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11. 发明公开

EP2771289A1 CONCENTRATION OF SUSPENSIONS 审中-公开
标题翻译： KONZENTRATION AUS SUSPENSIONEN
公开(公告)号：EP2771289A1
公开(公告)日：2014-09-03
申请号：EP12775508.0
申请日：2012-10-24
申请人： BASF SE
发明人： BERGER, Alexsandro , ADKINS, Stephen , HESS, Stephan
IPC分类号： C02F1/56 , C02F1/72
CPC分类号： C02F1/54 , C02F1/56 , C02F1/722 , C02F1/725 , C02F1/76 , C02F1/78 , C02F2305/14
摘要： A process of concentrating a suspension of solid particles in an aqueous medium comprising introducing into the suspension at least one organic polymeric flocculant and addition of an agent system, in which the solid particles in the suspension are flocculated by the action of the at least one organic polymeric flocculant and the so formed flocculated solid particles settle to form a settled layer of solids suspended in the aqueous medium, wherein the agent system comprises: i) at least one oxidising agent; ii) at least one control agent,
摘要翻译：将固体颗粒的悬浮液浓缩在水性介质中的方法，包括将至少一种有机聚合物絮凝剂引入悬浮液中并加入试剂体系，其中悬浮液中的固体颗粒通过至少一种有机物的作用而絮凝聚合物絮凝剂和如此形成的絮凝固体颗粒沉降以形成悬浮在水性介质中的固体沉降层，其中所述试剂体系包括：i）至少一种氧化剂; ii）至少一种控制剂，

12. 发明公开

EP2696986A1 DIAMINE COMPOUNDS AND THEIR USE FOR INVERSE FROTH FLOTATION OF SILICATE FROM IRON ORE 失效
标题翻译：二胺和它们用于铁矿石的二氧化硅反泡沫
公开(公告)号：EP2696986A1
公开(公告)日：2014-02-19
申请号：EP12715891.3
申请日：2012-04-04
申请人： BASF SE
发明人： BITTNER, Christian , NIEBERLE, Jörg , VACANO, Bernhard, Ulrich, von , BERGER, Alexsandro , BÖHN, Roland , OETTER, Günter
IPC分类号： B03D1/01 , B03D1/004 , B03D103/04 , B03D101/02
CPC分类号： B03D1/01 , B03D1/0043 , B03D1/02 , B03D2201/02 , B03D2203/04 , C07C233/17 , C07C233/18
摘要： The invention concerns a process for enriching an iron mineral from a silicate containing iron ore by inverse flotation comprising the addition of a collector or collector composition comprising at least one of the compounds of formulae RC(0)N(Z-0-X-NH
2 )
2 (la); RC(0)N(Z-0-X-NH
2 )
2 H
+ Y
- (lb); in which X is an aliphatic alkylene group containing 2 to 6 carbon atoms; Z is an aliphatic alkylene group containing 2 to 6 carbon atoms; Y
- is an anion; and R is a saturated or unsaturated, linear or branched, aliphatic or aromatic moiety having between 7 and 23 carbon atoms. The invention also relates to the novel compounds according to formulae (la) and (lb), compositions comprising said compounds and the use of compounds and formulations as collectors for enriching of iron mineral.

13. 发明授权

EP2696985B1 INVERSE FROTH FLOTATION PROCESS FOR THE SEPARATION OF SILICATE FROM IRON ORE WITH AMINE AND DIAMINE COMPOUNDS 有权
标题翻译：用胺和二胺化合物从铁矿中分离硅酸盐的反浮选浮选工艺
公开(公告)号：EP2696985B1
公开(公告)日：2018-02-21
申请号：EP12713724.8
申请日：2012-04-10
申请人： BASF SE
发明人： BITTNER, Christian , VACANO, Bernhard Ulrich von , BERGER, Alexsandro , BÖHN, Roland , OETTER, Günter , NIEBERLE, Jörg
IPC分类号： B03D1/01 , B03D103/04 , B03D101/02
CPC分类号： B03D1/01 , B03D1/016 , B03D1/02 , B03D2201/02 , B03D2201/04 , B03D2201/06 , B03D2203/04
摘要： Compounds of the formulae: RO—X—NH2 (Ia); RO—X—NH3+Y− (Ib); RO—X—NH—Z—NH2 (IIa); and RO—X—NH—Z—NH3+Y− (IIb), in which X is an aliphatic alkylene group containing 2 to 6 carbon atoms; Z is an aliphatic alkylene group containing 2 to 6 carbon atoms; Y− is an anion; and R is an aliphatic iso C13H27-group with average branching degree ranging from 1.5 to 3.5. The compounds are particularly suitable as flotation collectors for enriching an iron mineral from a silicate-containing iron ore.

