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11. 发明授权

US08124667B2 Method for grafting a fluorinated polymer and multilayer structures comprising said grafted fluoropolymer 失效
标题翻译：含氟聚合物的接枝方法和包含所述接枝的含氟聚合物的多层结构
公开(公告)号：US08124667B2
公开(公告)日：2012-02-28
申请号：US10584876
申请日：2004-12-28
申请人： Anthony Bonnet , Fabrice Chopinez , Pascal Sebire , Karine Triballier , Michael Werth , Michaela Steng
发明人： Anthony Bonnet , Fabrice Chopinez , Pascal Sebire , Karine Triballier , Michael Werth , Michaela Steng
IPC分类号： C08F275/00 , C08F259/00
CPC分类号： B32B27/28 , B32B27/08 , B32B27/18 , B32B27/304 , B32B27/32 , B32B27/34 , B32B2439/00 , B32B2553/00 , B32B2597/00 , C08F259/08 , C08L51/003 , C08L2666/02
摘要： The present invention relates to a method for radiation grafting a compound by irradiation, that can be grafted onto a fluoropolymer, so as to prevent destabilization of the fluorinated polymer. Said method comprises the following steps: a) the fluoropolymer is mixed in the melted state thereof with a graftable compound; b) the mixture obtained in a) is converted into films, plates, granulates or powder; c) the products from step b) are subjected to photonic (γ) or electronic (β) irradiation in a dose of between 0.5 and 15 Mrad; and d) optionally, the products from step c) are washed and/or a degassed. According to said method, a stabilizing agent is added to the fluorinated polymer. Said stabilizing agent can be an antioxidant, a graftable metal salt, or a combination of the two. The invention also relates to structures comprising at least one layer of said mixtures and at least one layer of another material, and to the use of said structures to obtain a barrier effect. Said structures act as a barrier to a plurality of fluids, especially to petrol and to air-conditioning fluids, and can take the form of bottles, tanks, containers, pipes, and all kinds of recipients. They can also be transformed into films used to produce packaging.
摘要翻译：本发明涉及通过辐射将化合物辐射接枝的方法，其可以接枝到含氟聚合物上，以防止氟化聚合物的不稳定。所述方法包括以下步骤：a）将含氟聚合物在其熔融状态下与可接枝化合物混合; b）将a）中得到的混合物转化成薄膜，板，颗粒或粉末; c）来自步骤b）的产物以0.5至15Mrad的剂量进行光子（γ）或电子（＆bgr）照射; 和d）任选地，来自步骤c）的产物被洗涤和/或脱气。根据所述方法，向氟化聚合物中加入稳定剂。所述稳定剂可以是抗氧化剂，可接枝的金属盐，或两者的组合。本发明还涉及包含至少一层所述混合物和至少一层另一种材料的结构，以及所述结构的使用以获得阻隔效应。所述结构用作对多种流体，特别是汽油和空调流体的屏障，并且可以采取瓶，罐，容器，管道和各种接收器的形式。它们也可以转化成用于生产包装的薄膜。

