atoms of the polyamine; or hydrogen; wherein the polyamine repeating units (1a) and (1b) comprise at least one carionic dye residue; and n is a number from 3-12. The dyes are distinguished by their depth of shade and their good fastness properties to washing, such as, for example, fastness to light, shampooing and rubbing.
摘要翻译：公开了阳离子低聚染料，其包含包含重复单元（1a）或（1b）的低分子量多胺，其中至少90％的多胺分子选自四胺，五胺和六胺; 并且R是阳离子染料的残基，其任选地经由接头共价键合到多胺的氮原子上; 或氢; 其中所述多胺重复单元（1a）和（1b）包含至少一个卡莲染料残基; n是3-12的数字。这些染料的特征在于它们的色调深度和它们对洗涤性能的良好牢度，例如耐光牢度，洗发剂和摩擦性。

17. 发明申请

US20110061180A1 POLYMERIC HAIR DYES 有权
标题翻译：聚合物染发剂
公开(公告)号：US20110061180A1
公开(公告)日：2011-03-17
申请号：US12812782
申请日：2009-01-07
申请人： Christian Cremer , Sophie Marquais-Bienewald , Olof Wallquist
发明人： Christian Cremer , Sophie Marquais-Bienewald , Olof Wallquist
IPC分类号： A61K8/81 , A61Q5/10 , C09B46/00 , C07C211/63
CPC分类号： C09B69/101 , C09B1/32 , C09B1/34 , C09B69/106
摘要： Disclosed are cationic oligomeric dye, comprising a low molecular weight polyamine comprising the repeating units (1a) or (1b), wherein at least 90% of the polyamine molecules are selected from tetramines, pentamines and hexamines; and R is the residue of a cationic dye, which is covalently bonded, optionally via a linker, to the nitrogen atoms of the polyamine; or hydrogen; wherein the polyamine repeating units (1a) and (1b) comprise at least one carionic dye residue; and n is a number from 3-12. The dyes are distinguished by their depth of shade and their good fastness properties to washing, such as, for example, fastness to light, shampooing and rubbing.
摘要翻译：公开了阳离子低聚染料，其包含包含重复单元（1a）或（1b）的低分子量多胺，其中至少90％的多胺分子选自四胺，五胺和六胺; 并且R是阳离子染料的残基，其任选地经由接头共价键合到多胺的氮原子上; 或氢; 其中所述多胺重复单元（1a）和（1b）包含至少一个卡莲染料残基; n是3-12的数字。这些染料的特征在于它们的色调深度和它们对洗涤性能的良好牢度，例如耐光牢度，洗发剂和摩擦性。

18. 发明申请

US20090229059A1 Oxazine Disulfide Dyes 有权
公开(公告)号：US20090229059A1
公开(公告)日：2009-09-17
申请号：US11992878
申请日：2006-09-27
申请人： Christian Cremer , Olof Wallquist
发明人： Christian Cremer , Olof Wallquist
IPC分类号： A61K8/49 , C09B19/00 , C09B17/02 , C09B21/00 , C09B49/06 , A61Q5/10
CPC分类号： C09B19/00 , A61K8/49 , A61Q5/065 , A61Q5/10 , C09B17/02 , C09B21/00 , C09B49/06
摘要： Disclosed are oxazine disulfide dyes of formula (1) D1-(Z1)r-Y1—S-A, wherein A is hydrogen; or a radical of formula (1a)*—S—Y2-(Z2)r-D2; Y1 and Y2 independently from each other are unsubstituted or substituted, straight-chain or branched, interrupted or uninterrupted C—1—C—10alkylene; C5-C10cycloalkylene; C5-C10arylene; or —C5-C10arylene-(C1-C10alkylene); Z1 and Z2 independently from each other are *—(CH2)p—C(O)—**; *—(CH2CH2—O)S—**; *—(CH2)p—C(O)O—**; *—(CH2)p—OCO—**; *—(CH2)P—N(R1)—**; formula 1(g); —(CH2)p—CON(R1)—**; *—(CH2)p—(R1)NC(O)—**; , 0-; —S—; —S(O)—; —S(O)2—; or a cationic biradical of a substituted or unsubstituted aromatic or heteroaromatic compound of the formula (1a); (1b); (1c); (1d); or (1e); wherein the asterix * indicates the linkage to D1 and/or D2; the asterix ** indicates the linkage to Y1 and/or Y2; W1 is N or a radical of CR5; R1, R2, R3, R4 and R5 independently from each other are hydrogen; C1-C14alkyl; C2-C14alkenyl; C5-C10aryl; C5-C10aryl-(C1-C10alkyl); or —C1-C10alkyl(C5-C10aryl); D1 and D2 independently from each other ar the residue of an organic dye selected from the radical of formula (1f); R6 and R7 independently from each other are hydrogen; C1-C20alkyl; C1-C20alkoxy; C3-C6cycloalkyl; C5-C10aryl; anellated aromatic groups; carboxylate; or sulfonate groups; R8, R9 and R10, R11 and R12 each independently from each other are hydrogen; unsubstituted or substituted, straight-chain or branched, monocyclic or polycyclic, interrupted or uninterrupted C1-C14alkyl, C2-C14alkenyl, C6-C10aryl, C6-C10aryl-C1-C10alkyl or C5-C10alkyl(C5-C10aryl); or R8 and R9 or R10 and R11, together with the linking nitrogen atom form a 5 to 7 membered carbocyclic ring which may contain one or more than one hetero atom; or R8 is linked to C1 together with N+ forming a 5-7 membered carbocyclic ring; or R9 is linked to C2 together with N+ forming a 5-7 membered carbocyclic ring; X is —O—; or —N(R9)—; or —S—; p is a number from 0 to 5; r is 0 or 1; and s is a number from 1 to 5. The compounds are useful for the dyeing of organic materials, such as keratin fibers, preferably human hair.