14. 发明授权

EP2696986B1 DIAMINE COMPOUNDS AND THEIR USE FOR INVERSE FROTH FLOTATION OF SILICATE FROM IRON ORE 失效
标题翻译：二胺和它们用于铁矿石的二氧化硅反泡沫
公开(公告)号：EP2696986B1
公开(公告)日：2015-09-30
申请号：EP12715891.3
申请日：2012-04-04
申请人： BASF SE
发明人： BITTNER, Christian , NIEBERLE, Jörg , VACANO, Bernhard, Ulrich, von , BERGER, Alexsandro , BÖHN, Roland , OETTER, Günter
IPC分类号： B03D1/01 , B03D1/004 , B03D103/04 , B03D101/02
CPC分类号： B03D1/01 , B03D1/0043 , B03D1/02 , B03D2201/02 , B03D2203/04 , C07C233/17 , C07C233/18

15. 发明授权

EP2882878B1 METAL LEACH AND RECOVERY PROCESS 有权
标题翻译： METALLLAUGUNGS-和恢复过程
公开(公告)号：EP2882878B1
公开(公告)日：2016-10-12
申请号：EP13745846.9
申请日：2013-08-07
申请人： BASF SE
发明人： NISBETT, Andrew , ADKINS, Stephen , FLANAGAN, Ian John , BERGER, Alexsandro
IPC分类号： C22B3/20 , B01D21/01 , C22B15/00
CPC分类号： C22B3/44 , B01D21/01 , C22B3/04 , C22B3/205 , C22B15/0084 , Y02P10/234 , Y02P10/236
摘要： The present invention relates to a metal leach and recovery process. The process involves subjecting a metal bearing material to a reactive process by combining said metal bearing material with a leaching agent to liberate at least one metal value and forming a first aqueous leach pulp. This first aqueous leach pulp is subjected to a solid liquid separation step thereby providing a first clarified aqueous leach solution and a second aqueous leach pulp. The first clarified aqueous leach solution is then subjected to solvent extraction thereby obtaining the first aqueous raffinate. The second aqueous leach pulp is subjected to at least two further solid liquid separation steps of which some or all are in a counter current decantation (CCD) arrangement. Each of the solid liquid separation steps of the CCD arrangement results in an aqueous liquor and aqueous suspension of solids wherein each aqueous suspension of solids resulting from each solid liquid separation step of the CCD arrangement is passed to the subsequent solid liquid separation step and the suspension of solids resulting from the final solid liquid separation step is removed from the process. Further, each aqueous liquor resulting from each solid liquid separation step of the CCD arrangement is passed to the previous solid liquid separation step. The further solid liquid separation steps result in at least one further clarified aqueous leach solution. The at least one further clarified aqueous leach solution is/are subjected to solvent extraction thereby obtaining at least one further aqueous raffinate. At least a portion of the one or more of the at least one further aqueous raffinates is fed into the final solid liquid separation is of the CCD arrangement. The process provides a flocculation system comprising either: (i) addition of an organic polymeric flocculant to or prior to at least one solid liquid separation step, which polymeric flocculant is formed from 2-acrylamido-2-methylpropane sulphonic acid (ATBS) or salts thereof as a homopolymer or copolymer with at least one water-soluble ethylenically unsaturated monomer; or (ii) addition of an organic polymeric flocculant and at least one support agent to or prior to at least one solid liquid separation step, which at least one support agent is selected from at least one of the group consisting of oxidizing agents, reducing agents, irradiation and free radical producing agents. The process provides significantly improved metal extraction and recovery.

16. 发明公开

EP2588500A1 COPOLYMERS OF MONOCARBOXYLIC ACIDS AND DICARBOXYLIC ACIDS, THEIR PREPARATION AND USE 有权
标题翻译：一元和二元羧酸，生产和使用的共聚物
公开(公告)号：EP2588500A1
公开(公告)日：2013-05-08
申请号：EP11730269.5
申请日：2011-06-30
申请人： BASF SE
发明人： LAUBENDER, Matthias , HEINTZ, Ewald , SEIDL, Clarissa , URTEL, Bolette , BERGER, Alexsandro
IPC分类号： C08F2/32 , C08F2/38 , C11D1/04
CPC分类号： C08F2/38 , C08F2/32 , C08F4/30 , C08F220/06 , C11D3/3757 , C08F222/06 , C08F230/02
摘要： The invention relates to a process for preparing a polymer by free-radical polymerization of at least one ethylenically unsaturated monocarboxylic acid and/or a salt thereof,at least one ethylenically unsaturated dicarboxylic acid and/or an anhydride and/or a salt thereof,in the presence of hypophosphorous acid and/or a salt thereof. The invention also relates to a polymer composition obtainable by this process. The invention also relates to the use of such a polymer composition as detergent additive, e.g. as dispersant, scale inhibitor or sequestrant for laundry detergents.