12. 发明申请

US20070149638A1 Method for grafting a fluorinated polymer and multilayer structures comprising said grafted fluoropolymer 失效
标题翻译：含氟聚合物的接枝方法和包含所述接枝的含氟聚合物的多层结构
公开(公告)号：US20070149638A1
公开(公告)日：2007-06-28
申请号：US10584876
申请日：2004-12-28
申请人： Anthony Bonnet , Fabrice Chopinez , Pascal Sebire , Karine Triballier , Michael Werth , Michaela Steng
发明人： Anthony Bonnet , Fabrice Chopinez , Pascal Sebire , Karine Triballier , Michael Werth , Michaela Steng
IPC分类号： C08J3/28
CPC分类号： B32B27/28 , B32B27/08 , B32B27/18 , B32B27/304 , B32B27/32 , B32B27/34 , B32B2439/00 , B32B2553/00 , B32B2597/00 , C08F259/08 , C08L51/003 , C08L2666/02
摘要： The present invention relates to a method for the radiation grafting of a compound that can be grafted onto a fluoropolymer, so as to prevent destabilization of the fluoropolymer, comprising the following steps: a) the fluoropolymer is melt-blended with a graftable compound; b) the blend obtained at a) is formed into films, sheets, granules or powder; c) the products from step b) are subjected to photon (γ) or electron (β) irradiation with a dose of between 0.5 and 15 Mrad; and d) optionally, the products from step c) are subjected to a washing and/or a degassing operation, and in which a stabilizer is blended into the fluoropolymer. The stabilizer may be an antioxidant, a graftable metal salt or else a combination of the two. The invention also relates to structures comprising at least one layer of these blends and at least one layer of another material. The invention also relates to the use of these structures in order to obtain a barrier effect. These structures form a barrier to many fluids and in particular to petrol and to air-conditioning fluids. These structures may be made in the form of bottles, tanks, containers, pipes, hoses and receptacles of all kinds. They may also be converted into films from which packaging is made.
摘要翻译：本发明涉及可以接枝到含氟聚合物上的化合物的辐射接枝方法，以防止含氟聚合物的不稳定化，包括以下步骤：a）将含氟聚合物与可接枝化合物熔融共混; b）在a）获得的共混物形成薄膜，薄片，颗粒或粉末; c）来自步骤b）的产物以0.5至15Mrad的剂量进行光子（γ）或电子（β）照射; 和d）任选地，来自步骤c）的产物进行洗涤和/或脱气操作，并且将稳定剂掺入含氟聚合物中。稳定剂可以是抗氧化剂，可接枝的金属盐或两者的组合。本发明还涉及包含这些共混物的至少一层和至少一层其它材料的结构。本发明还涉及这些结构用于获得屏障效果的用途。这些结构对许多流体形成屏障，特别是汽油和空调流体。这些结构可以以瓶，罐，容器，管，软管和各种容器的形式制成。它们也可以转化成从其制成包装的薄膜。

13. 发明授权

US09786803B2 Multilayer polyvinylidene films structures 有权
公开(公告)号：US09786803B2
公开(公告)日：2017-10-10
申请号：US14119016
申请日：2012-08-30
申请人： Amy A. Lefebvre , Gregory S. O'Brien , Samuel Devisme , Anthony Bonnet
发明人： Amy A. Lefebvre , Gregory S. O'Brien , Samuel Devisme , Anthony Bonnet
IPC分类号： H01L31/044 , H01L31/048 , H01L31/049 , B32B5/02 , B32B27/08 , B32B27/12 , B32B27/20 , B32B27/30 , B32B27/32 , B32B27/34
CPC分类号： H01L31/048 , B32B5/022 , B32B5/024 , B32B27/08 , B32B27/12 , B32B27/20 , B32B27/304 , B32B27/32 , B32B27/34 , B32B2307/712 , B32B2457/12 , H01L31/049 , Y02E10/50
摘要： The invention relates to a multi-layer weatherable film structure having an outer layer of a highly weatherable film, a layer having a high thermal deformation temperature, an optional tie layer, and a thin layer of polyolefin or polyamide. The highly weatherable film layer preferably is polyvinylidene fluoride. The polyolefin or polyamide layer is less than 500 microns in thickness, and preferably the whole film structure is less than 750 microns thick. The polyolefinjpolyamide side of the film structure can easily be adhered to many different substances—especially polyolefins and polyamides. This film can be used to provide a highly weatherable protective layer a substrate. One useful application for the film is in a photovoltaic module to protect the back side of the module from weathering and abrasion. The multi-layer film structure can be adhered to a typical polyolefin-based encapsulant layer and used as a backsheet encapsulant in a photovoltaic module.

14. 发明申请

US20130053498A1 FLUORINATED POLYMER AND ZINC OXIDE FILM FREE OF ANY ACRYLIC ODOR FOR PHOTOVOLTAIC USE 审中-公开
标题翻译：荧光聚合物和氧化锌薄膜不含任何用于光伏使用的丙烯酸酯
公开(公告)号：US20130053498A1
公开(公告)日：2013-02-28
申请号：US13660301
申请日：2012-10-25
申请人： Anthony Bonnet , Francois Beaume , Nicolas Devaux , Karine Triballier , Stephane Bizet , Frederic Godefroy
发明人： Anthony Bonnet , Francois Beaume , Nicolas Devaux , Karine Triballier , Stephane Bizet , Frederic Godefroy
IPC分类号： C08L27/16 , C08K3/26 , C08K3/22
CPC分类号： C08J5/18 , C08J3/226 , C08J2327/16 , C08J2427/16 , C08K3/22 , C08L27/12 , C08L27/16 , H01L31/0481 , Y02E10/50 , C08L33/12
摘要： The present invention relates to a process for forming a polymeric composition composed of a fluoropolymer and of zinc oxide (ZnO) of nanometric size from an acrylic masterbatch. The polymeric composition is intended for the manufacture of films transparent in the visible region and opaque to UV radiation. More particularly, in the composition according to the invention, the filler is present in a proportion by weight of 0.1 to 10%, preferably of 0.5 to 6%, the ZnO particles have a size ranging from 25 to 40 nm, preferably from 30 to 35 nm, these particles have a surface treatment and the said composition is devoid of acrylic polymers.
摘要翻译：本发明涉及由丙烯酸酯母料形成由含氟聚合物和纳米尺寸的氧化锌（ZnO）组成的聚合物组合物的方法。聚合物组合物用于制造在可见光区域透明且对UV辐射不透明的膜。更具体地说，在根据本发明的组合物中，填料的重量比为0.1〜10％，优选为0.5〜6％，ZnO粒子的粒度为25〜40nm，优选为30〜 35nm，这些颗粒具有表面处理，并且所述组合物没有丙烯酸聚合物。

