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11. 发明申请

WO2005105911A1 LOW SCORCHING FLAME RETARDANTS FOR POLYURETHANE FOAMS 审中-公开
标题翻译： POLYURETHANE FOAMS的低剪切阻燃剂
公开(公告)号：WO2005105911A1
公开(公告)日：2005-11-10
申请号：PCT/US2005/014166
申请日：2005-04-26
申请人： SUPRESTA LLC , WILLIAMS, Barbara, A. , WEIL, Edward, D. , FESMAN, Gerald , HALCHAK, Theodore , BRIGHT, Danielle, A.
发明人： WILLIAMS, Barbara, A. , WEIL, Edward, D. , FESMAN, Gerald , HALCHAK, Theodore , BRIGHT, Danielle, A.
IPC分类号： C08K5/521
CPC分类号： C08K5/1535 , C08K5/101 , C08K5/521 , C08L75/04
摘要： A flame retardant composition for use in flame retarding a polyurethane foam composition so that the foam has reduced scorch as a result of its manufacture, said flame retardant composition comprising a mixture of (a) a flame retardant of the type that normally causes scorch when used in such foam and (b) a benzofuranone derivative, as a anti-scorch stabilizer. Flame retarded polyurethane foams having reduced discoloration are also provided.
摘要翻译：一种用于阻燃聚氨酯泡沫组合物的阻燃组合物，使得泡沫由于其制造而使焦炭减少，所述阻燃组合物包含（a）当使用时通常引起焦烧的类型的阻燃剂的混合物（b）苯并呋喃酮衍生物作为防焦烧稳定剂。还提供了具有降低的变色的阻燃聚氨酯泡沫。

12. 发明申请

WO1998018802A1 PROCESS FOR MAKING MONOHYDROXY-TERMINATED PHOSPHATE COMPOSITIONS 审中-公开
标题翻译：制备单羟基终止的磷酸酯组合物的方法
公开(公告)号：WO1998018802A1
公开(公告)日：1998-05-07
申请号：PCT/EP1997005983
申请日：1997-10-23
申请人： AKZO NOBEL N.V.
发明人： AKZO NOBEL N.V. , BRIGHT, Danielle, A. , PIRELLI, Ronald, L.
IPC分类号： C07F09/12
CPC分类号： C07F9/12
摘要： The present invention is a process for forming monohydroxy-terminated aromatic oligomeric phosphates by the reaction of a diaryl halophosphate, such as diphenyl chlorophosphate, optionally in the presence of some monoaryl dihalophosphate, with an aromatic diol, such as resorcinol, to form the monohydroxy-terminated aromatic oligomeric phosphate. The reaction preferably employs a Lewis acid catalyst, such as magnesium dichloride.
摘要翻译：本发明是通过二卤代磷酸二苯酯（任选在一些二卤代二芳基酯存在下）与芳族二醇如间苯二酚的反应形成单羟基封端的芳族低聚磷酸酯的方法，形成单羟基封端的芳基低聚磷酸酯，封端的芳族低聚磷酸盐。该反应优选使用路易斯酸催化剂，例如二氯化镁。

13. 发明申请

WO1998004566A1 PROCESS FOR THE FORMATION OF HYDROCARBYL BIS(DIHYDROCARBYL PHOSPHATE) 审中-公开
标题翻译：形成烃基（磷酸二氢锂）的方法
公开(公告)号：WO1998004566A1
公开(公告)日：1998-02-05
申请号：PCT/EP1997003871
申请日：1997-07-14
申请人： AKZO NOBEL N.V.
发明人： AKZO NOBEL N.V. , BRIGHT, Danielle, A. , PIRRELLI, Ronald, L.
IPC分类号： C07F09/12
CPC分类号： C07F9/12 , C07F9/093
摘要： A process for forming a composition containing over, for example, about 90 % by weight of an alkylene-arylene bridging group-containing bis(diphenyl phosphate) compound and less than, for example, 10 % by weight of monophosphate by-product. This process involves the reaction of a composition containing a diphenyl halophosphate and an alkylene-arylene bridging group-containing diol, in the presence of a catalytic amount of a Lewis acid catalyst, utilizing a means, during the course of the reaction, for removal of hydrohalide by-product. The preferred means that are used for removal of hydrohalide by-product include: utilizing vacuum to remove such by-product; utilizing sparging with an inert gas; utilizing vacuum to remove such by-product in combination with performing the reaction in a hydrocarbon solvent; utilizing sparging with an inert gas in combination with performing the reaction in a hydrocarbon solvent; and utilizing vacuum and sparging with an inert gas in combination with performing the reaction in a hydrocarbon solvent to remove such by-product.
摘要翻译：用于形成含有例如约90重量％的含亚烷基 - 亚芳基桥连基的双（二苯基磷酸酯）化合物并且小于例如10重量％的单磷酸酯副产物的组合物的方法。该方法包括在催化量的路易斯酸催化剂的存在下，含有二苯基卤代磷酸酯和亚烷基 - 亚芳基桥连基团的二醇的组合物的反应，利用在反应过程中除去氢卤化物副产物。用于除去氢卤素副产物的优选方法包括：利用真空去除这种副产物; 利用惰性气体喷射; 利用真空除去这种副产物与在烃溶剂中进行反应的组合; 利用惰性气体喷射与在烃溶剂中进行反应的组合; 并与惰性气体一起使用真空和喷射，同时在烃溶剂中进行反应以除去这种副产物。