17. 发明授权

EP2588500B1 COPOLYMERS OF MONOCARBOXYLIC ACIDS AND DICARBOXYLIC ACIDS, THEIR PREPARATION AND USE 有权
标题翻译：一元和二元羧酸，生产和使用的共聚物
公开(公告)号：EP2588500B1
公开(公告)日：2016-08-10
申请号：EP11730269.5
申请日：2011-06-30
申请人： BASF SE
发明人： LAUBENDER, Matthias , HEINTZ, Ewald , GIEGER, Clarissa , URTEL, Bolette , BERGER, Alexsandro
IPC分类号： C08F220/06 , C08F4/30
CPC分类号： C08F2/38 , C08F2/32 , C08F4/30 , C08F220/06 , C11D3/3757 , C08F222/06 , C08F230/02

18. 发明公开

EP2882878A1 METAL LEACH AND RECOVERY PROCESS 有权
标题翻译： METALLLAUGUNGS- UNDRÜCKGEWINNUNGSPROZESS
公开(公告)号：EP2882878A1
公开(公告)日：2015-06-17
申请号：EP13745846.9
申请日：2013-08-07
申请人： BASF SE , BASF Schweiz AG
发明人： NISBETT, Andrew , ADKINS, Stephen , FLANAGAN, Ian John , BERGER, Alexsandro
IPC分类号： C22B3/20 , B01D21/01 , C22B15/00
CPC分类号： C22B3/44 , B01D21/01 , C22B3/04 , C22B3/205 , C22B15/0084 , Y02P10/234 , Y02P10/236
摘要： The present invention relates to a metal leach and recovery process. The process involves subjecting a metal bearing material to a reactive process by combining said metal bearing material with a leaching agent to liberate at least one metal value and forming a first aqueous leach pulp. This first aqueous leach pulp is subjected to a solid liquid separation step thereby providing a first clarified aqueous leach solution and a second aqueous leach pulp. The first clarified aqueous leach solution is then subjected to solvent extraction thereby obtaining the first aqueous raffinate. The second aqueous leach pulp is subjected to at least two further solid liquid separation steps of which some or all are in a counter current decantation (CCD) arrangement. Each of the solid liquid separation steps of the CCD arrangement results in an aqueous liquor and aqueous suspension of solids wherein each aqueous suspension of solids resulting from each solid liquid separation step of the CCD arrangement is passed to the subsequent solid liquid separation step and the suspension of solids resulting from the final solid liquid separation step is removed from the process. Further, each aqueous liquor resulting from each solid liquid separation step of the CCD arrangement is passed to the previous solid liquid separation step. The further solid liquid separation steps result in at least one further clarified aqueous leach solution. The at least one further clarified aqueous leach solution is/are subjected to solvent extraction thereby obtaining at least one further aqueous raffinate. At least a portion of the one or more of the at least one further aqueous raffinates is fed into the final solid liquid separation is of the CCD arrangement. The process provides a flocculation system comprising either: (i) addition of an organic polymeric flocculant to or prior to at least one solid liquid separation step, which polymeric flocculant is formed from 2-acrylamido-2-methylpropane sulphonic acid (ATBS) or salts thereof as a homopolymer or copolymer with at least one water-soluble ethylenically unsaturated monomer; or (ii) addition of an organic polymeric flocculant and at least one support agent to or prior to at least one solid liquid separation step, which at least one support agent is selected from at least one of the group consisting of oxidizing agents, reducing agents, irradiation and free radical producing agents. The process provides significantly improved metal extraction and recovery.
摘要翻译：本发明涉及金属浸出和回收方法。该方法包括通过将所述金属轴承材料与浸出剂组合以使金属轴承材料进行反应过程以释放至少一种金属值并形成第一含水浸出纸浆。将该第一含水浸出纸浆进行固液分离步骤，从而提供第一澄清水溶液浸出溶液和第二含水浸提纸浆。然后对第一澄清的含水浸出溶液进行溶剂萃取，从而获得第一含水浸膏。经受至少两个另外的固体液体分离步骤，其中一些或全部是反向倾析（CCD）布置。 CCD装置的每个固体液体分离步骤都得到含水液体和固体含水悬浮液，其中由CCD装置的每个固体液体分离步骤得到的固体的每个含水悬浮液被传送到随后的固体液体分离步骤，悬浮液从最终固液分离步骤得到的固体从该方法中除去。此外，由CCD装置的每个固体液体分离步骤产生的每个含水液体被传递到先前的固体分离步骤。进一步的固体液体分离步骤导致至少一种进一步澄清的含水浸出溶液。对至少一种进一步澄清的含水浸出溶液进行溶剂萃取，从而获得至少一种其它含水萃余液。至少一种其中一种或多种另外的含水溶剂的至少一部分进料到CCD装置的最终固液分离中。该方法提供了一种絮凝体系，其包括：（i）在至少一个固体液体分离步骤之前或之前加入有机聚合物絮凝剂，该聚合物絮凝剂由2-丙烯酰氨基-2-甲基丙烷磺酸（ATBS）或其盐形成作为与至少一种水溶性烯属不饱和单体的均聚物或共聚物; 或（ii）在至少一个固体液体分离步骤之前或之前加入有机聚合物絮凝剂和至少一种载体剂，所述至少一种载体剂选自氧化剂，还原剂，照射和自由基生成剂。该方法提供了显着改进的金属萃取和回收。