15. 发明申请

US20120298195A1 MOISTURE-RESISTANT FILM, MADE OF FLUORINATED POLYMER AND INORGANIC OXIDE, FOR PHOTOVOLTAIC USE 审中-公开
标题翻译：防紫外线，氟化聚合物和无机氧化物的制造，用于光伏使用
公开(公告)号：US20120298195A1
公开(公告)日：2012-11-29
申请号：US13522054
申请日：2011-01-07
申请人： Dominique Plee , Dominique Jousset , Francois Beaume , Anthony Bonnet
发明人： Dominique Plee , Dominique Jousset , Francois Beaume , Anthony Bonnet
IPC分类号： H01L31/02 , B32B27/08 , B32B27/20
CPC分类号： H01L51/448 , H01L31/0481 , H01L51/5253 , Y02E10/549 , Y10T428/24975 , Y10T428/256
摘要： The invention relates to a multilayer structure that includes: a layer of a composition including a fluorinated polymer and a zinc oxide (ZnO), said ZnO being present in said composition in the form of particles having a weight proportion of less than 1%, said ZnO particles having a size between 10 to 100 nm, and an adhesion promoter present in the body and/or surface of said layer; and at least one oxide layer (MOx) selected from among silicon oxide and aluminum oxide, and having a thickness of from 20 to 200 nm. Aid structure has excellent properties of transparency within the visible range, excellent properties of opacity to UV rays, as well as good mechanical resistance and aging resistance while having excellent moisture barrier properties. Said structure can thus be advantageously used in the front surface of photovoltaic panels or fro protecting organic light-emitting diodes.
摘要翻译：本发明涉及一种多层结构，其包括：包含氟化聚合物和氧化锌（ZnO）的组合物层，所述ZnO在所述组合物中以重量比例小于1％的颗粒形式存在，所述尺寸在10至100nm之间的ZnO颗粒和存在于所述层的主体和/或表面中的粘合促进剂; 和选自氧化硅和氧化铝中的至少一种氧化物层（MOx），其厚度为20〜200nm。辅助结构在可见光范围内具有优异的透明性，优异的紫外线不透明性以及良好的机械阻力和耐老化性，同时具有优异的防潮性能。因此，所述结构可有利地用于光伏面板的前表面或保护有机发光二极管。

16. 发明授权

US08129024B2 Multi-layer rotational moulding 失效
标题翻译：多层旋转成型
公开(公告)号：US08129024B2
公开(公告)日：2012-03-06
申请号：US11596555
申请日：2005-05-06
申请人： Gregory O'Brien , Anthony Bonnet
发明人： Gregory O'Brien , Anthony Bonnet
IPC分类号： B32B27/36 , B32B27/30 , B32B27/32 , B32B27/40 , B29C53/36
CPC分类号： B32B27/08 , B29C41/003 , B29C41/04 , B29C41/22 , B32B27/28 , B32B27/304 , B32B27/32 , B32B2323/04 , B32B2323/10 , B32B2327/12 , B32B2556/00 , Y10T428/31507 , Y10T428/3154 , Y10T428/3158 , Y10T428/31746 , Y10T428/31797 , Y10T428/31855 , Y10T428/31935 , Y10T428/31938
摘要： This invention discloses a multilayer article prepared by rotational molding that comprises: a) a layer A comprising a functionalized fluoropolymer; b) a layer B comprising a non-fluoropolymer containing functional groups; and c) optionally a layer C prepared from a polymer that is dissimilar from that of layer A and that is similar to or dissimilar from that of layer B and is adjacent to layer A and/or layer B and, if present, is characterized in that it has good adhesion to layer A and/or to layer B and is not a blend of layer A and layer B.
摘要翻译：本发明公开了一种通过旋转模塑制备的多层制品，其包括：a）包含官能化含氟聚合物的层A; b）包含含有官能团的非含氟聚合物的层B; 和c）任选地由与层A不同的聚合物制备的层C，其与层B类似或不同于层B并且与层A和/或层B相邻，并且如果存在，则其特征在于它对层A和/或层B具有良好的粘附性，并且不是层A和层B的共混物。