19. 发明申请

US20090130045A1 Nitrosulfide dyes 有权
公开(公告)号：US20090130045A1
公开(公告)日：2009-05-21
申请号：US11921810
申请日：2006-06-14
申请人： Christian Cremer , Olof Wallquist
发明人： Christian Cremer , Olof Wallquist
IPC分类号： A61K8/46 , C07C321/20
CPC分类号： A61Q5/10 , A61K8/418 , A61K8/46 , C09B49/02 , C09B51/00
摘要： Disclosed are nitro-sulfide dyes of formula (1), their salts, isomers, hydrates and other solvates, wherein R1, R2, R3, independently from each other are hydrogen; C1-C20alkyl or C1-C20alkoxy, which may be substituted by one or more C1-C5alkoxy, halogen, —NH2, mono-C1-C5alkylamino, di-C1-C5alkylamino, —NO2 or hydroxy; C3-C6cycloalkyl; —C(O)H; —C(O)—C1-C5alkyl; —C(O)OH; —C(O)O—C1-C5alkyl; halogen; NO2; OH; SH; phenyl, which may be substituted by one or more C1-C5alkyl, C1-C5alkoxy, halogen, —NH2, mono-C1-C5alkylamino, di-C1-C5alkylamino, —NO2 or hydroxy; or a radical of formula (1a) —NR4R5, wherein R4 and R5 independently from each other are hydrogen; C1-C12alkyl, which may be substituted by one or more C1-C5alkyl, C1-C5-alkoxy, hydroxy or —(CO)—H; —(CO)—C1-C5alkyl; phenyl or phenyl-C1-C4alkyl, wherein the phenyl moiety may be substituted by one or more C1-C5alkyl, C1-C5alkoxy, halogen, —NH2, mono-C1-C5alkylamino, di-C1-C5alkylamino, —NO2, carboxy or hydroxy; or a radical of formula (2); wherein at least one of the radicals R1, R2 or R3 is NO2; Y1 is C1-C10alkylene; C5-C10cycloalkylene; C5-C10arylene; or C5-C10arylene-(C1-C10alkylene); Z1 is the direct bond; formula (3); or a cationic biradical of a saturated, aromatic or heteroaromatic group; Q1 is —C(O)—; —C(O)O—; —OCO—; —N(R6)—X2—; —CON(R6)—; —(R6)NC(O)—; —O—; —S—; —S(O)—; or —S(O)2—; X1 and X2 independently from each other are the direct bond; C1-C10alkylene; C5-C10cycloalkylene; C5-C10arylene; or C5-C10arylene-(C1-C10alkylene); and R6, R7 and R8 independently from each other are hydrogen; C1-C14alkyl; C2-C14alkenyl; C6-C10aryl; C6-C10aryl-C1-C10alkyl; or C1-C10alkyl(C5-C10aryl); m is 1; or 2; U is hydrogen, if m is 1; or the direct bond, if m is 2; with the proviso that the method does not comprise contacting hair with an enzyme of the type of a protein disulfidisomerase (EC 5.3.4.1). Further, the present invention relates to novel sulfide compounds, compositions thereof, especially comprising other dyes, and to processes for their preparation.

20. 发明申请

US20110296631A1 POLYMERIC HAIR DYES 有权
标题翻译：聚合物染发剂
公开(公告)号：US20110296631A1
公开(公告)日：2011-12-08
申请号：US13133234
申请日：2009-12-04
申请人： Sophie Marquais-Bienewald , Christian Cremer , Olof Wallquist , Xian-Zin Zhou , Barbara Wagner
发明人： Sophie Marquais-Bienewald , Christian Cremer , Olof Wallquist , Xian-Zin Zhou , Barbara Wagner
IPC分类号： A61K8/88 , C07K14/00 , C07K2/00 , A61Q5/10
CPC分类号： A61K8/64 , A61K8/645 , A61K8/65 , A61K2800/4322 , A61Q5/065 , C09B69/10 , C09B69/101 , C09B69/106
摘要： Polymeric dye comprising oligo and polypeptides selected from natural or synthetic aminoacids bearing at least one covalently bounded cationic dye. Very good dyeing results on human hair are obtained with these dyes.
摘要翻译：包含寡核苷酸和多肽的聚合染料选自具有至少一种共价结合阳离子染料的天然或合成氨基酸。用这些染料获得人毛发上的非常好的染色结果。

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