14. 发明授权

EP1208144B1 PHOSPHORUS-CONTAINING FIRE RETARDANT THERMOPLASTIC POLYESTER COMPOSITION 有权
标题翻译：基于荧光物质，阻燃热塑性聚酯组合物
公开(公告)号：EP1208144B1
公开(公告)日：2005-11-23
申请号：EP00908717.2
申请日：2000-02-18
申请人： Akzo Nobel N.V.
发明人： LEVCHIK, Sergei V. , BRIGHT, Danielle, A. , ALESSIO, Gerald, R.
IPC分类号： C08L67/02 , C08L61/06 , C08K5/521 , C08K5/523 , C08K5/524 , C08K5/00
CPC分类号： C08K5/523 , C08L67/02 , C08L67/03 , C08L61/04
摘要： A fire retardant thermoplastic polyester comprising a phosphorus containing additive and a high charring polymer containing benzene rings in its main polymer backbone and that has a softening point of no less than about 120 °C exhibits improved fire resistance and no plate out of fire retardant additive during aging.

15. 发明授权

EP0789703B1 PROCESS FOR THE FORMATION OF HYDROCARBYL BIS(HYDROCARBYL PHOSPHATE) 失效
标题翻译：生成烃基二（磷酸烃基酯）的方法
公开(公告)号：EP0789703B1
公开(公告)日：2003-04-23
申请号：EP95937516.3
申请日：1995-10-20
申请人： AKZO NOBEL N.V.
发明人： BRIGHT, Danielle, A. , PIRRELLI, Ronald, L.
IPC分类号： C07F9/12 , C07F9/09
CPC分类号： C07F9/093 , C07F9/12
摘要： A process for the synthesis of a hydrocarbyl bis(dihydrocarbyl phosphate), such as a hydrocarbyl bis(diaryl phosphate), comprises the reaction of an unstable hydrocarbyl-containing diol, such as an aromatic group-containing diol, with a dihydrocarbyl halophosphate, such as diphenyl chlorophosphate, in the presence of a Lewis acid catalyst, such as magnesium dichloride, in the additional presence of an effective amount (e.g., up to about 100 % by weight of diol and halophosphate) of a liquid hydrocarbon, such as an aliphatic hydrocarbon, like heptane, or an aromatic hydrocarbon, such as toluene, to enhance the removal of hydrogen halide by-product and thereby increase the yield of hydrocarbyl bis(dihydrocarbyl phosphate).
摘要翻译：合成烃基双（二烃基磷酸酯）例如烃基双（二芳基磷酸酯）的方法包括使不稳定的含烃基二醇如含芳族基团的二醇与卤代磷酸二烃基酯反应，例如作为氯代磷酸二苯酯，在路易斯酸催化剂例如二氯化镁的存在下，在另外存在有效量（例如至多约100重量％的二醇和卤代磷酸盐）的液态烃例如脂族烃如庚烷或芳烃如甲苯，以增强卤化氢副产物的除去，从而提高烃基双（二烃基磷酸酯）的产率。

16. 发明授权

EP0937087B1 MONOHYDROXY-TERMINATED PHOSPHATES AND THEIR USE AS FLAME RETARDANTS 失效
标题翻译：磷酸终止MONOHYDROXYREST和它们作为阻燃剂
公开(公告)号：EP0937087B1
公开(公告)日：2003-09-10
申请号：EP97950045.1
申请日：1997-10-23
申请人： Akzo Nobel N.V.
发明人： BRIGHT, Danielle, A. , PIRELLI, Ronald, L.
IPC分类号： C07F9/12
CPC分类号： C07F9/12
摘要： The present invention is a process for forming monohydroxy-terminated aromatic oligomeric phosphates by the reaction of a diaryl halophosphate, such as diphenyl chlorophosphate, optionally in the presence of some monoaryl dihalophosphate, with an aromatic diol, such as resorcinol, to form the monohydroxy-terminated aromatic oligomeric phosphate. The reaction preferably employs a Lewis acid catalyst, such as magnesium dichloride.