17. 发明授权

US07767757B2 Thermoset materials with improved impact resistance 有权
标题翻译：具有改善耐冲击性的热固性材料
公开(公告)号：US07767757B2
公开(公告)日：2010-08-03
申请号：US11813799
申请日：2006-01-18
申请人： Olivier Guerret , Pierre Gerard , Jean-Pierre Pascault , Anthony Bonnet
发明人： Olivier Guerret , Pierre Gerard , Jean-Pierre Pascault , Anthony Bonnet
IPC分类号： C08L53/00 , C08L63/00 , C08F297/00 , C08F293/00
CPC分类号： C08L53/00 , C08L101/00 , C08L2666/14 , C08L2666/02 , C08L2666/04
摘要： The present invention relates to a thermoset material with improved impact resistance comprising, by weight: •99 to 20% of a thermoset resin, •1 to 80% of an impact modifier comprising at least one copolymer chosen from copolymers comprising A-B-C and A-B blocks, in which: each block is connected to the other by means of a covalent bond or of an intermediate molecule connected to one of the blocks via a covalent bond and to the other block via another covalent bond, A is a copolymer of methyl methacrylate and of at least one water-soluble monomer, C is either (i) a PMMA (homopolymer or copolymer) this PMMA comprising optionally a water-soluble monomer or (ii) a polymer based on vinyl monomers or mixture of vinyl monomers, B is incompatible or partially compatible with the thermoset resin and incompatible with the A block and the optional C block and its glass transition temperature Tg is less than the operating temperature of the thermoset material. The invention also relates to the use of these impact modifiers in thermosets.
摘要翻译：本发明涉及具有改进的抗冲击性的热固性材料，其包含重量百分比：99至20％的热固性树脂，1至80％的抗冲改性剂，其包含至少一种选自包含ABC和AB嵌段的共聚物的共聚物，其中：每个嵌段通过共价键或通过共价键连接到其中一个嵌段的中间分子连接，另一个通过另一个共价键连接到另一个嵌段，A是甲基丙烯酸甲酯和至少一种水溶性单体C是（i）PMMA（均聚物或共聚物），该PMMA包含任选的水溶性单体或（ii）基于乙烯基单体或乙烯基单体混合物的聚合物，B是不相容的或与热固性树脂部分相容并且与A嵌段和任选的C嵌段不相容，并且其玻璃化转变温度Tg小于热固性材料的操作温度。本发明还涉及这些抗冲改性剂在热固性材料中的应用。

18. 发明申请

US20090173407A1 MULTILAYER TUBE FOR TRANSPORTING WATER OR GAS 审中-公开
标题翻译：用于运输水或气的多层管
公开(公告)号：US20090173407A1
公开(公告)日：2009-07-09
申请号：US12094807
申请日：2006-11-23
申请人： Anthony Bonnet , Michael Werth
发明人： Anthony Bonnet , Michael Werth
IPC分类号： F16L9/14 , B32B1/08
CPC分类号： B32B27/08 , B32B1/08 , B32B7/12 , B32B15/08 , B32B27/28 , B32B27/304 , B32B27/306 , B32B27/32 , B32B2323/04 , B32B2327/00 , B32B2329/04 , B32B2597/00 , Y10T428/1383
摘要： The invention concerns a multilayer tube comprising (viewed form inside outwards of the tube): optionally a layer C1 comprising at least one fluorinated polymer; a layer C2 comprising at least one functionalized fluorinated polymer, optionally mixed with at least one fluorinated polymer; a barrier layer C3 comprising a barrier polymer selected among EVOH or a mixture based on EVOH, PGA or PDMK; a layer C4 of an adhering binder; a layer C5 comprising at least one polyolefin, optionally mixed with at least one functionalized polyolefin; optionally a barrier layer C6; optionally a layer C7 comprising at least one polyolefin, optionally mixed with at least one functionalized polyolefin.
摘要翻译：本发明涉及一种多层管，其包括（从该管的内部观察）：任选的包含至少一种含氟聚合物的层C1; 包含至少一种官能化氟化聚合物的层C2，任选地与至少一种含氟聚合物混合; 包含选自EVOH或基于EVOH，PGA或PDMK的混合物的阻隔聚合物的阻挡层C3; 粘合粘合剂的层C4; 包含至少一种聚烯烃的层C5，任选与至少一种官能化聚烯烃混合; 任选的阻挡层C6; 任选的包含至少一种聚烯烃的层C7，任选与至少一种官能化聚烯烃混合。