19. 发明公开

EP2696985A2 AMINE AND DIAMINE COMPOUNDS AND THEIR USE FOR INVERSE FROTH FLOTATION OF SILICATE FROM IRON ORE 有权
标题翻译：阿明二胺及其用途由铁矿石二氧化硅反泡沫
公开(公告)号：EP2696985A2
公开(公告)日：2014-02-19
申请号：EP12713724.8
申请日：2012-04-10
申请人： BASF SE
发明人： BITTNER, Christian , VACANO, Bernhard Ulrich von , BERGER, Alexsandro , BÖHN, Roland , OETTER, Günter , NIEBERLE, Jörg
IPC分类号： B03D1/01 , B03D103/04 , B03D101/02
CPC分类号： B03D1/01 , B03D1/016 , B03D1/02 , B03D2201/02 , B03D2201/04 , B03D2201/06 , B03D2203/04
摘要： Compounds of the formulae: RO—X—NH2 (Ia); RO—X—NH3+Y− (Ib); RO—X—NH—Z—NH2 (IIa); and RO—X—NH—Z—NH3+Y− (IIb), in which X is an aliphatic alkylene group containing 2 to 6 carbon atoms; Z is an aliphatic alkylene group containing 2 to 6 carbon atoms; Y− is an anion; and R is an aliphatic iso C13H27-group with average branching degree ranging from 1.5 to 3.5. The compounds are particularly suitable as flotation collectors for enriching an iron mineral from a silicate-containing iron ore.

20. 发明公开

EP2696984A2 AMINE AND DIAMINE COMPOUNDS AND THEIR USE FOR INVERSE FROTH FLOTATION OF SILICATE FROM IRON ORE 审中-公开
标题翻译：阿明二胺及其用途由铁矿石二氧化硅反泡沫
公开(公告)号：EP2696984A2
公开(公告)日：2014-02-19
申请号：EP12712668.8
申请日：2012-04-10
申请人： BASF SE
发明人： BITTNER, Christian , NIEBERLE, Jörg , VON VACANO, Bernhard, Ulrich , BERGER, Alexsandro , BÖHN, Roland , OETTER, Günter
IPC分类号： B03D1/01 , C07C29/34 , C07C217/08 , B03D101/02 , B03D103/04
CPC分类号： B03D1/02 , B03D1/01 , B03D1/016 , B03D2201/02 , B03D2201/04 , B03D2201/06 , B03D2203/04 , C07C29/34 , C07C217/08
摘要： The invention relates to a process for enriching an iron mineral from a silicate containing iron ore by inverse flotation comprising the addition of a collector or collector composition comprising at least one of the compounds of formulae RO-X-NH
2 (Ia); RO-X-NH
3
+ Y
- (Ib);RO-X-NH-Z-NH
2 (IIa); and RO-X-NH-Z-NH
3
+ Y
- (IIb), in which X is a linear or branched aliphatic alkylene group containing 2 to 6 carbon atoms; Z is a linear or branched aliphatic alkylene group containing 2 to 6 carbon atoms; Y- is an anion; and R is an aliphatic group of the formula (I) C
5 H
11 CH(C
3 H
7 )CH
2 - (I) wherein the C
5 H
11 moeity of the aliphatic group of the formula (I) comprises 70 to 99% by weight n-C
5 H
11 -, and 1 to 30% by weight C
2 H
5 CH(CH
3 )CH
2 - and/or CH
3 CH(CH
3 )CH
2 CH
2 -.

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