17. 发明公开

EP1456290A1 NON-HALOGENATED PHOSPHATE ANTI-SCORCH ADDITIVE FOR POLYURETHANE FOAM 审中-公开
标题翻译： ANTI-烧焦无卤磷酸酯等附加POLYURETHANSCHAEUME
公开(公告)号：EP1456290A1
公开(公告)日：2004-09-15
申请号：EP02795961.8
申请日：2002-12-19
申请人： AKZO NOBEL N.V.
发明人： WILLIAMS, Barbara, A. , BRIGHT, Danielle, A. , PINZONI, Emanuel
IPC分类号： C08K5/523 , C08L75/04
CPC分类号： C08G18/48 , C08G2101/0008 , C08G2101/0083 , C08K5/523 , C08L75/04
摘要： Non-halogen, flame-retardant polyurethane foam compositions having reduced discoloration or scorch during their manufacture contain an effective amount of a flame retardant of the formula: where Ar is an aryl or an alkaryl group, R is neopentylene, and the average value of n is 1 to 10

18. 发明授权

EP0915891B1 PROCESS FOR THE FORMATION OF HYDROCARBYL BIS(DIHYDROCARBYL PHOSPHATE) 失效
标题翻译： METHOD FOR REPRESENTING烃基双（烃基磷酸酯）
公开(公告)号：EP0915891B1
公开(公告)日：2002-01-02
申请号：EP97932839.0
申请日：1997-07-14
申请人： Akzo Nobel N.V.
发明人： BRIGHT, Danielle, A. , PIRRELLI, Ronald, L.
IPC分类号： C07F9/12
CPC分类号： C07F9/12 , C07F9/093
摘要： A process for forming a composition containing over, for example, about 90 % by weight of an alkylene-arylene bridging group-containing bis(diphenyl phosphate) compound and less than, for example, 10 % by weight of monophosphate by-product. This process involves the reaction of a composition containing a diphenyl halophosphate and an alkylene-arylene bridging group-containing diol, in the presence of a catalytic amount of a Lewis acid catalyst, utilizing a means, during the course of the reaction, for removal of hydrohalide by-product. The preferred means that are used for removal of hydrohalide by-product include: utilizing vacuum to remove such by-product; utilizing sparging with an inert gas; utilizing vacuum to remove such by-product in combination with performing the reaction in a hydrocarbon solvent; utilizing sparging with an inert gas in combination with performing the reaction in a hydrocarbon solvent; and utilizing vacuum and sparging with an inert gas in combination with performing the reaction in a hydrocarbon solvent to remove such by-product.

19. 发明公开

EP0915891A1 PROCESS FOR THE FORMATION OF HYDROCARBYL BIS(DIHYDROCARBYL PHOSPHATE) 失效
标题翻译： METHOD FOR REPRESENTING烃基双（烃基磷酸酯）
公开(公告)号：EP0915891A1
公开(公告)日：1999-05-19
申请号：EP97932839.0
申请日：1997-07-14
申请人： Akzo Nobel N.V.
发明人： BRIGHT, Danielle, A. , PIRRELLI, Ronald, L.
IPC分类号： C07F9
CPC分类号： C07F9/12 , C07F9/093
摘要： A process for forming a composition containing over, for example, about 90 % by weight of an alkylene-arylene bridging group-containing bis(diphenyl phosphate) compound and less than, for example, 10 % by weight of monophosphate by-product. This process involves the reaction of a composition containing a diphenyl halophosphate and an alkylene-arylene bridging group-containing diol, in the presence of a catalytic amount of a Lewis acid catalyst, utilizing a means, during the course of the reaction, for removal of hydrohalide by-product. The preferred means that are used for removal of hydrohalide by-product include: utilizing vacuum to remove such by-product; utilizing sparging with an inert gas; utilizing vacuum to remove such by-product in combination with performing the reaction in a hydrocarbon solvent; utilizing sparging with an inert gas in combination with performing the reaction in a hydrocarbon solvent; and utilizing vacuum and sparging with an inert gas in combination with performing the reaction in a hydrocarbon solvent to remove such by-product.

20. 发明公开

EP0937087A1 PROCESS FOR MAKING MONOHYDROXY-TERMINATED PHOSPHATE COMPOSITIONS 失效
标题翻译：用于生产磷酸盐组合物终止MONOHYDROXYREST
公开(公告)号：EP0937087A1
公开(公告)日：1999-08-25
申请号：EP97950045.0
申请日：1997-10-23
申请人： Akzo Nobel N.V.
发明人： BRIGHT, Danielle, A. , PIRELLI, Ronald, L.
IPC分类号： C07F9
CPC分类号： C07F9/12
摘要： The present invention is a process for forming monohydroxy-terminated aromatic oligomeric phosphates by the reaction of a diaryl halophosphate, such as diphenyl chlorophosphate, optionally in the presence of some monoaryl dihalophosphate, with an aromatic diol, such as resorcinol, to form the monohydroxy-terminated aromatic oligomeric phosphate. The reaction preferably employs a Lewis acid catalyst, such as magnesium dichloride.

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