19. 发明申请

US20080145652A1 Multilayer Film Based on a Fluoropolymer and an Acrylic Polymer 审中-公开
标题翻译：基于含氟聚合物和丙烯酸聚合物的多层膜
公开(公告)号：US20080145652A1
公开(公告)日：2008-06-19
申请号：US11816479
申请日：2006-02-21
申请人： Anthony Bonnet , Sandrine Duc
发明人： Anthony Bonnet , Sandrine Duc
IPC分类号： B32B5/00
CPC分类号： B32B27/28 , B32B7/12 , B32B21/08 , B32B25/08 , B32B27/08 , B32B27/10 , B32B27/304 , B32B27/322 , B32B2250/40 , B32B2262/062 , B32B2307/584 , B32B2307/71 , B32B2307/712 , B32B2307/714 , C08L33/04 , C08L33/16 , C09D133/04 , Y10T428/265 , C08L2666/04
摘要： The invention relates to the use of a multilayer film for protecting a substrate which gives off volatile compounds which comprises: a surface layer comprising, by weight, from 70 to 100%, preferably from 90 to 100%, of a fluoropolymer and from 0 to 30%, preferably from 0 to 10% of an acrylic polymer; an adhesive layer comprising from 50 to 100% of an acrylic polymer, from 0 to 50% of a fluoropolymer, from 1 to 10% of a UV stabilizer and from 0 to 50% of an impact modifier, characterized in that the thickness of the surface layer is between 2 and 15 μm, preferably between 2 and 10 μm, more preferably still between 3 and 8 μm, and the thickness of the adhesive layer is between 30 and 75 μm, preferably between 30 and 60 μm, more preferably still between 30 and 50 μm. The invention also relates to a substrate protected by the multilayer film.
摘要翻译：本发明涉及多层膜用于保护产生挥发性化合物的基质的用途，该基质包括：包含70至100％，优选90至100％的含氟聚合物和0至 30％，优选0至10％的丙烯酸类聚合物; 粘合剂层，包含50-100％的丙烯酸类聚合物，0-50％的含氟聚合物，1-10％的UV稳定剂和0-50％的抗冲改性剂，其特征在于：表层为2至15μm，优选2至10μm，更优选为3至8μm，并且粘合剂层的厚度为30至75μm，优选为30至60μm，更优选为介于 30和50妈妈。本发明还涉及由多层膜保护的基板。

20. 发明申请

US20070078236A1 Reactive thermosetting system with long storage life 审中-公开
标题翻译：具有长寿命的活性热固系统
公开(公告)号：US20070078236A1
公开(公告)日：2007-04-05
申请号：US10585700
申请日：2005-01-07
申请人： Anthony Bonnet , Elisabeth Loerch , Laurent Gervat , Regis Cipriani , Francois Beaume
发明人： Anthony Bonnet , Elisabeth Loerch , Laurent Gervat , Regis Cipriani , Francois Beaume
IPC分类号： C08L63/02
CPC分类号： C08G59/18 , C08J3/24 , C08J2363/00 , C08L63/00 , C08L2666/08 , C09J163/00 , C08L2666/04
摘要： The present invention relates to a process which makes it possible to produce semifinished products, such as reactive textiles or films for composites, starting from two formulations, one based on epoxide resin and on a rheology-control agent and the other based on a hardener and on a rheology-control agent. These semifinished products are stable during storage but they can react together when the temperature is increased to form the desired thermoset material.
摘要翻译：本发明涉及一种方法，其可以从两种制剂，一种基于环氧树脂和一种流变控制剂，另一种基于硬化剂制备半成品，例如用于复合材料的反应性纺织品或薄膜，在流变控制剂上。这些半成品在储存期间是稳定的，但是当温度升高以形成期望的热固性材料时它们可以一起反应。

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